This report describes a production scale procedure for purifying and concentrating the plutonium contained in the stripping solution from a tributyl phosphate extraction process. Conclusions from exploratory laboratory tests on the variables effecting the efficiency are included.

The experiments described in this report were designed to explore the feasibility of precipitating plutonium from 35 percent TBP in Gulf BT using peroxide, fluoride, sulfide, sulfite, sulfate, cocalate, hydroxide, iodate and phosphate ions from anhydrous, dilute and concentrated aqueous sources.

From summary: The University of Colorado, under contract with the Los Alamos Scientific Laboratory (LASL), is currently performing an evaluation of geochemical relationships of water and sediments and seasonal variations to uranium for the South Platte drainage of northeastern Colorado. As a preliminary part of this study, samples were collected from 125 sites near Sterling and Fort Morgan, Colorado, during the period from December 20, 1976, to January 15, 1977. During this period the weather in the area was clear to partly cloudy, with daytime temperatures ranging from -12 to 12 C. Only a trace of precipitation, in the form of very light snow flurries, occurred during the sampling period. The sample site locations and numbers (the first two digits have been omitted) are shown on Plate I.

From 1995 sites in the San Juan Mountains area, 1706 water and 1982 sediment samples were collected during June-July 1976 and analyzed for uranium. The area includes the southern third of the Colorado mineral belt which has yielded rich ores of gold, silver, copper, lead, zinc, and molybdenum. The broadly domed mountains are capped by 2500 m of Tertiary volcanics, deeply eroded to expose a Precambrian crystalline core. Adjacent plateaus underlain by Mesozoic sedimentary rocks were included in the reconnaissance. Average value of uranium in water samples from mountains was less than 0.5 parts per billion, from plateaus was 1-2 parts per billion, from Mancos shale areas exceeded 2 parts per billion. Anomalous sediment samples, 40 ppm uranium, came from near Storm King Mountain and upper Vallecito Creek. Other anomalous areas, including the Lake City mining district, were well defined by 4-30 parts per million uranium in sediment and 3-30 parts per billion uranium in water. Anomalous areas not previously reported indicate favorable areas for future exploration.

Plutonium sheet of uniform thickness and good surface can be made by the extrusion of a tube which is then split and flattened. This report describes the equipment and the operating conditions for making sheet 0.005 to 0.055 in. thick with areas up to 24 in. square.

From introduction: This report describes work done in the Raton, New Mexico, National Topographic Map Series (NTMS) quadrangle (1:250 000 scale) by the Los Alamos Scientific Laboratory (LASL) as part of the nationwide Hydrogeochemical and Stream Sediment Reconnaissance (HSSR).

From introduction: This report presents uranium and other elemental data resulting from the Hydrogeochemical and Stream Sediment Reconnaissance (HSSR) of the Shiprock National Topographic Map Series (NTMS) quadrangle, New Mexico/Arizona, by the Los Alamos Scientific Laboratory (LASL).

A report discussing HSSR results for the Rock Springs NTMS Quadrangle.

A report describing the results of a detailed hydrogeochemical survey directed by the Los Alamos Scientific Laboratory of well waters in parts of the Saint Johns and Socorro Quadrangles.

Report documenting the results of chemical analysis for 1583 water and 503 sediment samples in the Dalhart quadrangle of northeastern New Mexico, northwestern Texas, and western Oklahoma. It includes an overview of the area, methods, data analysis, and evaluation.

During the spring and summer of 1976, 2144 water and water transported sediment samples were collected from 1685 locations spread over an approximate 21 000 km area of the northern end of the Powder River Basin in northeast Wyoming.

From introduction: This report describes work done in the Trinidad, Colorado, National Topographic Map Series (NTMS) quadrangle (US Geological Survey, 1955) by the Los Alamos Scientific Laboratory (LASL) as part of the nationwide Hydrogeochemical and Stream Sediment Reconnaissance (HSSR).

A uranium metal critical assembly consisted of a 15 inch diameter core with an average U235 content of 16-1/4%, surrounded by a 3 inch thick natural uranium reflector. The critical mass was 692 kg of core material.

Reflected cylindrical exponential columns of bare and natural uranium were constructed of stacked plates of oralloy (93.4%) and tuballoy. Average concentrations of U235 ranging from 0,72% to 9.18% were investigated. Flux distributions, buckling values, and spectral indices were obtained. The indicated U235 concentration for infinite critical mass is about 5.5%.

From introduction: This report describes work done in the Sterling, Colorado, National Topographic Map Series (NTMS) quadrangle (1:250 000 scale) by the Los Alamos Scientific Laboratory (LASL) as part of the nationwide Hydrogeochemical and Stream Sediment Reconnaissance (HSSR).

From summary: This data release presents analytical results obtained for a pilot study being done in portions of the Sterling and Greeley, Colorado, National Topographic Map Series (NTMS) quadrangles (Fig. 1) by the University of Colorado under contract to the Los Alamos Scientific Laboratory (LASL) as part of the nationwide Hydrogeochemical and Stream Sediment Reconnaissance (HSSR).

As part of the LASL portion of the US EROA NURE program, water samples from 534 locations and sediment samples from 2936 locations were taken over a 7770 square kilometers area of the Estancia Valley in 1975 and analyzed for uranium.

This is the second part of a report of a uranium hydrogeochemical and stream sediment pilot survey of areas of New Mexico.

Critical conditions were obtained for a series of uranium-graphite fueled assemblies in the C/Oy range 150 to 500 with thick graphite reflectors and Be or D2O islands. Perturbations were studied in order to find the effect on reactivity of geometrical changes and engineering features. Information from these studies was used to develop a mock-up of an optimum reactor geometry for the first rocket reactor test device, Kiwi-A. Studies on a zero power mock-up (Zepo-A) helped establish its design details. A cold critical check was made of the Kiwi-A reactor.

Data on critical configurations of fissionable metals are summarized in a form emphasizing the influence of conditions commonly of concern in nuclear safety questions.

Bibliography of unclassified work published by the Los Alamos Scientific Laboratory during 1972-1976. This volume contains listings of publications, organized by topic, with title, author, and citation information.

Bibliography of unclassified work published by the Los Alamos Scientific Laboratory during 1972-1976. This volume contains indexes to authors, publication numbers, and keywords.

Supplementary data containing a keyword-in-context index to accompany a report on the Los Alamos Scientific Laboratory research publications.

A report discussing HSSR results for the Leadville NTMS Quadrangle