Abstract: "A general description is given of the permanent zirconium plant at Y-12. Equipment is described and materials of construction are listed. Photographs illustrating principal equipment and reduced construction drawings are also presented. Operating conditions and costs information are listed."

Abstract: A re-evaluation of the cost of producing essentially hafnium free zirconium as zirconium oxide at a rate of 150,000-200,000 pounds zirconium per year by solvent extraction of the metal thiocyanates in a permanent plant has been made. Using part of the present temporary facilities, the cost, with five year amortization of the plant, will be $3.15 per pound zirconium. A by-product of the mixed oxides of hafnium and zirconium, having at least fifty percent hafnium and perhaps as high as ninety percent hafnium, can be made available with little additional cost.

Abstract: Use of the mixer-settler apparatus as a rapid means of determining improved conditions for plant operation is described including the experimental details. The preparation of highly purified samples of both zirconium oxide and hafnium oxide is discussed. (This document is concerned almost entirely with explorations of small scale continuous systems. Another document dealing with this general problem using small scale batch operations is being published simultaneously. It should prove of advantage to the reader to study this companion report, Document Y-611, by Barton, Overholser, and Grimes, to obtain a complete picture of the available information.).

From abstract: "The extraction of acids with long-chain amines is described. Preliminary results on the extraction of the amine salts of polonium, plutonium and uranium are given."

Technical report calculating "effective removal cross sections" for Pb, Fe and O from measurements of fast neutron does in the water surrounding the BSF reactor. The values for Pb and Fe agree quite well with those previously determined from Lid tank data, whereas that for O is somewhat lower. [From Abstract]

Technical report. Areas covered are properties of uranium halides, properties of uranium nitrides, and hydride formation at high pressure.

Introduction: This report embodies the results of an investigation as to the possibility of removing the bulk of the iron from gunk solutions of various concentrations by precipitation of the iron with phthallic acid and subsequent precipitation of tuballoy. The method consists of dissolving the phthallic acid in the gunk solution and then adding NH₃ to a suitable pH, precipitating the iron, and leaving the tuballoy in solution.

Abstract: The distillation and residue extraction recovery procedures developed for the recovery of uranium from Kinney and diffusion pump oil, were applied to contaminated precipitron oil. The effectiveness and advisability of using the method, in whole or in part, is discussed, and various recommendations for processing this particular type of oil are presented. Additional contaminating substances present in this type of oil added to the complexity of the problem but a satisfactory recovery procedure was, nevertheless, successfully developed.

The following report presents data from the SALMON experiment, an experiment made to study the mechanics of a tamped nuclear detonation in a salt dome in terms of generated shock waves as they are propagated out of the dome and progressively through the crust and mantle of the earth. This experiment was made in the Tatum salt dome, Mississippi, October 22, 1964.

Abstract: The report describes the results of an experimental study involving the injection of a gaseous secondary jet into an unbounded supersonic flow field which was uniform outside of a turbulent boundary layer. The investigation was principally concerned with the formulation of the shock wave shapes and streamline patterns to be associated with typical turbulent, two-dimensional jet-interaction flows. In support of this objective, results are presented for a Mach 5 test conducted using a flat-plate model containing a sonic secondary jet directed normal to the main-stream. The jet-interaction flow field was primarily investigated for jet strengths (ratio of jet gas stagnation pressure to free-stream static pressure) of 180 and 550. Intermediate strengths were also studied but in lesser detail. Local flow properties were measured throughout the flow field and surface pressure distributions were recorded fore and aft of the secondary jet. From these data and complementary shadowgraph studies, the streamline pattern and attendant shock structure were formulated.

The following report provides data taken from investigations on radiation and the different biologic effects on it.

The following document is meant to inform the reader on the makings of a cement base for the hot filament mass spectrometer source as part of a publication in the review of scientific instruments, "Laboratory and Shop Notes".

This report follows a test made to determine the effect of temperature on the distribution of nitric acid between "carbitol" and gunk, extracting a number of samples of aqueous copper nitrate with samples of "carbitol" of various acidities. The data obtained is covered in Table 1.

Report outlining a study that tested the use of colorimetric methods with high concentration phosphoric acid as a solvent for rapid analysis of mixtures of T^+4 and T^+6.

"Changes, corrections and additions to the original report are included in this addendum. These are brought about by further development of the design by Blaw-Knox, ANL and ORNL. The changes are listed in accordance with the main headings, pages and paragraphs to which they apply."

Report discussing the fractionation study of tri-n-butyl orthophosphate as the organic phase using a solution of trivalent rare earth chlorides or nitrates as the aqueous phase.

Report discussing several experiments investigating the effect of radiation on metals, specifically on intermetallic diffusion, mechanical properties of 347 stainless steel and electric resistance of 347 stainless steel.

Abstract: "A novel procedure employing ion exchange resins was developed to separate chromate ions from hydrogen peroxide, permitting, permitting the subsequent analysis of peroxide to determine its decomposition in sodium chromate solutions. At high pH's, peroxide was absorbed anionically on the ion exchange resins along with chromate. By selecting a resin which would be effective at nearly neutral conditions, chromate was satisfactorily separated from peroxide. It was found that the rate of peroxide decomposition in slightly alkaline sodium chromate solutions was dependent on temperature, pH, aeration, and chromate concentration. No significant effect on decomposition was caused by visible light."

The following report is a study of the separating qualities of a loop-type separator that can obtain separation with a smaller pressure drop.

Abstract: "Uranium monocarbide-Zircaloy II alloy cermets were developed and tested for chemical and physical properties. It was determined that pure uranium monocarbide can be prepared by vacuum are melting techniques. Following melting, the combination, hot pressing, and corrosion behavior of dense monocarbide has been studied. The preparation of uranium monocarbide-Zircaloy II cermet bodies was investigated by means of hot pressing, cold pressing and sintering, warm pressing, extrusion, and hot rolling. The corrosion resistance of the cermets was related to such variables as composition, preparation technique, and powder size. 01 per cent uranium monocarbide, 70 per cent zircaloy II cermets withstood corrosion tests in 680 F water. Cermets having above 30 weight per cent uranium monocarbide were not corrosion resistant."

From introduction: "The purpose of the present report is to describe briefly certain improvements that have been made in the experimental facilities and to present the results of further measurements on critical masses and spatial neutron flax distributions in Be reflected reactors having square and thin slab geometries."

Abstract:"A method is described for the electroreduction of plutonium to the +3 valence state in a nitric acid-sulfamic acid solution. Exploratory experiments in the search for a coulometric titration of Pu(III) using electrolytically generated ceric ion are also described. The results strongly indicate that a convenient procedure can be devised. Suggestions for future work are presented."

From abstract: The estimation of beryllium oxide in beryllium metal depending on the differential solubilities of the two material in dilute hydrochloric acid is presented. The results compare favorably with the present beryllium chloride volatilization procedure. Alternate methods are described, and the limitations and possible errors are discussed.

"The most hasardous conditions relating to the storage and handling of the SRE fuel are those in which water and fuel form a possible critical assembly. Therefore, this memorandum is primarily devoted to an analysis of the conditions necessary for a critical mixture of water and SRE fuel. Certain special geometries are then analyzed for their safeness."