Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery (open access)

Density and Viscosity of Solutions in the Tributyl Phosphate Process for Uranium Recovery

The following report discusses the presentation of preliminary density and viscosity data which may explain whether higher viscosities of the Deo Base-TBP systems, and a change in density differences between the two phases will lead to unsatisfactory column operation.
Date: November 29, 1949
Creator: Burger, L. L. & Slansky, C. M.
System: The UNT Digital Library
Determination of Organic Acids in Process Solutions (open access)

Determination of Organic Acids in Process Solutions

Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated potentiometrically with standard potassium hydroxide solution. Since nitric acid and organic acids are present, two end points are observed. The potassium hydroxide added between these end points is equivalent to the organic acids. In the titration, CO2 from the atmosphere or in the potassium hydroxide is a source of error. The former was avoided and correction was made for the latter."
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
System: The UNT Digital Library
Alpha Particle Detection and the A. C. Operated Detector "A" (Howler) (open access)

Alpha Particle Detection and the A. C. Operated Detector "A" (Howler)

Abstract: This discussion concerns the operation, construction, and servicing of an alpha rate meter of medium sensitivity (30,000 alpha particles full scale per minute) and good stability. The instrument is equipped with an oscillator which increases both in frequency and loudness as the alpha activity is increased. The oscillator circuit includes an anticipator which causes a change in frequency depending directly upon the rate of change of alpha activity. Maximum sensitivity is approximately 100 millivolts full scale. Grid current varies from 1 to 5 x 10^-14 amperes. A general discussion of time constants and accuracy is included. Tables of stopping power, ionization and alpha activity are appended.
Date: January 29, 1946
Creator: Neil, Hugh G.
System: The UNT Digital Library
The Ammonia Reduction and its Application to the Preparation of Green Salt (open access)

The Ammonia Reduction and its Application to the Preparation of Green Salt

From introduction: The present report is a summary of the experimental work on a laboratory scale to date involving the ammonia reduction and the one step TF4 processes.
Date: December 29, 1945
Creator: Clinton Engineer Works
System: The UNT Digital Library
Effects of Receiver Slots on Quantity and Quality of Product and Recycle (open access)

Effects of Receiver Slots on Quantity and Quality of Product and Recycle

Abstract: "Variations in receiver slot design produce changes in quantity and quality of product and recycle, not only instantaneously, but also as a function of time in approaching equilibrium. The case of fixed feed concentration and fixed inventory of Uranium is described here for standard and Dip-Lip wider R slot receivers. The effects of the two types of receivers on recycle and product X and W concentrations, X production rate, plant X utilization efficiency, integrated X production and effective mass output are shown graphically."
Date: May 29, 1947
Creator: Harmatz, Benjamin
System: The UNT Digital Library
Summary of an investigation of vanadium and uranium occurrence in Huerfano Park district, Raton Basin area, Huerfano and Costilla counties, Colorado (open access)

Summary of an investigation of vanadium and uranium occurrence in Huerfano Park district, Raton Basin area, Huerfano and Costilla counties, Colorado

A report on the SOM-vanadium occurrences of the Huerfano Park District.
Date: September 29, 1943
Creator: Emerson, John F.
System: The UNT Digital Library
Technical Report for the Months of April, May and June, 1944; Chemical Research - General (open access)

Technical Report for the Months of April, May and June, 1944; Chemical Research - General

Technical report. Quite pure anhydrous ThCl4 in small quantity (8-10 g charge) has been prepared by the action of a mixture of Cl2 and CCl4 vapor on ThO2 at 675 degrees to 725 degrees C.
Date: July 29, 1944
Creator: Kraus, Charles A. (Charles August), 1875-1967
System: The UNT Digital Library
A Comparative Analysis of the Liquid Metal Heat Transfer Systems for WMA (open access)

A Comparative Analysis of the Liquid Metal Heat Transfer Systems for WMA

Introduction. As stated in Report KAPL 116, one of the objectives of the KAPL reactor is "to provide a prototype demonstration of the practical general of electrical power from Nuclear energy using molten sodium as the primary coolant. The reactor will generate steam at a temperature of 550 degrees F and 465 psia, including 90 degree superheat potentially capable of an efficiency of twenty-eight per cent in electrical output." The work reported here is intended to increase the scope and supply an independent check on the heat transfer system analysis that has previously been done. The purpose of these analyses is to investigate the effects on load rating and top reactor temperature.
Date: April 29, 1949
Creator: Selby, J. D.
System: The UNT Digital Library
Interaction of Be with Fission Neutrons (open access)

Interaction of Be with Fission Neutrons

To determine whether or not the (n,2n) reaction in Be would produce a net increase in fission neutrons in a power plant, the distribution of In resonance neutrons slowed down from fission energies in a graphite block was measured with and without a 2" of Be in front of a U3O8 slab undergoing fission. The thermal neutrons producing the fissions were obtained by slowing down neutrons from a cyclotron source. The observed distribution without Be was well represented by a Gaussian source range 36 cm. (corresponding to an initial fission energy of 3 MeV) and a similar sink of range 7.8 cm. The total In resonance intensity with Be was 5% less than without Be. On the assumption that the effect of the Be is entirely due to its different mean free path and moderating power, the In distribution with Be was calculated. Since the m.f.p. as a function of energy is not known for Be, two separate calculations were made using the highest (2.9 cm.) and the lowest (1.80 cm.) possible values for the effective Be m.f.p. Both calculated curves were found to be higher than the observed Be distribution, indicating that at least 10% of the fission neutrons …
Date: April 29, 1942
Creator: Borst, L.; Allison, S. K.; Wheeler, John Archibald, 1911-2008 & Weinberg, Alvin Martin, 1915-2006
System: The UNT Digital Library