Report discussing studies on various types of protective coatings for a molybdenum sheet. Procedures, materials, and results of each coating are included.

From abstract: "In this report we present data obtained with the optical simulation apparatus on image quality as a function of the parameters of neutron scattering and image detector resolution...Also included in this report is a brief description of a large area (5 inch diameter) neutron beam exposure facility being set up at the reactor for the phase three work."

The following report follows a series of experiments on the freezing points of 25 UN-H2O-HNO3 solutions.

Report discussing reaction of hydrogen with uranium in a range of temperatures and pressures. Experimental materials, methods and results are included.

Abstract: "A method for determination of dibutyl phosphate in solvent streams containing tributyl phosphate is outlined. The method is based on analysis for total uranium of total phosphate after removal of uranium and phosphate in excess of that present as uranyl dibutyl phosphate. Results on plant solvent samples are presented. Difficulties with precipitation of [...] dibutyl phosphate, when fresh solvents were employed, are discussed. Small amounts of nonphosphate uranium-complexing agents were found in plant solvents. Diluent degradation is postulated as the source of these components. Emulsion-formation tendencies appeared to correlate better with concentrations of these contaminants than with dibutyl phosphate content."

Report discussing a study of various resistance-welding methods for end capping PWR uranium oxide fuel rods. Flash, upset, and spot welding were all investigated.

The following report describes two rapid, micro methods for the determination of UNH in Redox waste samples that had been developed fir the concentration range 0.2 to 100 g/l.

The following report analyzes the results taken from studies on the characteristics of the bond interface formed between zircaloy 2 and uranium-12 w/o molybdenum alloys.

From abstract: "The extraction of acids with long-chain amines is described. Preliminary results on the extraction of the amine salts of polonium, plutonium and uranium are given."

Technical report calculating "effective removal cross sections" for Pb, Fe and O from measurements of fast neutron does in the water surrounding the BSF reactor. The values for Pb and Fe agree quite well with those previously determined from Lid tank data, whereas that for O is somewhat lower. [From Abstract]

From abstract: "Scattering cross sections have been computed for zero-energy neutrons incident upon a square well of spheroidal symmetry, depth 42 Mev, and volume equal to that of a sphere of radius 1.45 x 10⁻¹³ ^1/3 cm."

Report that summarizes unreported neutron-yield data for the MnSO₄ tank method. Other yield measurements had been reported in other quarterly reports prior to the completion of this one.

Abstract: And investigation of the interactions between 300-Mev neutrons and xenon was made by means of a cloud chamber in a pulsed magnetic field of 21,700 gauss placed in the neutron beam of the 184-inch Berkeley cyclotron. Eighty-seven negative pion events and 257 other stars were analyzed. In addition an experimental check was made on the energy of the incoming neutrons. Classification, identification, and angular and energy distributions of prongs associated with all events are presented. Interpretations of results are given.

From summary: The object of the study was to determine if the heavy metal ions within the concentration ranges normally found in pile cooling water were responsible for corrosion of aluminum.

Abstract: "Laboratory production of an explosion between UNH and "red oil" under calcination conditions has been accomplished. Attempted production of a vapor phase explosion was unsuccessful below 150-160 C. Since such severe conditions are necessary to obtain an explosive reaction, it appears that present Purex plant design is adequate to avoid explosive conditions."

Technical report. Areas covered are properties of uranium halides, properties of uranium nitrides, and hydride formation at high pressure.

The resonance absorption of a lump is described in terms of three components. Calculations of resonance absorption are carried out using the model for the resonance spectrum of uranium recently derived; calculations are also made with variations of this model which involve local fluctuations in level strengths. For metal and oxide lumps the agreement with observation is satisfactory. For dilute mixtures, whose resonance activation was measured by Mitchell, computed values fall 20% to 30% above measured ones.

Abstract. If a pile rod gets bowed within its cooling tube it becomes warmer on the side which approaches the tube wall, and thermal expansion tends to warp it in the same direction as the original displacement. This was discussed roughly in N-601, and it was there concluded that the mechanism was not important for an isolated short slug. In connection with current development of continuous jacket (cartridge) assemblies, it seems desirable to look at this question again. In this case it is possible that the effect may be of some concern.

Introduction: This report embodies the results of an investigation as to the possibility of removing the bulk of the iron from gunk solutions of various concentrations by precipitation of the iron with phthallic acid and subsequent precipitation of tuballoy. The method consists of dissolving the phthallic acid in the gunk solution and then adding NH₃ to a suitable pH, precipitating the iron, and leaving the tuballoy in solution.

Abstract: The distillation and residue extraction recovery procedures developed for the recovery of uranium from Kinney and diffusion pump oil, were applied to contaminated precipitron oil. The effectiveness and advisability of using the method, in whole or in part, is discussed, and various recommendations for processing this particular type of oil are presented. Additional contaminating substances present in this type of oil added to the complexity of the problem but a satisfactory recovery procedure was, nevertheless, successfully developed.

"This bibliography is limited to book and journal references covering methods and instruments in general for measuring high temperatures. The search included only literature from 1950 to the present [1957]."

Report summarizing physical studies on Redox solutions and metal waste solutions, including refractometric investigations.

The behavior of insoluble corrosion products in the HRT is generally understood and studies of the removal of these solids by hydroclones can logically be terminated after the effect of higher processing rates by the multiple hydroclone has been determined. Chemical descaling may be required to supplement solids removal by hydroclones. Laboratory studies to find suitable reagents will be continued in conjunction with decontamination work presently in progress.

The creep problems associated with zircaloy-2 process tubes and the factors affecting the creep of these tubes were discussed in detail. Emphasis was placed on the determination of the tube wall thickness for an SPR tube, whose minimum thickness is limited by creep considerations. It was concluded that, at the present time, there is not enough information available to design zircaloy-2 process tubes on a realistic basis. Various experiments were suggested to supplement the creep rate testing program being pursued by Battelle Memorial Institute.