The Spectroscopy Research Laboratory is concerned with research and development in the fields of nuclear magnetic resonance, microwaves, infrared and optical spectroscopy, spectrochemistry, and x rays. Research is directed toward fruitful methods of isotope analysis; new element and compound analytical methods having application to immediate Laboratory or long-range commission needs; and fundamental research on isotopes, elements, and compounds. The work is reported on a project basis to give a more complete picture of the purpose, activity, and status of each program. More detailed information on reported or inactive projects may be obtained from the previous semiannual report.

Nuclear physics research with 22-Mev protons in the 86-in. cyclotron included angular-distribution measurements of neutrons from (p,n) reactions in nine target elements; measurement of the angular distribution of fission fragments from proton-induced fission of U233, U225, U228, Th230, and Th232; measurement of alpha-particle angular distributions from (p,α) reactions a study of the neutron-deficient isotopes of terbium and completion of an extensive program of the measurement of activation cross sections. Two more targets for cyclotron production of isotopes were developed, and the production yields for 14 radioisotopes are summarized. A new record for continuous beam power on a production target, 36 kw for 5 hr, was achieved. The design of a beam-deflector system for the 86-in. cyclotron has been completed, and several of the components have been fabricated ; a shutdown for installation is scheduled for October 8. The deflected N+++ beam of the 63-in. cyclotron was used in a study of the gain and loss of electrons by nitrogen lens passing through thin foils, and the equilibrium charge distribution of lens as a function of energy was thus obtained. The excitation functions were measured for nitrogen-induced reactions on both nitrogen and oxygen. Assembly restrictions of the prepared 114-in. heavy-particle cyclotron …

Experience in handling and purifying rubidium metal, prior to high-temperature corrosion testing, has been obtained. Some of the physical and chemical properties of this metal are listed. Distillation and filtration experiences are described, and the analysis of samples following such purification procedures are given. Stripping procedures following corrosion testing are discussed briefly. Results of preliminary corrosion experiments indicate that Inconel in a satisfactory container material for boiling rubidium at temperatures up to 1520°F.