Effect of Temperature on Beta-Ray Measurements (open access)

Effect of Temperature on Beta-Ray Measurements

Summary: "This report investigates photographic methods of measuring beta radiation and includes a study of temperature effects on these measurements. Experimental data are submitted to show that an increase in film temperature before and during beta irradiation causes a definite increase in density for the same dosage. Recommendations drawn from experience gained in the experimental works are offered."
Date: November 23, 1949
Creator: Stevens, A. J.
System: The UNT Digital Library
A Method of Recovering Thorium from Slag Materials (open access)

A Method of Recovering Thorium from Slag Materials

Abstract. a method of recovering thorium from slag from the bomb process of producing thorium has been developed. HCl and NaOH are the only chemicals required in quantity. Materials required for a representative slag are given.
Date: March 23, 1945
Creator: Johnson, Oliver & Fisher, R. W.
System: The UNT Digital Library
Procedures for the Separation of Products Resulting From Bombardment of Heavy Elements (open access)

Procedures for the Separation of Products Resulting From Bombardment of Heavy Elements

Technical report that attempts to bring together the various chemical procedures which proved most useful in studying the results of cyclotron bombardment or small scale neutron bombardments of heavy element targets. The report is limited to the elements of the "actinide", or second rare earth series, starting with thorium and including the newly discovered elements of atomic number 95 and 96. Every attempt is made to include all details necessary so this report can serve as a practical laboratory guide. The report covers separation problems, time factors, and dealing with dangerously radioactive targets.
Date: September 23, 1946
Creator: Thompson, Roy
System: The UNT Digital Library
A Method for Preparing Large Tungsten-Copper Pieces (open access)

A Method for Preparing Large Tungsten-Copper Pieces

Abstract: "This report includes details of the procedure along with the die and equipment descriptions for preparing tungsten copper alloy pieces."
Date: September 23, 1946
Creator: Hirsch, Harold
System: The UNT Digital Library
Fabrication of Ceramic Shapes (open access)

Fabrication of Ceramic Shapes

Abstract: "This report indicates some of the methods employed at Los Alamos for the fabrication of refractory products."
Date: December 23, 1946
Creator: Mullen, Terence & Taub, James M.
System: The UNT Digital Library
Summary of Research on Experimental Refractory Bodies of High-Melting Nitrides, Carbides, and Uranium Dioxide (open access)

Summary of Research on Experimental Refractory Bodies of High-Melting Nitrides, Carbides, and Uranium Dioxide

Abstract: A procedure for the preparation of the nitrides and carbides of several metals and the preparation of the refractory bodies from them is described. The investigation shows that reasonably strong and dense bodies can be prepared from these materials as well as from UO₂. Evidence showing the tendency toward instability at high temperatures of Be₃N₂, TaN, and ThN is presented. Evidence is also given indicating that the hexagonal structure reported by others for TaN is actually that for Ta₂N. A lattice for Th₂N₃ is proposed. The melting points of ThN, UN, and UC are determined to be 2630 ± 50°C,2650 ± 100°C, and 2590 ± 50°C respectively.
Date: April 23, 1949
Creator: Chiotti, P.
System: The UNT Digital Library
The Analysis of Impurities in Various Stages of Recycled Carbon Tetrachloride and Correlation with Chlorination Properties (open access)

The Analysis of Impurities in Various Stages of Recycled Carbon Tetrachloride and Correlation with Chlorination Properties

The following report discusses findings resulting from experiments on recycled carbon tetrachloride at various stages of the proposed purification process.
Date: May 23, 1946
Creator: Hudson, R. L.; Burkhart, L. E. & Larson, C. E.
System: The UNT Digital Library
Modified Liquid Phase Reactor (open access)

Modified Liquid Phase Reactor

The following report describes a modified Kraus type reactor that had been constructed for use in bets chemical conversion operations.
Date: June 23, 1944
Creator: Zuidema, J. W. & Ballard, A. E.
System: The UNT Digital Library
Voltage Regulator for Electroplating Control (open access)

Voltage Regulator for Electroplating Control

This report describes an instrument used for electrolytic separation. It was one of four instruments previous used and improved, yet lacked details until now. The instrument's design and operation is described herein.
Date: December 23, 1946
Creator: Rogers, Lockhard Burgess & Pickle, C. B.
System: The UNT Digital Library
The Application of Tracer Techniques to the Determination of Uranium Extraction Coefficients (open access)

The Application of Tracer Techniques to the Determination of Uranium Extraction Coefficients

Abstract: This report deals with the development of a method using tracer technique for determining uranium extraction coefficients on solutions of low uranium concentration. It was found that extraction coefficients could be determined on systems containing as low as one part per million uranium using 1900 level uranium as the tracer. Results of several extraction series are presented in which aluminum nitrate is used as the salting agent and dibutyl carbitol the organic extractant.
Date: January 23, 1947
Creator: Lee, D. A.; Woodard, R. W. & Clewett, G. H.
System: The UNT Digital Library
The Metabolism of Thorium, Protoactinium, and Neptunium in the Rat (open access)

The Metabolism of Thorium, Protoactinium, and Neptunium in the Rat

From abstract: "The distribution of carrier-free thorium, protoactinium and neptunium in the rat following intramuscular and oral administration has been studied. Oral adsorption for all three is negligible. Following parenteral administration, the skeleton is the organ showing the highest degree of prolonged and selective localization."
Date: August 23, 1946
Creator: Lans, H.; Scott, E. G.; Crowley, J. & Hamilton, J. G.
System: The UNT Digital Library
The Determination of Thorium in Uranium-Thorium Alloys, Using Cupferron (open access)

The Determination of Thorium in Uranium-Thorium Alloys, Using Cupferron

Technical report describing that the use of controlled amounts of carbonate, acting both as complexing agent buffer led to a fairly satisfactory procedure for the determination of Th in Th-U alloys, using cupferron. The alloy, dissolved in NHO2, in the presence of HF, is treated with H2SO4 and the mixture is evaporated in SO2 fumes. The solution is diluted and (NH4)2CO2 is added. Th is precipitated from this solution with cupferron. The precipitate is weighed as ThO2 after ignition. An accuracy of 6% was obtained. A method was developed specifically for the determination of Th in U-Th alloys containing 1 to 10% Th. An ion exchange resin in column is used to separate Th from U, with NH2OH-HCl as complexing agent. The Th is then precipitated, ignited, and weighed in the conventional manner.
Date: November 23, 1945
Creator: Eckert, A. C. & Bane, R. W.
System: The UNT Digital Library
Jacket Temperature Near End of Slug (open access)

Jacket Temperature Near End of Slug

Some situations which give rise to a hot ring around the slug near the end are considered; namely rounded slug ends in the long cartridge design, and the Wilkins effect in the current unbonded short slug design.
Date: June 23, 1944
Creator: Young, Gale Jay
System: The UNT Digital Library