Abstract: "The sensitivity to fast neutrons of a CP Meter ionization chamber of the type used for health physics beta and gamma survey measurements has been investigated."

The following report describes polarographic methods that determine saturated aliphatic carbonyl compounds.

Introduction: "The adoption of aluminum nitrate as salting agent in the Redox process made it imperative that a method be available for determining plutonium in the presence of aluminum. However, large amounts of aluminum have been found to interfere with the determination of plutonium by the lanthanum fluoride procedure. Previous attempts to increase the accuracy of the lanthanum fluoride method, by precipitating LaF3 from 4 M HF (rather than 2 M), have been successful only when the initial plutonium level was high."

The following report describes methods used to determine tributylphosphate in a deodorized shell base. An infrared absorption method is developed to emphasize toward determination of TBP in RCW streams, the organic waste streams.

The following report summarizes an investigation made to determine the extent to which zirconium and zirconium alloys exhibit delayed failure as caused by a combination of absorbed hydrogen and applied stress during the period September 15, 1961, to September 14, 1962.

The following report is the first semi-annual report of a literature survey designed to investigate the uses and technology of radioisotopes in the countries of the world from 1955 to the present. This survey includes two phases: 1) involves the direct comparison of radioisotopic work in all fields in various countries as demonstrated at international conferences. 2) involves a more detailed examination and evaluation of the individual fields of interest selected previously (Phase II is also expected to comprise the bulk of the remainder of this investigation).

This document is the third in a series of progress report that records investigations of graphite bodies. Along with the report, two appendices are given to describe the different graphite bodies: "Synthetic Binders for Carbon and Graphite" and "High Temperature Physical Properties of Molded Graphites".

Quarterly report describing progress on a project to develop and evaluate high-temperature tungsten alloys. This report discusses experimentation with fabrication to improve thermal stability of tested combinations by further alloying.

Abstract: "Decontamination factors of the order of 10-4 were obtained for Beta and Gamma emitters present as fission products when uranium was precipitated from 50 mC activity level solutions as uranyl oxalate under normal uranium yield conditions for three cycles (~60%). Factors of the order of 10-3 were obtained by the use of this reaction with similar solutions under relatively high uranium yield conditions for three cycles (~90%). The uranium peroxide precipitation reaction proved to be of no value on such solutions, yielding decontamination factors of only 17.1 Beta emitters and 1.2 for Gamma emitters for three cycles."

The following memorandum outlines the procedures used on the neutralization of HNO3 in redox ICU and IAW streams, and the factors influencing their choice. The procedures involve a) hexone removal by evaporation in the presence of a retardant, b) destruction of the retardant, c) nitric acid elimination by boiling with aluminum and d) concentration of the remaining solution by evaporation.

Abstract: "A completely Lagrangian scheme for differencing hydrodynamical equations in two dimensions is described. The method conserves mass exactly. The advantages of Lagrangian over Eulerian schemes are briefly mentioned. An appendix gives the generalization to three dimensions."

The following document provides measurements, equations and figures describing the minimum power coil geometries for D.C. magnetic mirrors.

Abstract: "A scheme is discussed in which D+ ions would be accelerated to about 100 kev in a conventional accelerator, then be sent through a gas target frmo which about half the ions would emerge neutral with very little scattering or energy loss; the neutral beam would then cross into a magnetic field and part of the atoms would be ionized and trapped by colliding with the already trapped ions. The smallest mirror machine with a central field of 30-40 kilogauss, 2;1 mirror ratio and β = 01 to 0.5 that would trap most of the neutral beam in the steady state, would be about a meter in diameter and require the order of hundreds of amperes of D+ ions into the neutralizer. The smallest stellerator with a field of 30 kilogauss and β = 0.1 that would trap most of the neutral beam would be about a meter long and require about 10 amperes of D+ ions. A preliminary mirror machine experiment that might be done using the 1/2-ampere, 100-kev D+ beam from the UCRL spare MTA injector is discussed. A method of starting these machine is discussed."

From introduction: "The purpose of this report is to summarize some of the observations on the dispersion and rate of disengaging of liquid-liquid systems and suggest some possible lines of future work."

This report follows critical-assembly studies made to provide engineering and physics data to aid in developing the Gas Cooled Reactor Experiments.

The following report is a bibliography containing reports, books and journals on the production of high temperatures (2000-3000 F). The literature provided only covers to the end of 1957.

Abstract. A review of all work on uranium hydride published in the CC, CT, CN and CE reports to January 1, 1944, is presented. Some additional information not yet published has been included, so this report includes all data known from the above sources and at Ames to the above date. This report supersedes all previous report on uranium hydride coming out of the Ames laboratory.

Introduction. the colorimetric determination of iron based on the formation of the colored ferrous-1,10-phenanthroline complex has been used successfully by a number of investigators. In this technical report, its adaptation to the routine determination of iron in cerium, thorium, and beryllium metals and their compounds is described.

Technical report describing the purification and separation by distillation of UO2F2 from D2O. In the experiment which is discussed 2,129.6 lbs of UO2F2 were dissolved in 6,605 lbs of D2O. The average isotopic purity of the D2O decreased during the distillation from 99.77% to 99.73%. The dissolved impurities were less than those present originally in the heavy water.

Abstract. Fourteen commercial enamel frits from five different manufacturers were tested to determine their abilities to protect Nb-1% Zr during the forging cycle in the temperature range of 1800 to 2300 deg F. One frit was found to afford good coverage and protection at 2200 deg F at times up to 5 hours of exposure. Adherence was excellent during upset forging of a coated Nb--1% Zr sample heated 45 minutes at 2200 deg F. Another frit afforded good protection and coverage at 1700 deg F. (auth)

The average energies of neutrons emitted from a graphite column at 22 degrees C were compared by measurement of the cross section of boron for neutrons which are stopped by cadmium. At a distance from the neutron source great enough to insure that the neutrons were in thermal equilibrium the average energies of the emerging neutrons were found to be proportional to the temperature within the limits of the experimental error. A measurement made with boron absorbers which had been thus standardized in the graphite column indicated neutrons emerging from the chain reacting pile to have an average temperature approximate 60 +- 50 degrees above that of thermal neutrons emerging from the graphite column at 22 degrees C. Such a measurement made inside the chain reacting pile indicated the average temperature of neutrons therein to be about 65 degrees +- 15 degrees above the average temperature of neutrons in the graphite column.

Abstract. Temperatures are measured at two points in an internally heated jacketed slug which is cooled by water flowing in an off-center annulus around the slug. The variations of these temperatures with water velocity, water temperature, power, and the amount the annulus is off center are measured. The temperature near the slug surface which approaches and comes in contact with the water jacket does not increase as much as anticipated. The temperature near the slug surface on the side which is moved away from the water jacket increases nearly as much as on the side approaching the slug. An explanation for this unexpected increase of temperature as on side moving away from the jacket is given.

From abstract: "Experiments covering the coprecipitation of Thorium and Uranium peroxides are described on synthetic and actual 1300 cycle machine wash effluents."

The following report discusses the results of a survey that was initiated to ascertain the availability of uranium hydride in tonnage quantities.