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The Hydrolysis of Tributyl Phosphate Ad Its Effect on the Purex Process
From abstract: "The rate of hydrolysis of TBP and the effect of the hydrolysis products in the Purex Process have been studied. Hydrolytic conditions may be encountered in the process which would lead to formation of dibutyl phosphoric acid, causing significant losses of tetravalent plutonium in stripping. This situation may be easily alleviated by reducing and stripping the plutonium in the trivalent state."
Date:
December 13, 1951
Creator:
Reilly, V. J. & Lanham, W. B.
System:
The UNT Digital Library
Crystal Densities of Uranium Chlorides
Abstract: "Using xylene as the densimetric solvent, the crystal densities have been determined by the pyknometric method for the following chlorides, UCl3, UCl4, UCl6(UCl4), UCl6 and U02Cl2."
Date:
December 13, 1946
Creator:
Sterett, C. C. & Calkins, V. P.
System:
The UNT Digital Library
Airborne Reconnaissance in Southwestern Arkansas
Introduction: Reconnaissance for uranium in central and southwestern Arkansas was carried out as a joint project of the U.S. Atomic energy Commission and the U.S. Geological Survey during March and May 1954. The project was planned as an investigation of several areas of known abnormal radioactivity, and as a search for others, by airborne and ground radiometric reconnaissance.
Date:
December 13, 1954
Creator:
Malan, R. C. & Nash, A. L.
System:
The UNT Digital Library
The Crystal Structure and Thermal Expansion of Gamma Plutonium
Gamma plutonium is found to be orthorhombic with eight atoms in a unit cell of dimension (1t 235 degree C) [formula]. The calculated density is [formula]. The space group is Fddd and the positions of the eight atoms are: [formula]. Each plutonium atom is bonded to ten others at an aver distance of [formula], four being at [formula], two at [formula] and found at [formula]. The mean linear coefficients of thermal expansion are found to be [formula].
Date:
December 13, 1953
Creator:
Zachariasen, William H. (William Houlder), 1906-1979 & Ellinger, F. H.
System:
The UNT Digital Library
Equation of State of Solids
Data which determine points on the Hugoniot curves of fourteen solids are given in the technical report.
Date:
December 13, 1954
Creator:
Walsh, J. M. & Yarger, F L.
System:
The UNT Digital Library
The Weighting of Intensities
Technical report. From report : "The method of least squares refinement is based on the prediction of the theory of errors that, if the errors of the observed structure factors follow the Gaussian distribution, the most nearly correct atomic parameters will be those which result in the minimization of the residual R = Σi [√wi(|Fo| - |Fc|)i]2."
Date:
December 13, 1962
Creator:
Hershaft, Alex & Corbett, John D.
System:
The UNT Digital Library
The Crystal Structure of Bis(Meta-Chlorobenzoyl) Methane
Technical report. From Abstract : "The crystal structure of bis(meta-chlorobenzoyl) methane has been determined by three dimensional anisotropic least squares refinement of scintillation counter data. The molecule was found to be nearly planar with a maximum deviation from the least squares molecular plane of 0.068Å and an average deviation of 0.023Å. Fourier transform techniques to locate phenyl rings provided the key to the structure determination. The intramolecular bond distances and thermal parameters of the oxygen atoms support a resonant, enol ring with a symmetric, intramolecular hydrogen bond. The structure confirms conslusions from the structure of bis(meta-bromobenzoyl) methane where the symmetry of the molecule was forced by the crystal symmetry."
Date:
December 13, 1962
Creator:
Engebretson, Gordon R. & Rundle, R. E.
System:
The UNT Digital Library
Chemical Properties of Sodium Triethylhydroborate and Sodium Triisopropoxyhydroborate
Technical report abstract: Sodium hydride and triethylborane react to form sodium triethylhydroborate, NaBH(C2H5)3. This compound, a liquid at rooom temperature, was found to be soluble in hexane and mineral oil. A study was made of the thermal decomposition of sodium triethylhydroborate and its behavior toward boron trifluoride, boron trichloride, methyl borate, carbon dioxide, silane, and ethylene. Sodium triisopropoxyhydroborate, NaBH(OC3H7)3, was prepared and also found to be soluble in hexane and mineral oil. The reactions of this compound with methyl borate, triethylborane, silicon tetrachloride, and boron trichloride were investigated.
Date:
December 13, 1956
Creator:
Pearson, Richard King, 1926-; Edwards, L. J. & Maginnity, P. M.
System:
The UNT Digital Library