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Method to prepare Semtex (open access)

Method to prepare Semtex

This procedure requires the binder and uncoated RDX be prepared in separate steps, see Figure 1: (1) The binder and dye are mixed by agitation with a water-insoluble organic solvent (e.g., toluene), I; (2) The RDX/PETN is agitated thoroughly with water, II; (3) The binder solution I is added to the RDX/water mixture at II with thorough mixing to form a slurry III; (4) In the next step the solvent is distilled off at IV leaving resulting granules; (5) The next step is followed by filtration at V, which may be done by vacuum; (6) The composition is then dried at VI to a dough-like consistency.
Date: November 26, 2006
Creator: Alcaraz, A. & Dougan, A.
Object Type: Report
System: The UNT Digital Library
Evaluating GC/MS Performance (open access)

Evaluating GC/MS Performance

Evaluating the chemical background in the GC/MS system (system background) and solvent purity. This procedure will allow the analyst to verify that the GC/MS is free of chemical interferences or contamination and verify the solvent being utilized is free of interferences - Conduct a GC/MS analysis without injecting a solvent (system background) and Conduct a GC/MS analysis inject 1uL of CH2Cl2 solvent (Solvent background). GC conditions: (1) Injector Temperature (C): Injector Temperature is typically set at 250; (2) Transferline Temperature (C) - The Transferline Temperature is typically set at 280 C; (3) Constant flow (Sec./cm2) - This value, in seconds per cubic cm. Typically, set at 32; (4) Splitless mode (Sec.) - This value, in seconds, is the time before the purge valve opens. Typically, set at 45 seconds; (5) Starting Temperature (C): The Starting Temperature value can be set at 40 C; (6) Hold Time 1 (Min.) - Hold Time 1 is the amount of time, in minutes at the Starting Temperature that Ramp 1 Temperature is held. Typically set at 3 minutes; (7) Ramp 1 Rate (C/Min.) - Ramp 1 Rate is the temperature rise per unit time and has a typically value of 8 C per minute …
Date: November 26, 2006
Creator: Alcaraz, A. & Dougan, A.
Object Type: Report
System: The UNT Digital Library
Seminole Sentinel (Seminole, Tex.), Vol. 98, No. 14, Ed. 1 Sunday, November 26, 2006 (open access)

Seminole Sentinel (Seminole, Tex.), Vol. 98, No. 14, Ed. 1 Sunday, November 26, 2006

Semiweekly newspaper from Seminole, Texas that includes local, state, and national news along with extensive advertising.
Date: November 26, 2006
Creator: Wright, Dustin
Object Type: Newspaper
System: The Portal to Texas History
Polk County Enterprise (Livingston, Tex.), Vol. 124, No. 95, Ed. 1 Sunday, November 26, 2006 (open access)

Polk County Enterprise (Livingston, Tex.), Vol. 124, No. 95, Ed. 1 Sunday, November 26, 2006

Semi-weekly newspaper from Livingston, Texas that includes local, state and national news along with advertising.
Date: November 26, 2006
Creator: White, Barbara
Object Type: Newspaper
System: The Portal to Texas History
The Panola Watchman (Carthage, Tex.), Vol. 133, No. 93, Ed. 1 Sunday, November 26, 2006 (open access)

The Panola Watchman (Carthage, Tex.), Vol. 133, No. 93, Ed. 1 Sunday, November 26, 2006

Semiweekly newspaper from Carthage, Texas that includes local, state, and national news along with advertising.
Date: November 26, 2006
Creator: unknown
Object Type: Newspaper
System: The Portal to Texas History
Altus Times (Altus, Okla.), Vol. 108, No. 205, Ed. 1 Sunday, November 26, 2006 (open access)

Altus Times (Altus, Okla.), Vol. 108, No. 205, Ed. 1 Sunday, November 26, 2006

Daily newspaper from Altus, Oklahoma that includes local, state, and national news along with advertising.
Date: November 26, 2006
Creator: Bush, Michael
Object Type: Newspaper
System: The Gateway to Oklahoma History
The Express-Star (Chickasha, Okla.), Ed. 1 Sunday, November 26, 2006 (open access)

The Express-Star (Chickasha, Okla.), Ed. 1 Sunday, November 26, 2006

Daily newspaper from Chickasha, Oklahoma that includes local, state, and national news along with advertising.
Date: November 26, 2006
Creator: Bush, Kent
Object Type: Newspaper
System: The Gateway to Oklahoma History
When the guest of honor is a party pro, it better be good: Austin fête celebrates author (open access)

When the guest of honor is a party pro, it better be good: Austin fête celebrates author

Article about Lara Shriftman and Elizabeth Harrison, co-owners of marketing, public relations, and planning firm Harrison & Shriftman and co-authors of the book "Party Confidential."
Date: November 26, 2006
Creator: Scheidnes, Jean
Object Type: Article
System: The UNT Digital Library
Sapulpa Daily Herald (Sapulpa, Okla.), Vol. 92, No. 13, Ed. 1 Sunday, November 26, 2006 (open access)

Sapulpa Daily Herald (Sapulpa, Okla.), Vol. 92, No. 13, Ed. 1 Sunday, November 26, 2006

Daily newspaper from Sapulpa, Oklahoma that includes local, state, and national news along with advertising.
Date: November 26, 2006
Creator: Mattox, Jami
Object Type: Newspaper
System: The Gateway to Oklahoma History
The Baytown Sun (Baytown, Tex.), Vol. 86, No. 1, Ed. 1 Sunday, November 26, 2006 (open access)

The Baytown Sun (Baytown, Tex.), Vol. 86, No. 1, Ed. 1 Sunday, November 26, 2006

Daily newspaper from Baytown, Texas that includes local, state, and national news along with advertising.
Date: November 26, 2006
Creator: Clements, Clifford E.
Object Type: Newspaper
System: The Portal to Texas History