This report covers an investigation made to develop a gasometric determination that can determine 1.2 x 10-(-5) g. of nitrite with a precision (99% limits) of +/- 8%, and discusses how this procedure works.

From introduction: "It is the purpose of this report to give two further methods of determining end point of pontentiometric titration, neither of which require the plotting of a graph."

Introduction: Static, total immersion corrosion tests were carried out at room temperatures with Carboloy grades 44-A, 78, 907, X-3119-A and X-3119-B in Redox process solutions (ANL, June 1, 1949 Flowsheet) 1AX, 1AF, and 1AS.

From statement of objectives: The purposes of the work described in this report are to provide data useful for designing and operating the dissolver solution clarification equipment to be installed in the Redox production plant.

Summary: "The low carbon 18-8 stainless steels containing approximately 1.7 per cent boron used for vertical safety rods at Hanford were found to be structurally stable in the temperature range 0-450 C. The addition of boron decreases the stability of this metastable austenitic alloy. Sufficient ferrite formation is induced by sub-zero temperature treatments to result in dimensional changes and a magnetic alloy. The difficulties encountered in machining this material are believed to be due primarily to segregation in the castings resulting in small areas of the hard intermetallic compound, FeB."

From introduction: This report summarizes a study of the composution and physical properties of a number of hydrocarbon diluents together with some generalizations regarding relations between [vapor pressure, density and viscosity] properties.

The following report describes the procedures developed for the x-ray photometric determination of uraniuim in metal oxides and sludge and compares results, precision, and length of time of analyses by the General Electric X-Ray Photometer with analyses by the present titration method.

The stability of fluorothene (polytrifluorochloroethylene, Kel-F) to gamma radiation has been investigated to estimate the probable life expectancy of fluorothene equipment exposed to Purex process solutions. Samples of fluorothene were exposed to total gamma radiation dosages up to 10 degree R. The results of these tests substantiate the findings reported by Sisman and Bopp in their compilation of data on the affects of radiation on plastics.

Large savings in waste storage space may be realized by lowering the pH at which TBP waste is stored. Additional savings in neutralizing chemicals and operating time would also increase the monetary gain from such a process change. However, before such a change could be made, the corrosive effect of TBP waste at a lower pH on the mild steel waste storage tanks had to be determined.

Temperature calculations have been made to aid in planning a production test for low level irradiation of the thin rectangular uranium wafers. These uranium wafers, under irradiation in the outer fringe sone, are expected to have a maximum temperature which is less than 10 C above the local water temperature.

Previously, W. S. Figg and T. W. Ambrose (HW-51767 Rev) have investigated the problem of flow decay following electrical power loss to the PRTR primary coolant pumps. However, since the time of their study many reactor piping changes have been made in the design; therefore, it has become advisable to re-examine the problem incorporating these changes.

In the last two or three years there has been a notable improvement in the knowledge and understanding of reactor lattice physics. During this interval, measurements of parameters have been improved and the methods of analysis have been greatly strengthened. It has become apparent that the classical ways for computing the lattice parameters are not sufficient. It is the purpose of this report to publish under one cover as much of the most recent information as possible.

Instrumentation shall be provided as shown on the attached drawing, SK-1-26835 for Confinement System Control. The Primary objective of the confinement system shall be to provide maximum possible confinement of contamination, consistent with building limitations, in the event of any contamination, consistent with building limitations, in the event of any credible reactor accident resulting from equipment failure or reactor mis operation.

The hazards associated with several possible mechanical failures were analyzed for the PRTR. The consequences of these failures were evaluated for inclusion in the Final Hazards Summary Report.

This specification is specifically designed for the procurement of Zircaloy tubing to be used in the of swaged, UO fuel elements, an, and the Pu fuel elements for the Plutonium Recycle Test Reactor. Requisition G-385923 contains the following information pertinent to this specification: 1. Dimensions and dimensional tolerance. 2. Source of zirconium sponge and conditions for us of Zircaloy scrap. 3. Inspection requirements. 4. Shipping instructions.

The Biology Operation, Hanford Laboratories, required plutonium dioxide particles in five different micron and sub-micron size ranges. These were to be supplied as a water suspension in small containers. It was necessary to design equipment, suitable for hood operation, which would give a satisfactory separation of these particles.

In the continuing search for better methods of effecting the secondary fusion welded closure in Alsi bonded aluminum clad uranium metal fuel element, an article on "The Twin-Argon Welding Process" by J. A. Donellon was recently found in the September 1954 issue if the British Welding Journal. From a review of the article, the process appeared to have enough possibilities to warrant exploring it. Communication were established with the General Electric Company, Ltd..

Investigation of aqueous and steam corrosion at elevated temperature has been carried on at Hanford for several tears. A number of reports have been published on various phases of the corrosion program but, except for monthly reports, little has been written on the progress of the Corrosion and Coatings Operation alloy development program. This interim report will outline the more important current phases of the aluminum alloy program.

At the present time, high-radioactivity-level wastes at Hanford are neutralized and stored as liquid in underground tanks lined with mild steel. This method of storage is relatively inexpensive and is satisfactory on a short-term basis. However, on a long term basis, liquid storage is less desirable than solid storage because of the greater mobility of the liquid. In addition, storage as aa solid would significantly reduce the volume of waste stored. Consequently, various research and development studies have been undertaken in an attempt to develop a practical waste solidification.

The purpose of this document is to describe the design and construction of a full-scale, electrically-heated model of a 19-rod PRTR fuel element for use in heat transfer experiments.