Urine Analysis for Tritium Oxide (open access)

Urine Analysis for Tritium Oxide

This report analyzes a procedure based on the production of acetylene from the active water, with subsequent measurement of the ionization caused by the tritium beta particle. This eliminates the troublesome absorption on the chamber walls when hydrogen is used, and provides a rapid method for the preparation of the urine samples.
Date: July 27, 1949
Creator: Healy, J. W.
System: The UNT Digital Library
The Rapid Determination of Nitric Acid and Thorium in Thorium Nitrate Solutions (open access)

The Rapid Determination of Nitric Acid and Thorium in Thorium Nitrate Solutions

Abstract. The physico-chemical methods of determining nitric acid and thorium nitrate in solutions containing these two materials were investigated. Conductimetric titration with sodium hydroxide can be used to determine nitric acid accurately. the titration of thorium nitrate requires a separate standardization of the base however, since a basic salt is precipitated rather the normal hydroxide. The titration of thorium is reproductible however, so and empirical standardization can be used. The measurement of the specific gravity and refractivity of the solutions provides a method of determining the concentrations in terms of these two variable. Equations for the concentrations in terms of specific gravity and refractively are given, both in pure solutions and in those saturated with methyl isobutyl ketone.
Date: November 27, 1945
Creator: Newton, A. S.; Powell, J. (James), 1932- & Figard, P
System: The UNT Digital Library
The Effect of the Maxwell Distribution of Velocities on the Neutron Density and Diffusion Length in a Metal Sphere (open access)

The Effect of the Maxwell Distribution of Velocities on the Neutron Density and Diffusion Length in a Metal Sphere

The change in the simple [formula] distribution of neutrons in a spherical lump of uranium caused by the distribution in velocities of thermal neutrons is calculated. If the calculated curve is fitted as well as possible by a simple [formula] curve, it is shown that the value of [formula] obtained in this way is a function of [formula], the radius of the sphere. For small radii the [formula] obtained in this manner will be as much as 25% greater than the [formula] corresponding to average velocity neutrons. The change in the thermal utilization caused by the distribution in velocities is discussed. The flux of neutrons into a sphere is calculated taking into account the velocity distribution and this is compared with the usual theory.
Date: June 27, 1944
Creator: Plass, Gilbert N.
System: The UNT Digital Library
Identification and Characterization of Shielded Isotopes in Uranium Fission (open access)

Identification and Characterization of Shielded Isotopes in Uranium Fission

Abstract: "The first shielded isotope, 34th Br-82 has been isolated in fission. Its fission yield is about 3 x 10-(-5)%. This is a direct measurement of the yield of a primary fission product and gives direct information as to the distribution of nuclear charge among primary fission fragments of given mass numbers as discussed by Glendenin and Coryell."
Date: November 27, 1946
Creator: Feldman, Milton H.
System: The UNT Digital Library
Studies on the Electrolytic Reduction of Nitric Acid (open access)

Studies on the Electrolytic Reduction of Nitric Acid

Report discussing the reduction of nitric acid that results from its use at the cathode for the electrolysis of uranyl nitrate. From introduction: "It is the purpose of this report to give the results of studies on the reduction of nitric acid of different concentrations, at different types of electrodes, and for various current densities in order to ascertain the effects of such changes."
Date: March 27, 1943
Creator: Hamer, Walter J.
System: The UNT Digital Library
A Study of the Deposition of Boron on Glass and on Metals in the Development of Methods for the Preparation of Diborane (open access)

A Study of the Deposition of Boron on Glass and on Metals in the Development of Methods for the Preparation of Diborane

Report discussing an experiment in which films of boron were deposited on glass and on metals by the thermal deposition of diborane at tempertatures between 500 and 600°C.
Date: March 27, 1944
Creator: Schlesinger, H. I.; Schaeffer, George W. & Barbaras, Glen D.
System: The UNT Digital Library
Experimentation on the Extraction of Uranium from Western Ores (open access)

Experimentation on the Extraction of Uranium from Western Ores

The following report supplements a previous report by E.R. Saunders and M. C. Carosella and a report by A. J. Gailey and E. O. Brimm based around the same subject. This report describes a number of tests in which leaching temperatures of 115 and 125 C were tried for the extractions of uranium from western ores.
Date: December 27, 1943
Creator: Saunders, E. R. & Carosella, M. C.
System: The UNT Digital Library
The Leakage of Neutrons from a Heterogeneous Pile (open access)

The Leakage of Neutrons from a Heterogeneous Pile

Abstract: "The leakage of neutrons from a heterogenous pile with finite aides is calculated developing the method used in CP-992. The change in the fraction of neutrons absorbed by the moderator is obtained using the results of the calculation of the leakage."
Date: December 27, 1943
Creator: Plass, Gilbert N.
System: The UNT Digital Library
The Preparation of TClâ‚„ With Hexachloropropylene (open access)

The Preparation of TClâ‚„ With Hexachloropropylene

Report discussing various reaction methods for preparing TClâ‚„ with hexachloropropylene, as well as various methods for drying the TClâ‚„ after the reaction. Experimental methods are described in detail, and experimental results are presented.
Date: July 27, 1945
Creator: Pitt, B. M.; Curran, W. F.; Schmitt, J. M.; Wagner, E. L. & Miller, A. J.
System: The UNT Digital Library
Recovery of Tuballoy From Solutions Containing Fluoride Ion (open access)

Recovery of Tuballoy From Solutions Containing Fluoride Ion

"Another extraction method is described herein for the quantitative recovery of tuballoy from solutions containing high concentrations of fluoride ion. The method consists of the addition of aluminum nitrate to the solution in order to complex the fluoride ion, followed by saturation with calcium nitrate and extraction of the tuballoy with dibutyl carbitol.
Date: February 27, 1945
Creator: Smith, Fred; Tober, Frank W., 1919-1995; Lord, E. J.; Andrews, L. J. & Gates, J. W., Jr.
System: The UNT Digital Library
The Ion Velocitron (open access)

The Ion Velocitron

This report analyzes the separation of ions using the velocity of the ion measured through a long evacuated drift tube.
Date: January 27, 1947
Creator: Cameron, A. E. & Eggers, D. F.
System: The UNT Digital Library
Electrolytic Reduction of Uranyl Ion (open access)

Electrolytic Reduction of Uranyl Ion

From introduction: "Due to the hydrogen overvoltage at the surface of a mercury cathode, uranium solutions is hydrochloric acid may be reduced not only to the tetravalent state, but until considerable trivalent uranium is formed. Other metallic ions act as oxidation-reduction catalysts as well as being reduced themselves. The following paper is a study of the various reactions taking place in solution and at the surface of the cathode."
Date: May 27, 1946
Creator: Nichols, Ambrose R., Jr.
System: The UNT Digital Library
The Preparation of High-Purity Beryllium Oxide (open access)

The Preparation of High-Purity Beryllium Oxide

Abstract. A method for the preparation of beryllium oxide of high purity is presented. Beryllium basic acetate (BeO-3Be(C2H3O2)2) is prepared from the metal or a convenient salt, a chloroform solution of this material extracted with redistilled water, the dried basic acetate distilled in a quartz apparatus, and this purified material converted to the oxide by fuming down with sulfuric acid and igniting at 1000 degrees C. Impurities detectable spectrographically were reduced to a very low level.
Date: May 27, 1946
Creator: Tomkins, F. S.; Cressman, G. W. & Tolmach, L. J.
System: The UNT Digital Library
Fractionation of Fission Products and Heavy Elements by Volatilization Methods (open access)

Fractionation of Fission Products and Heavy Elements by Volatilization Methods

Technical report describing the attempt to separate the long lived fission product oxides by volatilization methods. A fractionization crucible was used. The fractionations give a fair idea of the relative volatilities of the longer lived fission products and also of the degrees of separation of the plutonium oxide or oxides from the fission products.
Date: August 27, 1946
Creator: Erway, N. D. & Simpson, O. C.
System: The UNT Digital Library
The Diffusion Length of Thermal Neutrons in Uranium (open access)

The Diffusion Length of Thermal Neutrons in Uranium

Measurements made in a uranium cylinder result in a mean value of 1.55 cm. for the diffusion length L for distances of 1 to 4 cm. from the base of the cylinder. Calculations give a value which agrees with the experimental result and show further that L increases from 1.40 to 1.63 cm. as the neutrons diffuse a distance of 5 cm. into the uranium.
Date: May 27, 1944
Creator: Hughes, Donald James, 1915-1960 & Bragdon, E. W.
System: The UNT Digital Library
A Case of Rod Warping (open access)

A Case of Rod Warping

Warping of a rod by a variation in heat transfer coefficient around the periphery is considered. Estimates for some simple cases are given, and a more precise numerical calculation is carried out in ne instance.
Date: May 27, 1944
Creator: Murray, F. & Young, Gale Jay
System: The UNT Digital Library
Summary of the Research Progress Meeting (open access)

Summary of the Research Progress Meeting

Technical report includes three reports of research progress: 1)Neutron scattering by A. Bratenahl; 2) Nuclear Cross Sections, Norman Knable.
Date: May 27, 1948
Creator: Wakerling, R. K.
System: The UNT Digital Library