Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery (open access)

Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery

The following report discusses the presentation of preliminary density and viscosity data which may explain whether higher viscosities of the Deo Base-TBP systems, and a change in density differences between the two phases will lead to unsatisfactory column operation.
Date: November 29, 1949
Creator: Burger, L. L. & Slansky, C. M.
System: The UNT Digital Library
Determination of Organic Acids in Process Solutions (open access)

Determination of Organic Acids in Process Solutions

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
System: The UNT Digital Library
Heating in the Graphite Due to a Cadmium Control Rod (open access)

Heating in the Graphite Due to a Cadmium Control Rod

From introduction: "This paper employs a multigroup method similar to that of J. S. Story, AERE-TR-177 to calculate, for cylindrical geometry, that heat energy source density in graphite due to absorption and Compton scattering of those gammas produced by neutron capture in a water filled cadmium control rod."
Date: September 29, 1951
Creator: Newkirk, W. H.
System: The UNT Digital Library
Darex Pilot Plant Studies (open access)

Darex Pilot Plant Studies

The Atomic Energy Commission has assigned the Hanford Atomic Products Operation the responsibility of providing the technology and facilities for the interim reprocessing of slightly enriched uranium fuels discharged from power and propulsion reactors. The fuel from the various reactors vary greatly in physical dimensions and in the composition of the core and cladding. For the purposes of chemical reprocessing, the fuels may be divided into the three main categories of aluminum, Zircaloy or stainless steel clad elements. The fuels may be sub-divided by the nature of the core material; e.g. metallic uranium, uranium dioxide, uranium-molybdenum alloys uranium-aluminum alloys, etc.
Date: October 29, 1959
Creator: Shefcik, J. J.
System: The UNT Digital Library
Effect of the PRTR High Pressure Loop on Plutonium Recycle Program Objectives (open access)

Effect of the PRTR High Pressure Loop on Plutonium Recycle Program Objectives

For purposes of an earlier consideration of the effects of in-reactor test loops on PRTR operation and program, the design of the high pressure, H20 cooled fuel test loop was assumed to be similar to that for the high pressure, gas cooled loop. Detailed design criteria for the H20 loop have recently been completed so that this assumption is no longer necessary. Therefore, to insure that the effects of all proposed in-reactor loops are fully evaluated with respect to Plutonium Recycle Program objectives, the present study has been carried out. Much of the qualitive discussion in the original analysis is still considered valid. Thus, rather than repeating the entire analysis as it pertains to the H20 loop, only those departures resulting from differences between the assumed design and the scope design are presented.
Date: October 29, 1959
Creator: Peterson, R. E.
System: The UNT Digital Library
Stability of Chromel-Alumel Thermocouples in Carbon Dioxide at 1000°C (open access)

Stability of Chromel-Alumel Thermocouples in Carbon Dioxide at 1000°C

Tests on twenty identically prepared 26 gauge Chromel-Alumel thermocouples have been completed. It appears that wires of this material without protection are unsatisfactory mechanically and thermoelectrically for service in atmospheres of CO₂ at 1000°C.
Date: November 29, 1955
Creator: Burton, H. H.
System: The UNT Digital Library
All In-Well Permeability Testing Packer (open access)

All In-Well Permeability Testing Packer

Disposal of liquid radioactive wastes to ground requires knowledge of the area ground-water hydrology. Information is desired on direction and velocity of ground-water flow. Direction of flow can be determined from maps showing contours on the water table surface, such contours being derived from well water elevations. Ground-water velocity is more difficult to ascertain.
Date: September 29, 1959
Creator: Raymond, J. R.
System: The UNT Digital Library
A Doorway Monitor (open access)

A Doorway Monitor

The purpose of this work was to produce a reliable, inexpensive instrument for the detection of hard beta contamination on the clothing of personnel. Also, the monitoring was required to be accomplished without interrupting the normal activities of the employees.
Date: April 29, 1955
Creator: Campbell, D. A. & Test, L. D.
System: The UNT Digital Library
Chemistry-Separation Processes for Plutonium and Uranium (open access)

Chemistry-Separation Processes for Plutonium and Uranium

Attached hereto are copies 1 through 4 of a classified secret report titled "Purex - A Hanford Separations Plant." We are also sending under separate cover a classified confidential report No. HW-36496 titled "Photographs of Purex - A Hanford Separations Plant," which is a counterpart of the above report. These documents are submitted for publication and should be incorporated as a single article.
Date: April 29, 1955
Creator: Mundt, W. J.
System: The UNT Digital Library
Evaluation of Glass-Clad Bayonet Heaters (open access)

Evaluation of Glass-Clad Bayonet Heaters

This report describes the results of evaluation tests made on several glass-coated bayonet heaters supplied to Separations Equipment Development by the Pfaudler Company. The glass-coated heaters were found to be resistant to thermal shock, mild mechanical shock, and chemical attack by boiling 60% nitric acid.
Date: July 29, 1955
Creator: Krieg, J. T. & Amos, L. C.
System: The UNT Digital Library
Particle Distribution From a Unit Source - Part A (open access)

Particle Distribution From a Unit Source - Part A

Thus we see that the derivation of elementary age theory is based on replacing the probability of collision governed by the Milne kernel by a Gaussian probability having the same zeroth and second moments. It is apparent that the age theory distribution will fail close to the source and at many free paths from the source.
Date: April 29, 1955
Creator: Anthony, G. W.
System: The UNT Digital Library
Resonance Capture of Neutrons in Metal and Oxide Cylinders (open access)

Resonance Capture of Neutrons in Metal and Oxide Cylinders

Reactivity measurements conducted in the Hanford Test Pile are interpreted to yield resonance integrals for uranium, uranium oxide, thorium and thorium oxide. The experiments were made using cadmium filters and are discussed in terms of the multiplication factor of the Hanford Test Pile.
Date: June 29, 1956
Creator: Davis, M. V.
System: The UNT Digital Library
Effect of the PRTR Fuel Elemental Rupture Test Facility on Plutonium Recycle Program Objectives. (open access)

Effect of the PRTR Fuel Elemental Rupture Test Facility on Plutonium Recycle Program Objectives.

To insure a full evaluation of the effects of in-reactor loops with respect to all phases of the Plutonium Recycle Program, a separate study of each loop has been undertaken. An initial study was carried out which analyzed the effects of in-reactor loops using the design criteria for the gas loop as a basis. As soon as the design criteria for the H2O high pressure loop became available, a more detailed evaluation was completed for that loop. Recent completion of the scope description of the PRTR fuel element rupture test loop now permits an individual evaluation of this loop.
Date: January 29, 1960
Creator: Peterson, R. E.
System: The UNT Digital Library
Project CGC-830 Plant Modifications for Reprocessing Non-Production Reactor Fuels (open access)

Project CGC-830 Plant Modifications for Reprocessing Non-Production Reactor Fuels

Facilities are to be designed for installation at Hanford for the reprocessing of irradiated, low enrichment fuels from non-production reactors, see Reference 1 and 2. The initial design of the processing facilities is to be based on processing the fuels discharged from the Dresden, Yankee, Piqua, Pathfinder and Shippingport (blanket elements only) reactors. Properties of the fuels and cladding make it impossible to completely process them in existing equipment, although the separation and decontamination can be performed in existing facilities once the fueks have been placed in solution form.
Date: July 29, 1960
Creator: Bierman, S. R.; Graf, W. A.; Kass, M.; Kligfield, G.; McKee, R.W.; Patridge, L. F. et al.
System: The UNT Digital Library