Five irradiated and five unirradiated wafers were analyzed. Each wafer was analyzed for samarium by emission spectrography. The unirradiated wafers were analyzed for uranium by coulometric and potentiometric methods and for uranium isotopes by mass spectrometry. The irradiated wafers were analyzed for uranium and plutonium by coulometric methods, for plutonium isotopes by the 256-channel alpha pulse analyzer, and for the isotopes of uranium and of plutonium by mass spectrometry. The methods of preparing wafers for analysis are discussed; the data are tabulated.

The feasibility of improving the mechanical properties at 1700-1800°F of oxidation-resistant Fe-Al-Cr alloys by means of a refractory dispersion has been explored. A literature search was conducted, preliminary experimental determinations of properties of the alloy and its oxides were carried out, and certain mathematical relations between dispersion characteristics and metallurgical variables were derived. The results indicate that the alloys can be strengthened sufficiently by using a dispersion with an interparticle spacing of about 2-3 µ. High-temperature native oxides of the Fe-Al-Cr alloy consist largely of Al2O3 and in theory would serve as a satisfactory second phase.