The following report provides data from completed tests for corrosion testing of stellite-T347 stainless steel test cylinders.

This report analyzes infrared absorption measurements that were made in the regions of carbonyl band and hydroxyl band absorptions on solutions of water in hexone and water in acetone, confirming intermolecular association of water and hexone.

Abstract: An investigation was conducted to determine the absorption and translocation of fission products by Russian thistle from a localized spot of contaminated soil. The amount and identity of the radioactive elements absorbed and translocated by the Russian thistle is given along with the location of these elements in the plants. Beta radioactivity to the amounts of 10 microcuries per gram caused no visible effects on the growth habits of sectioned material are included.

From summary: "The methods of calibrating the 305 pile for impurities and density differences in graphite are reviewed and calibration constants are calculated theoretically."

Report discussing an impinging experiment "to test the pitting tendencies of different qualities of water," specifically, alum coagulated water without sodium dichromate, alum coagulated water plus 2 ppm sodium dichromate, and ferrifloc coagulated water without sodium dichromate.

The results of electrical resistance measurements have been used as a means of following changes occurring in metals due to irradiation. The electrical conductivity is sensitive to changes in composition and to cold-work or structure damage. In an anisotropic metal, such as uranium, the director of measurement also influences to some extent the values obtained. For these reasons it is essential to use the same material, and if possible the same piece of material, in comparing the electrical properties before and after irradiation. This report is a description of the measurements made on pieces of the same uranium rod before and after an exposure of approximately 150 MWD/T. The results, while preliminary in nature and dealing only with one sample and exposure level, provide data for which a comparison may be made of the electrical resistivity of irradiated and non-irradiated uranium metal.

The gas commonly used in the chamber of the Simpson Proportional Alpha Counter (ASP) is the high grade, 99% pure methane. The cost of the gas has often raised the question of finding an adequate substitute and a number of substitutions have been attempted. Commercial methane has been substituted successfully for 99% pure methane and its use is recommended in ASP counters. Neither commercial nor technical methane caused any significant changes in instrument operation.

This report contains the results of tests which demonstrated the feasibility of using graphite labyrinth type seals, i.e., a bushing machined with alternate grooves and lands on the inside diameter to create a sufficient pressure drop to provide a satisfactory seal.

The primary objective of the tests described herein was to determine if the standard five bend connector (drawing H-1-23475) and/or the T. F. Robinson three bend connector (drawing SK-1-20855) fabricated from Type 304 stainless steel tubing would satisfy the requirements of the K reactors. Results of the tests show that the standard five bend connector made from Type 304 stainless steel 0.065 inch wall tubing, in the as bent condition, with either cadmium plated Parker brass nuts and sleeves or cadmium plated high carbon steel nuts and sleeves, is suitable for installation of the K reactors.

This work was performed to develop a general chemical method for the determination of small amounts of plutonium in solution. The work showed that a coulometric titration based on the preliminary oxidation of the plutonium to Pu (VI) followed by titration with electrolytically-generated ferrous ion to Pu (IV) was such a general method and was subject to few interferences. The significance of the work is that a chemical determination of plutonium can be made for amounts of plutonium heretofore determined only by radioassay methods, and the chemical determination of larger amounts are made more readily and with higher precision than with previous methods. The work also extends the application of coulometric titration methods to a new substance.

In the reference document, a statistical method for analyzing run to rupture tests involving two metal types, a test material and a control standard, is presented. It often happens that more than two metal types are involved in a production test. In this document, the statistical procedure recommended for this situation is presented.

Report discussing a possible solution for providing a remotely operated way of handling samples at an irradiation facility. Explanation of operating requirements, equipment, and a possible layout is included.

Report discussing a test aimed at determining if high velocity water could cause severe pitting in 72-S aluminum. This test was designed after an increase in the amount of pitting-caused water leaks in reactors.

Well-type scintillation counters have found use in many radiochemical laboratories. A gamma scintillation well counter has been used to measure the gamma activity of liquid samples in the 325 Building counting room for about a year. This well counter has been built and calibrated so that gamma activity measurements made with it can be easily compared with measurements made with the gamma scintillation counter (GSC). The well counter is electronically identical to the present GSC and differs only in the shape of the crystal used and the physical arrangement of the lead shield. The crystal contains a well which allows a tube containing the sample to be inserted in the crystal. The physical arrangement of the detector greatly simplifies the preparation of liquid samples for activity measurement. The 325 Building well counter and its application to chemical research and plant process analysis will be discussed in the following paragraphs. An operating procedure is also included.

Methods of the Radiation Monitoring Operation of the Chemical Processing Department.

The information in this report is based on experience with a similar unit installed on experimental pule columns in the 321 Building. These installations were made to demonstrate the feasibility of the system. In one case, the installation on the 2A Prototype Column, the differential pressure cell (D/P cell) bottom interface control system was monitored by a capacitance-type instrument. The other installations were made on glass columns and were monitored visually.

Purex process which utilizes solvent extraction to separate and purify uranium and plutonium from each other and from fission products contained in irradiated uranium fuel elements.

The HAPO Critical Incident Alarm, Model I, is an instrument designed to give an audible and visual alarm signal in the event of a critical incident to which it is exposed. There will be thirty-one (31) of these instruments installed and several spares located in the various manufacturing buildings in the Chemical Processing Department where there exists any possibility of a critical incident occurring. The instrument is intended as a post or after-the-fact warning device. It will offer no protection prior or leading up to, nor prevent, a critical incident. They are intended to be operated from the 115 V. A.C., 60 C.P.S. emergency line power. The instrument is self-contained, including the radiation detector, and will be calibrated to alarm at 500 mr/hour in a gamma field.

Nearly all nuclear reactors being designed and built today- whether for research, power, or productions of fissionable materials- use recirculating fluids for cooling. However, a number of production reactors are still operating with single-pass cooling by treated natural water. The Hanford Atomic Products Operation of the General Electric Company presently operates production reactors for the AEC at Richland, Washington. The first reactors were built during World War II, and utilized a standard water treatment which was designed to provide large quantities of settled, filtered Columbia River water for once-through cooling.

Zirflex cladding waste is to be neutralized to pH 10 before transfer to waste storage tanks. This treatment causes the precipitation of zirconium oxide or hydroxide, which may lead to flow difficulties during transfer. The purpose of this investigation was to determine the physical properties and flow characteristics of the neutralized slurry to assist in the selectin of satisfactory transfer equipment and storage conditions.

Space has been reserved near the southeast corner of the 100-N Area for the 122-N Decontamination Facility. Previous correspondence between Burns and Roe, Inc and General Electric bae discussed various facilities which might be needed in the building. The concepts of the decontamination processes are under active development by research groups at Hanford. At present, there are several workable processes known; each one has one or more fairly serious drawbacks.

In many cases of analysis of two-phase flow in systems, considerable computation or program time could be saved if the critical pressures ratio were known. If a reservoir or plenum pressure is fixed, the usual computational procedure involves the assumption of several critical pressures and the generation of several momentum terms to find the applicable critical pressure ratio and thereby the critical flow. The formulation of an equation of state make it possible to compute critical pressure ratios directly.

The amount of dry air or inert gas supplied to a "one pass" glove box ventilation system is proportional to the glove box inleakage. Most glove boxes in the 234r5 Building are equipped with sundry attachments, each contributing to the inleakage. No individual leak rate date is available for these auxiliary components in the "as installed" condition. Nor is the effect of time upon the leak rates known. Knowledge of these values, or at least an indication of the order of magnitude of the leakage attributable to each item, would provide a basis for analyzing glove box ventilation problems and for establishing criteria for new glove box designs.

A coolant line rupture during operation of a high temperature gas cooled graphite moderated reactor would present a serious hazard. The reactor would immediately depressurize and a great deal of air would be introduced into the coolant stream. As the air passed over the graphite moderator a runaway oxidation reaction would probably ensue unless an adequate safety system were available. This investigation was designed to evaluate chlorine as a reactor safeguard to be used to control a runaway reaction. Throughout this study, a small amount of chlorine in an air stream has demonstrated the ability to substantially reduce the oxidation rate of graphite. This has been the case even where the principal oxidizing agent was molecular oxygen or ozone.