The following report follows the studies of electroplating on uranium and concurrent metallurgical clodding.

Abstract: Chemical and physical data on twenty binary uranium compounds that may prove suitable for refractory nuclear fuels were assembled. The compounds were those with aluminum, boron, carbon, iron, nickel, nitrogen, silicon, or sulfur. Too little is known at this time about the compounds to evaluate any of them for fuel. The program is being extended in an effort to provide the needed data.

The following document is a note describing the building process of an improved nuclear density gauge in comparison to previous gauges, within the interval of July 1 to August 1, 1959.

From introduction: "The ORNL-ANP liquid-to-liquid heat exchanger design and development effort has been based on an exceptionally high performance matrix of closely-spaced small diameter tubes that permits practically pure counter-flow operation. In the course of full-scale aircraft power plant design work a number of charts for this type of heat exchanger has been prepared. These charts were intended in part to show the effects of the various parameters in a readily understandable form, and in part to simplify and to reduce markedly the chore of making detailed design calculations. These charts have proved so helpful it seemed very worthwhile to assemble them into a report along with brief explanations and sample calculations."

From abstract: "On the 86-inch cyclotron a 41-kw beam has been calorimetered at a net ion loading efficiency of 40%; the average proton current was 1.85 ma at 22.5 Mev. Practical specific yields have been determined for (p,2n) reactions on zinc and bismuth. The investigation of products of proton-induced fission of uranium has been continued and new techniques are being used in measuring angular distribution of reaction products. The 63-inch heavy particle cyclotron is now in operation; N+++ particles have been accelerated to ~25 Mev. In preliminary tests, induced activities have been detected in carbon, nitrogen, and oxygen targets. A hot-cathode ion source is ready for test operation. The 22-inch cyclotron is being used in an investigation of the problems associated with the use of rf and dc electrodes for the acceleration of protons from the ion source into the dees. Radiation-induced corrosion in Inconel tubing containing #21 eutectic (ANP) has been produced by proton irradiation in the 86-inch cylclotron; it is shown that the corrosion was not due to thermal effects. Approximately 150 grams of highly purified U 238 (< 5 ppm U 235) have been prepared, and two grams of thorium 230 (ionium) has been enriched to 90.6%."

Technical report outlining the physical operability of 30% tributyl phosphate in a hydrocarbon dilutent for the extraction of uranium from more feed slurries. Operability had been satisfactorily demonstrated in jet mixing columns at the pilot plant of the Mallinckrodt Chemical Works. [From Abstract]

"In the past ten years quantities of alpha-, beta-, gamma- and neutron-emitting isotopes handled in enclosures have increased from microcuries to kilocuries. Contaminated-atmosphere problems have increased accordingly. Developments at Berkeley are reviewed with particular emphasis on recent equipment, viz: a multiple-purpose gas scrubber and a total-capture system for slug-dissolver off gas."

Introduction: "The carrier (pyroelectric) concentration method is commonly used in the spectrographic analysis of plutonium metal. This report describes work which lead to substantial improvements in accuracy, precision and ease with which the analysis is made. Included are data from analyses of plutonium metal by the original and the improved carrier methods, and the cupferron extraction method."

Report presenting a spectrochemical method for analyzing the concentration of iron and silicon in uranium, which requires approximately 1/3 of the time required for the previously used "wet method."

Report describing alternative methods for depleting a large turnings inventory in a short period of time.

Report covering an experiment on a method for determining the crystallographic orientation within uranium rods. From summary: "The crystallographic orientation existing in rolled uranium rods may be determined by comparing the diffraction pattern obtained from an unknown specimen with the diffraction pattern obtained from a sample known to be randomly oriented."

The following document describes suggestions on the application of the A-48 ion accelerator beam currents to the Sherwood Program.

Abstract: A study has been made of the source, acceleration, and neutralization of ions for application to space propulsion. A summary is made in this paper of some of the most important problems in this area and their solutions.

Introduction: "During the last quarter, members of the Chemical Development Group have been concerned with six major projects. (1) thermal and radiation properties of organic materials as moderators and coolants, (2) thermal and radiation stability of mirconium hydride, (e) reactor accessibility (transport of radioactive materials in cooling systems, ................. There have been, in addition, a number of smaller service projects, mostly of an analytical nature.:

The following report follows a test with the purpose of determining the effect upon image fidelity by exposing a television camera to high intensity radiation over an extended period. Provided later in the report are notes on the design of the utiliscope camera used for these tests due to notable design features.

The purpose of this report is to present information on materials which can possibly be employed in the HF-H₂O-H₂SO₄-system in the extractive distillation process to be investigated at NBL.

"In order to determine the factors involved in the scale-up of cores with concentric inlet and outlet pipes, a 48 inch carbon steel flow model, geometrically similar to a 6 foot diameter core, has been assembled and tested...Visual studies were made of dye and gas behavior in the sphere, and quantitative measurements of point residence times were obtained through the use of conductivity cells actuating a Brush recorder. Static pressure drop across the core was measured."

Thesis discussing the heats of reduction, oxidation potentials, and measurements of autoreduction and disproportionation for aqueous ions of americium.

Review of a study regarding a lid-tank shielding facility's properties, including fast-neutron and gamma dose rates and thermal-neutron fluxes, which were mapped in a symmetry plane. The removal cross section of gadolinium was determined through comparison with various other materials.

Abstract: A description is given of the design and operation of a windowed autoclave system employed in the study of corrosion by pressurized hot water. The device has been used to obtain time-lapse motion pictures of the swelling and rupture of deliberately defected zirconium-clad uranium specimens. A method is described by which corrosion rates were calculated from pressure and temperature measurements. A typical set of pictures taken during a test is presented, and corrosion rates are reported for uranium-0, 5, 10, 15, and 20 w/o zirconium alloys subjected subjected to 600 F water.

Purpose: "This test was conducted to gain information and experience in the handling of heavy aggregate concrete. The results from this test were to establish procedures for a subsequent program -- "Construction Test of High Density Concrete Shielding.""

There have been numerous independent suggestions to use high speed shocks to heat deuterium gas to thermonuclear temperature (E. Teller, R.R. Wilson, H. Grad, W. Marshall)², and extensive experimental work in this field is being carried on by, e.g., Kolb³, and S. Janes⁴. Our own work in this field has been directed towards a fundamental understanding of the strong shock process in the limit of no particle collision, to find out if within this limit the ion heating following the passage of the shock is large enough to give rise to a thermonuclear reaction.

A simple method of solving for the phase shifts of the pion-proton scattering is presented. The rapid solution afforded can be utilized, as the Ashkin diagrams have been employed, to give starting values to an electronic computer or alternatively to analyze with more ease the variation of the phase shifts as a function of the input data in terms of the coefficients of the angular distributions. A new plot of a function of the total cross section versus the pion energy is introduced. The nearly straight line resulting should help to evaluate the experimental data.

In certain phases uranium processing it is poss!ble for operating personnel to acquire internal deposits of uranium. This body burden can be acquired by injection, as in contamination of a wound, by ingestion, of by inhalation. In order to estimate internal exposures, some means of determining the location and extent of these internal deposits is essential.