The following report describes two rapid, micro methods for the determination of UNH in Redox waste samples that had been developed fir the concentration range 0.2 to 100 g/l.

Introduction: This report embodies the results of an investigation as to the possibility of removing the bulk of the iron from gunk solutions of various concentrations by precipitation of the iron with phthallic acid and subsequent precipitation of tuballoy. The method consists of dissolving the phthallic acid in the gunk solution and then adding NH₃ to a suitable pH, precipitating the iron, and leaving the tuballoy in solution.

The following document is meant to inform the reader on the makings of a cement base for the hot filament mass spectrometer source as part of a publication in the review of scientific instruments, "Laboratory and Shop Notes".

This report follows a test made to determine the effect of temperature on the distribution of nitric acid between "carbitol" and gunk, extracting a number of samples of aqueous copper nitrate with samples of "carbitol" of various acidities. The data obtained is covered in Table 1.

Report discussing the fractionation study of tri-n-butyl orthophosphate as the organic phase using a solution of trivalent rare earth chlorides or nitrates as the aqueous phase.

The effect of air, nitrogen, helium, argon, and a mixture of twenty volume percent of hydrogen in argon on the wetting of a stainless steel (Type 446), a two percent chromium-one half percent molybdenum type steel, and a plain carbon type steel by liquid bismuth was investigated

A digital-to-analog converter is described which is a part of a system that converts punched-tape digital data to analog data in a series of points drawn by an x-y plotter. The converter is designed to plot accurately tapes that contain information other than coded numerical coordinates. Operation of the converter is also described along with format requirements and power supplies. (J.R.D.)

Figures 1 and 2 summarize total decay energies for the four radioactive series. The alpha-decay energy obtained by measuring the energy of the alpha particle leading to the ground state includes the energy of the recoil nucleus. The curve shown in figure 3 defines in broad outline the conditions and regions of alpha instability. A great deal more is to be learned from a more detailed examination of the region where alpha radioactivity is prominent. Of great value to the experimentalist is that he is able to predict alpha energies, and the agreement between predicted and measured values often serves as a criterion for isotopic assignment. A number of systems for correlating alpha decay energies have been employed, and that perhaps most widely used is illustrated in figure 4. Here the isotopes of each element on a mass number vs. energy plot are joined, resulting in a family of curves which over a wide region comprise a series of nearly parallel lines.

Plutonium sheet of uniform thickness and good surface can be made by the extrusion of a tube which is then split and flattened. This report describes the equipment and the operating conditions for making sheet 0.005 to 0.055 in. thick with areas up to 24 in. square.

The following temperature measurement tabulation consists of two parts. Part I lists all HRT thermocouples, their location, the junction box thru which the leads pass, and their termination, if on an instrument. Part II lists all temperature read out instruments and their location. A total of 577 thermocouples are listed in this tabulation. The roughly 77,000 ft of wire used in connecting them up cost $6,799. Temperatures are read on 24 instruments. Cost of these was approximately $15,688. Accessories such as patch panels, conduit, disconnects, etc., used in installing the thermocouples cost about $8,069. Total cost for material and instruments for temperature measure comes to approximately $30,556.

The horizontal and vertical power distribution for a 5 x 7 fuel element loading of the TSR is presented. (auth)

Few data exist for the thermal conductivity and viscosity of gases at very high pressure. The possibility of using gases for heat transfer media at pressures up to 100 atmospheres and above raised the problem of estimating variations in the conductivity and viscosity at high pressure. Generalized plots are presented which are based on the work of Enskog, Eucken, and Hirschfelder et al. Some pertinent data from Hirschfelder et al and from Hilsenrath et al are presented.

The method is based on caustic precipitation and centrifugation (which removes the Cs and small amounts of Sr, rare earths, Zr, Nb, and Ru). These are removed in the supernatant and run through a cation exchange column. This separates Zr-NB and Ru. The effluent is precipitated and the Zr-Nb is stored in an asphalt pit. The Ru then may be recovered from the precipitate. The precipitate from the original centrifugation is calcined, pressed and transported to a deep well.

THOROBRED is an IBM-704 code for the calculation of nuclear and economic characteristics of two-region homogeneous reactors operating on a U-Th fuel cycle in the steady state. The major input variables are reactor dimensions, power level, thorium concentration, chemical and purification systems cycle times, corrosion rates, fraction of Pa loss, and nuclear and economic data. The output includes equilibrium isotope concentrations, neutron balance, and a breakdown of fuel cost. Running times are normally less than one minute per case.