In the separation of mixtures of radioactive iron and cobalt from neutron irradiated targets and in the removal of iron from cobalt targets for cyclotron production of radioiron, it is desirable to have a method superior to extraction from isopropyl ether in efficiency and ease of manipulation. Recent studies by Moore and Kraus on the separation of cobalt and nickel and on the behavior of iron in hydrochloric acid on Dowex-l resin in relation to the selective adsorption of chloride complexes of these elements have suggested the use of resin for the separation of iron and cobalt.

On January 12, 1953, an explosion occurred in the Savannah River pilot plant which has been used since November, 1951 by du Pont personnel to train operators and to test equipment for their new Purex production plant. The explosion occurred in an evaporator in which a uranyl nitrate solution containing some organics was being concentrated to a high degree to remove nitric acid. This memorandum reviews the facts surrounding the incident as obtained from the official Preliminary Technical Report'', and by talking to du Pont personnel. These facts are interpreted as fast as possible and the current design for the Hanford Purex production plant is re-evaluated in the light of these data.

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At the present time, production commitments require that each of the two dissolvers used at the Redox Plant be charged with 4.95 tons of irradiated metal every other day. After the aluminum jackets are removed from the slugs, the uranium is dissolved in three ``outs`` of 1.65 tons each. Because meteorological conditions often limit the time when the radioactive dissolver off gases may be emitted without contamination of the surrounding area, the dissolving requirements are frequently too great to maintain the required dissolver charging schedule. Unless the dissolving time cycles (or the meteorological limitations) can be reduced to assure that charging every other day can be maintained, phase 2 rates cannot be met even after activation of the third (spare) dissolver. As a means of reducing the dissolver time cycle and enabling the charging of each dissolver on alternate days throughout the year, a proposal was submitted that each dissolver charge be dissolved in two cuts of 2.475 tons each. This report presents the results of the plant test to determine the operational feasibility and relative merits of this proposal. Moreover, the information obtained may be used on a supplemental basis for the design of the Purex Plant dissolvers. 3 …

It is recommended that the Design Committee approve the installation of a refrigeration system in the 105-C gas circulation system for removal of moisture from the reactor following a process tube leak as was previously approved by the C-431 Project Committed. Engineering studies show that this refrigeration system is necessary to provide sufficient water removal capacity in order that the water absorbing capacity of the system furnished by the silica gel towers will not be a limit to the rate at which a reactor can be rehabilitated following a serious leak.

This is a listing of the classified periodic and series reports originated at the Hanford Atomic Products Operation for the period 1943 to June, 1953, and of similar reports received from the Hanford Operations Office. This listing also traces the continuity of reports that have undergone title changes during this period. This has been done by cross referencing to titles previously or subsequently used. The primary grouping of these reports is according to the intervals at which they were issued, e.g., weekly, monthly, annually, etc. Within each group, the reports are arranged alphabetically by title; for each individual title a note at the right hand margin gives the inclusive dates for the period during which reports of that title were issued. Those not shown with closing date are being issued currently. Specific document numbers for each title are found in the catalogs of the 700 Area and 300 Area Classified Files. The list is intended primarily to assist Classified Files in locating periodic reports requested by Plant personnel. However, it is also hoped that it may emphasize to authors the need for retaining an established title for a periodic report. Unnecessary changes of title every few months for the same …

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A project proposal is now under preparation for converting all areas to the alum and activated silica coagulation process, and modifying the present test installations to permanent facilities. The conversions will be designed to service increased water flows resulting from the reactor plant expansion program now under way. As an alternate to the installation of permanent facilities at the various areas, the possibility of hauling already prepared activated silica from those areas having excess capacity to those areas requiring large capital expenditures was suggested. The purpose of this study is to make an economic evaluation of the operating costs of hauling activated silica compared to the increased capital investment necessary to manufacture activated silica at various areas.

A scheme was proposed whereby the third and second uranium cycle salt wastes in the Redox plant are combined, stripped, evaporated, and then returned as scrub to the first (and possibly second) cycles as scrub, operating as a dual scrub column. It is the purpose of this report to study this proposed method of back-cycling, and to investigate other methods of reducing chemical and waste storage costs.