Technical report. Numerous application of various column adsorption techniques to inorganic analytical chemistry have appear in the literature. The comparatively recent introduction of ion exchange resins has resulted in the development of efficient, simple, and rapid column adsorption methods. the principal service of column adsorption methods to analytical chemistry is that of providing a relatively simple means of separating an element in a sufficiently pure state so that a direct precipitation, ignition, and weighting, for example, will suffice to complete the quantitative analysis. Systems involving uranyl nitrate will naturally be emphasized in this report but information will be included concerning the separation of the individual members of a series from one another, such as in the alkaline earths and the rare earths.

Technical report: Measurements have been made on the equilibrium between Cu, Cu2+, U4+, and UO22+ in H2SO4 in an attempt to establish the value of the U4+ - UO22+ couple potential. The value of the formal potential for the U3+ - U4+ couple in 1N HCl at 0 degrees C was determined to be + 0.65 v.

Abstract. A satisfactory method has been found for dissolving thorium metal and thorium oxide in heat-treated 25-12 stainless steel vessels without excessive corrosion of the vessels. The dissolution medium consists of strong HNO3 containing a small amount of fluoride or fluo-silicate. the fluoride required has no harmful effects on a subsequent solvent-extraction step for a separation of uranium isotopes from the dissolved thorium.

Technical report that attempts to bring together the various chemical procedures which proved most useful in studying the results of cyclotron bombardment or small scale neutron bombardments of heavy element targets. The report is limited to the elements of the "actinide", or second rare earth series, starting with thorium and including the newly discovered elements of atomic number 95 and 96. Every attempt is made to include all details necessary so this report can serve as a practical laboratory guide. The report covers separation problems, time factors, and dealing with dangerously radioactive targets.

Abstract. the Laplacian of a beryllium metal lattice with 3.3 kg of uranium metal per cell and a volume ratio of 17.2 was measured in the removable region of the CP-2 machine. the sandwich effect with different moderators made interpretation of the observations very uncertain. The best result found was Be = 407 x 10(-6) cm(-2).

Technical report with short reports from the (A) Crystal Structure Section ; (B) Mass Spectroscopy Section ; and (C) Metallurgy Section.

The following report discusses the deposition of radioactive elements during a nuclear fission in the skeleton. Studies are concerned with chronic effects of toxic radiation developing within the bone marrow and decontaminating the cells.

Abstract: "The first shielded isotope, 34th Br-82 has been isolated in fission. Its fission yield is about 3 x 10-(-5)%. This is a direct measurement of the yield of a primary fission product and gives direct information as to the distribution of nuclear charge among primary fission fragments of given mass numbers as discussed by Glendenin and Coryell."

Abstract: "Preliminary studies are reported on the use of the ion exchange resins for the adsorptions of purines, uracil, nucleotides, kynurenic acid, and coproporphyrin. Adenine and guanine are adsorbed on IR-100 resin from neutral solution and eluted by HCl. Kynurenic acid and coproporphyrin are adsorbed from neutral solution on IR-4 resin and eluted by HCl. Coproporphyrin is strongly adsorbed on IR-100 resin from either acid, alkaline, or neutral solution. Kynurenic acid is poorly adsorbed on IR-100 resin from neutral aqueous solution. The preliminary application of these procedures to the spectro-photometric study of urine is described."

The following report records the study of albino rats subjected to beta rays and analyzes the skin reactions and metabolic patterns.

From abstract: "Experiments covering the coprecipitation of Thorium and Uranium peroxides are described on synthetic and actual 1300 cycle machine wash effluents."

From introduction: This report is concerned primarily with the coprecipitation phenomenon and its application to plant problems.

Abstract: "A method of recovering the tuballoy from the trap washes of the high temperature salvage chlorinator is described."

Abstract: "Using xylene as the densimetric solvent, the crystal densities have been determined by the pyknometric method for the following chlorides, UCl3, UCl4, UCl6(UCl4), UCl6 and U02Cl2."

Abstract: "The results obtained from the tests conducted for the purpose of determining the corrosivity of a 30 percent-solution of uranyl fluoride to various metals indicate that stainless steels (type 302, 304, 321 and 316) have very good resistance; while monel, nickel and aluminum, respectively, exhibit diminishing resistance. Stainless steel, type 316, was the most resistant of the specimen tested."

Abstract: "Tests have been developed for both the qualitative detection and quantitative determination of fluorine in chlorine. The qualitative test is made by passing the gas through manganous chloride. If the pink solid tubes brown there is greater than 0.5 percent of fluorine in the gas. The quantitative test is a modification of the Steiger and Marvin Test with oxidized titanium solution."

Abstract: "The definitions of the fundamental measures of calutron operation including enhancement, current ratio, and process efficiency are set forth with derivations of the relationships between them. An analysis of the plant process is carried out for both the tanks limited and the charge limited case. Equations are derived for plant X output and plant X utilization efficiency. Effective production is defined and the value of increment to a mass of product material in terms of effective production is determined. An equation giving the X concentration below which product material should be reprocessed is derived."

Abstract: "A survey report of the known production and experimental methods for the preparation of anhydrous tuballoy tetrachloride with references of each method."

From introduction: "This meeting was called by Mr. S. H. Smiley in order to review progress made on the corrosion problem since the last meeting on September 5th, and to devise a definite program on the specific problem of the corrosion of the coolant coolers."

Abstract: This discussion concerns the operation, construction, and servicing of an alpha rate meter of medium sensitivity (30,000 alpha particles full scale per minute) and good stability. The instrument is equipped with an oscillator which increases both in frequency and loudness as the alpha activity is increased. The oscillator circuit includes an anticipator which causes a change in frequency depending directly upon the rate of change of alpha activity. Maximum sensitivity is approximately 100 millivolts full scale. Grid current varies from 1 to 5 x 10^-14 amperes. A general discussion of time constants and accuracy is included. Tables of stopping power, ionization and alpha activity are appended.

Abstract: "The half-life of polonium has been measured by a calorimetric method using samples several thousand times larger than have been previously available. The value is found to be 138.3 +/- 0.1% days."

This report follows a test made to determine the effect of temperature on the distribution of nitric acid between "carbitol" and gunk, extracting a number of samples of aqueous copper nitrate with samples of "carbitol" of various acidities. The data obtained is covered in Table 1.

Introduction: "The product of a special run made in XAX was submitted to the Assay Department for a determination of the residual content of the 235 isotope. The charge material on this run was impoverished, with a ratio of approximately 1:2,000. The sample was submitted in the form of purified T3O8."

From introduction: Complete removal of fluorine iron waste gases also containing uranium hexaflouride was the object of researches described in this chapter.