From introduction: "This report is concerned with exploratory experiments designed to studies the efficiency of a number of scavengers for zirconium and niobium adsorption and to provide preliminary information on the best conditions to employ on the most satisfactory of those scavengers studied, namely Super Filtrol FO. The data in this report include data obtained through October, 1949, and are by no means considered to be final. The investigation is currently being actively continued."

Objective: "The laboratory equilibrium study RC-E-1 described in this report was carried out to obtain uranium equilibrium curves at various concentrations of nitric acid and of TBP."

Abstract: "An experimental study was made to determine the effective shielding provided by a modern reinforced-concrete office building (AEC Headquarters building) from nuclear fallout. Pocket ionization chambers were used for measurement of the radiation-field strength. Fallout was simulated with distributed and point-source configurations of Co-60 and Ir-192 sources. Four typical sections were selected for study, and experiments were performed on each. These included an external wing with exposed basement walls and an external wing with a buried basement. Roof studies were made on an internal wing with a full basement and on the east end of wing A, which has a thin-roof construction. The thick-roof construction of 8 in. of concrete and 2 in. of rigid insulation covers all the building except the east end of wing A, which has 4 in. of concrete and 2 in. of insulation."

Technical report describing the Brookhaven National Laboratory nuclear reactor and the physical studies of heat transfer and efficiency conducted to improve nuclear reactor operations.

"This bibliography lists selected books, articles, and unclassified reports which have appeared in the following abstracts and indexes between August 1959 and December 1960."

"This bibliography is a compilation of titles to unclassified reports, journal articles and conference papers written by members of the University of California Radiation Laboratory, Livermore and Berkeley, relating to Project Sherwood (Controlled Thermonuclear Reactions) from 1953 through 1957."

"The laboratory experiments and field testing which were carried out in the development of a homogeneous gas labeling device are described. Detailed drawings of the injector and its most critical components are included. Recommendations are made for a production model of the device along with estimated costs of construction."

Abstract: "Steady states decomposition product partial pressures of water exposed to an epithermal neutron flux of about 2 x 10-11, at 235F, were 0.4 to 0.65 psi. Recombination studies were made by adding hydrogen and oxygen gases to water under irradiation at different temperature and flux levels. The data show a significant effect of temperature on the rate of pressure drop of the added hydrogen and oxygen. In operating at two flux levels, 1.2 x 10-11 and 2.0 x 10-11, no difference in the rate of pressure drop with flux could be detected with the instrumentation on the test apparatus."

Report discussing progress made in metallurgy by the Ames Laboratory during the the term from October 1, 1950 to March 31, 1951.

Report discussing the progress made on various chemistry research projects at Ames Laboratory during the period from October 1, 1950 to March 31, 1951.

Abstract: An analysis of the improved Model Number 350 Process Monitor was made so that it could be determined if this instrument would fulfill the need for gamma radiation detection instruments in the production buildings of Y-12. The results of these tests indicated the possibility of marked improvement in the monitor characteristics with minor redesigns. After these improvements have been made, this instrument will be a satisfactory monitor for this area.

Progress is reported on (1) direct cycle boiling reactor studies, (2) solvent extraction, (3) fluoride volatilization separation process, (4) elevated temperature separations, (5) fluidization studies, (6) development of analytical techniques, (7) processing and utilization of radioactive wastes.

The development of methods which were successful in producing zirconium Hanford type process tubing by roll forming and inert are welding (He) flat strip to which appropriate rails had ben previously attached by resistance welding is described in this report. Grade 2 drip arc melted crystal bar material was used.

A report about the start of preliminary measurements of the thermal conductivity of clad uranium and Zircaloy 2 prior to irradiation.

A report about elevated-temperature properties of dilute uranium-aluminum and uranium-zirconium alloys. Hot-hardness measurements show that small amounts of wither aluminum or zirconium increase the hardness of uranium at elevated temperatures.

The purpose of this report is to present the information obtained relative to the characteristic adsorption of radioisotopes in a long (forty feet) laboratory soil column treated with a high salt, process waste of high activity density. The movement of adsorbed cations in a soil column subjected to prolonged leeching by water also was determined.

Introduction: In conjunction with the final design and development of a 70 MW sodium intermediate heat exchanger and a sodium steam generator, an analysis is required which can be used as a basis for a determination to scale up or scale down the designs. Included in this analysis are those considerations leading to the recommendation of the best prototype test unit and to some of the limits imposed on scaling up or down when considering future applications of designs other than those actually tested. In addition, these considerations include aspects required to accurately predict the performance, operation, mechanical reliability, and feasibility of fabrication of the 70 MW design.

Abstract. The design, selection, and calculation of the Army Package Power Reactor shielding are described. The APPR-1, a prototype of a package reactor for remote locations, has a primary shield of iron and water. this shield has been adopted to permit fast erection and to provide low transported weight. economically, including transportation cost, the iron water shield is better than a lead water shield and is competitive with a concrete shield for a remote site. Because of the location at Fort Belvoir,Va., the shielding requirements for the APR-1 are considerably more stringent than those for a reactor at a remote base. Since the secondary shielding which surrounds the entire primary system must provide protection for personnel at any location outside the vapor container, concrete is provided for this need.

It has been found relatively easy to form uranium in the gamma phase temperature range by hot pressing, forging, or extrusion. The metal is quite plastic and flows readily to form a shape. Several temperatures from 800 degree C to 1000 degree C were investigated. No forming difficulties were experienced with the metal at the several temperatures concerned. The major difficulty in gamma phase hot pressing or extruding was associated with the tools. Metals or ceramics were not successful as tools for one or more reasons concerned with: lack of hot strength, reactions with the uranium, failure in thermal shock, and tendency to spall. Graphite was found to be the best material available, but it is not entirely satisfactory because of low strength. Uranium formed in the gamma phase possesses some refinement of grain structure as compared with as-cast metal; however, the grain size is quite large. No physical properties of the gamma phase formed metal were determined.

In HAPO solvent extraction processes there are two independent aspects of nitrous acid chemistry. One concern the decomposition of the solvent through nitration reactions and the attendant problems. These reactions are autocatalytic in the presence of nitric acid and have threshold values for both temperature and nitric acid concentration for a given solvent below which nitrous acid disappears and above which it is generated with continuous destruction of the solvent. These reactions are identical to those found in the prior study of the hexone system.

"This is the fourth Quarterly Report on Task II dealing with Methods Development for Radio-Tracing of Coal Product Hydrocarbons With Tritium. The problem of radio-chemical purity of traces is resolved by developing a new method of labeling with tritium that generates essentially no highly tagged side products or impurities."

Some numerical calculations have been done which permit the deduction of many properties of the synchrotron oscillation problem. For the presentation of the numerical results, it is useful to review the formulation framework to which the results are to be fitted. These are worked out for an arbitrary circular accelerator. The algebra woud have to be modified slightly to include straight sections but the numerical results are still useful.

A new gas-liquid countercurrent system (the ANCO system from Anisole-Complex) for the enrichment of boron isotopes has been developed. It is believed that use of this systems will result in a considerably lower unit cost for enriched boron-10 than was previously possible. The system utilizes the exchange reaction between BF3 (gas) and BF3·anisole (liquid) to concentrate boron-10 in the liquid phase. The single stage isotopic separation factor for this system has been found to vary from 1.039 at 0°C to 1.029 at 30°C. The isotopic exchange reaction has been shown to be rapid. Vapor pressures of the complex as a function of temperature have been measured and the heat of formation of the complex determined. Laboratory experiments show that quantitative removal of the BF3 from the complex can be accomplished by heating. A complete miniature ANCO plant was constructed and operated in the laboratory to test the feasibility of the system. The system was found to operate efficiently with a minimum of attention, and to enrich the isotopes of boron as expected. Based upon the experience obtained with the laboratory ANCO unit, a pilot plant large enough to utilize a 6-inch diameter exchange column was designed. The design calculations of …

Progress on projects on experimental physics, theoretical physics, MTA Target-Physics Program, accelerator construction and operation, chemistry, biology and medicine, plant and equipment.