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The Conversion of UF4 to U3Os (open access)

The Conversion of UF4 to U3Os

Methods of conversion of UF4 to U3O8 by fusion with ammonium oxalate dihydrate and other salts are described.
Date: May 28, 1941
Creator: Tevebaugh, A. D.; Tevebaugh, R. D.; Cline, W. D. & Warf, James C.
System: The UNT Digital Library
Slowing Down of Neutrons (open access)

Slowing Down of Neutrons

From introduction: "The Boltzmann equation expressing conversation of particles in phase space is set up."
Date: August 18, 1941
Creator: Breit, G.
System: The UNT Digital Library
The Production of Fluorocarbons by the Reaction of Fluorine With Silicone Carbide (open access)

The Production of Fluorocarbons by the Reaction of Fluorine With Silicone Carbide

This technical report details the production of fluorocarbon by reactions between fluorine and silicon carbide. The report contains two figures depicting aspects of the process.
Date: December 1941
Creator: Priest, Homer F. & Grosse, A. V.
System: The UNT Digital Library
Measurement of Density of Liquid UF6 (open access)

Measurement of Density of Liquid UF6

This report describes a method and apparatus used to determine the density of liquid sodium hexafluoride. The report includes a drawing of the density cell used in the experiment.
Date: March 29, 1942
Creator: Priest, Homer F.
System: The UNT Digital Library
The Preparation of Tungsten Hexafluoride (open access)

The Preparation of Tungsten Hexafluoride

From introductory paragraph: "Because of the possibility that tungsten hexafluoride might occur as an impurity in uranium hexafluoride it seemed worthwhile to prepare some of the material in order to become familiar with its mode of preparation, reactions, etc."
Date: June 1942
Creator: Priest, Homer F. & Colton, R.
System: The UNT Digital Library
Report on Determination of Densities of Several Uranium Compounds (open access)

Report on Determination of Densities of Several Uranium Compounds

This technical report details a process in order to determine the densities of several uranium compounds.
Date: August 10, 1942
Creator: Priest, Homer F. & Priest, G. L.
System: The UNT Digital Library
Viscosities and Densities of Fluorolube Oils (open access)

Viscosities and Densities of Fluorolube Oils

Abstract: Since the viscosity-temperature relationships of fluorocarbons are somewhat unusual, when compared to hydrocarbons, for example, it was decided to measure the viscosities, at several temperatures, of various fluorolube oils. The calculation of the viscosity of a blend of oils is at best an uncertain operation, varying considerably with the method used. A comparison of various methods was indicated, in order that reasonably accurate values might be assumed for theoretical composites. The densities were measured at corresponding temperatures for use in converting viscosities, and for their value, per se.
Date: April 28, 1943
Creator: Haendler, H. M.; Burger, L. L.; Sheldon, Z. D. & Barber, E. J.
System: The UNT Digital Library
A Colorimetric Method (open access)

A Colorimetric Method

From abstract: "This paper gives a method for determining Uranium using sodium cresotate as a colorimetric reagent. A precision is obtained of better than 2%. In carrying out analyses for Uranium in corrosion products by existing methods such as ignition to the oxide, silver reductor, or titration with ceric sulfate, it became apparent that a rapid, fairly accurate method for determining uranyl ion would be of great value. Such a method is described in this paper. The most logical color to use is that given by the ferrocyanide complex, but upon studying this, it proved to be unsatisfactory. Sodium salycilate also gives a color which has been used with some success, but its color appears to fade and is not very sensitive. A similar compound, sodium cresotate, was found to give an orange-red color and is the reagent used in the method to be described."
Date: June 30, 1943
Creator: Priest, H. F. & Priest, G. I.
System: The UNT Digital Library
Capture Cross Section of Pb208 for C Neutrons (open access)

Capture Cross Section of Pb208 for C Neutrons

From abstract: "Using the method of induced radioactivity, the capture cross section of Pb[^]208 for C neutrons is found to be .00045 ± .00015 x 10[^]-24 cm[^]2. This is definitely lower than the value of .001 x 10[^]-24 reported by Maurer and Ramm."
Date: November 5, 1943
Creator: Levinger, Joseph S., 1921-; Compton, A. H.; Allison, Samuel King, 1900-1965; Watson, W. W. & Snell, A. H.
System: The UNT Digital Library
Report No. EC-2, Dated from March 24, 1943 to November 5, 1943, Contained in the Engineer's Log Book (open access)

Report No. EC-2, Dated from March 24, 1943 to November 5, 1943, Contained in the Engineer's Log Book

This technical report consists of day by day experimental data reported in Engineer's Log book, Electro-Chemistry Department, supporting Report No. EC-11 dated November 15, 1944, by W. L. Grube, Research Laboratories Division, General Motors Corporation.
Date: November 6, 1943
Creator: Grube, William L.
System: The UNT Digital Library
Report on Methods of Preparation of Inorganic Fluorides (open access)

Report on Methods of Preparation of Inorganic Fluorides

From abstract: "Frequently it has been desirable to prepare pure anhydrous metal fluorides. Several general methods have proved satisfactory depending on the type of fluoride to be prepared."
Date: November 11, 1943
Creator: Priest, H. F.
System: The UNT Digital Library
Physical Properties of Uranyl Sulfate Solutions (open access)

Physical Properties of Uranyl Sulfate Solutions

Abstract: Measurements are reported of the solubility of uranyl sulfate in water at several temperatures, of the density of uranyl sulfate solutions as a function of concentration, of the variation of density of uranyl sulfate solutions of three different concentrations over a temperature range from 0[degree]C. to about 93[degree]C., and of the pH of uranyl sulfate solutions as a function of concentration as well as of temperature. The pH measurements were taken on uranyl sulfate samples prepared in several different ways and some conclusions are drawn as to the purity of theses samples.
Date: December 15, 1943
Creator: Helmholz, Lindsay. & Friedlander, G.
System: The UNT Digital Library
Report No. EC-3, dated from November 6, 1943 to December 31, 1943 Contained in Engineer's Log Book (open access)

Report No. EC-3, dated from November 6, 1943 to December 31, 1943 Contained in Engineer's Log Book

This technical report contains day by day experimental data reported in Engineer's Log Book, Electro-Chemistry Department, supporting Report No. EC-11 dated November 15, 1944, by W. L. Grube, Research Laboratories Division, General Motors Corporation.
Date: January 3, 1944
Creator: Grube, William L.
System: The UNT Digital Library
The Statistics of the Hypocritical Water Boiler (open access)

The Statistics of the Hypocritical Water Boiler

From introductory paragraph: "In a slightly hypocritical water boiler the introduction of a single neutron may give rise to a fairly large burst of neutrons which dies out slowly. As was shown some time ago by Frankel and Nelson with the help of A. Horn the statistics of this multiplication process can be treated in a simple way for the hypothetical case that the number of neutrons produced per fission is two."
Date: January 8, 1944
Creator: Frankel, S. P.
System: The UNT Digital Library
Capture of Fast Neutrons by Pb208 (open access)

Capture of Fast Neutrons by Pb208

From abstract: "Comparison of the activity produced by fast neutrons on lead with other activations corroborates the assignment of the 3.2 hr. activity as Pb209, and the assignment of the reaction as capture of fast neutrons. Two different measurements show that the neutrons captured have energies greater than 100 KEV. This average capture cross section for primary neutrons from 7.5 MEV deuterons on a thick target of beryllium is measured as 10[^]-27 ca[^]2."
Date: April 17, 1944
Creator: Levinger, Joseph S., 1921-; Compton, A. H.; Allison, Samuel King, 1900-1965; Watson, W. W. & Snell, A. H.
System: The UNT Digital Library
Test Results on Clinton Alpha Amplifier Used with an Offner Columbia Scaler (open access)

Test Results on Clinton Alpha Amplifier Used with an Offner Columbia Scaler

Technical report describing development of the Clinton alpha amplifier. The circuit for the Clinton alpha amplifier which is used with an Offner scaler is shown attached to the report. It consists of a pre-amplifier mounted in a cylindrical alpha chamber, followed by a three state amplifier and a pulse height selector in a separate cabinet. Pulses are fed from the pulse height selector in the amplifier to the input tube of the Offner scaler. Through the third stage of the amplifier, this circuit is exactly the same as the California circuit now used by the chemical section for alpha counting. A type 961 Offner scaler was used for these tests. None of the latest Offner scalers type961A, were available to us when the tests were made. Method of testing is given, results are tabulated, computations are made, and eight graphs are given. it appears that the Clinton amplifiers used with a Offner scaler will give substantially the same performance as that given by the California circuit.
Date: July 1, 1944
Creator: Ostdahl, H. E.
System: The UNT Digital Library
Identification and Crystal Structure of Barium Hydrogen Phosphate (open access)

Identification and Crystal Structure of Barium Hydrogen Phosphate

From abstract: "The report describes the complete structure of barium hydrogen phosphate, Ba HPO4, as determined by means of x-ray diffraction. The crystal is orthorhombic, with cell dimensions given by a=5.71 A b=7.05 A c=4.61 A. The calculated density is 4.15gm/cm[^]3 for two molecules in the unit cell. The space group is C[subscript]2v[superscript]7-pmn. The barium, phosphorus, and two sets of oxygen lie in the plane of symmetry. The third set of oxygens are in general positions. Parameters for these atoms have been found, and interatomic distances calculated. The positions of the hydrogens are indicated by the characteristics O-H-O distance (2.58A) between two oxygens."
Date: August 8, 1944
Creator: Mooney, Rose C. L.; Compton, A. H.; Allison, Samuel King, 1900-1965; Stearns, J. C. & Zachariasen, William H. (William Houlder), 1906-1979
System: The UNT Digital Library
Test Results on Bias Setting for the Chicago Scaler Offner Models (open access)

Test Results on Bias Setting for the Chicago Scaler Offner Models

Abstract: The counting accuracy of the Chicago Scalers, Models 961A and 961B, is a function of the bias setting of the limiter (V2). this report gives quantitative data supporting this thesis. A method of making bias settings is suggested. These tests were run at the suggestion of Mr. V. C. Hanson.
Date: September 11, 1944
Creator: Bradley, Wendell H.; Epstein, Bernard. & Wakefield, Ernest
System: The UNT Digital Library
The Thermal Conductivity of Liquid UF6 (open access)

The Thermal Conductivity of Liquid UF6

From introduction: "The measurement of the thermal conductivity of liquid TF6 presented unusual difficulties because of two of its properties which necessitated working with a closed system. The properties were (1) the liquid can exist as such only above 64.05°C. at which temperature its saturated vapor pressure is 1140 mm. of mercury, and (2) the compound reacts rapidly with moist air. Also because of the liquid's extremely corrosive nature, it was necessary to design a cell of special corrosion resistant materials."
Date: October 11, 1944
Creator: Priest, Homer F.
System: The UNT Digital Library
Manufacturing Specifications for the Higinbotham Scaler (open access)

Manufacturing Specifications for the Higinbotham Scaler

Technical report which includes a description of scaling action in a Higinbotham circuit, of operation of the output circuit, of operation of the regulated high voltage supply. Acceptance and performance specifications are given. also included are cuts showing the bottom and top view of a scaler of this type. The scaling circuit diagram and major parts list is attached. To facilitate testing, the circuit of a satisfactory pulse generator is included together with a cathode - follower.
Date: November 9, 1944
Creator: Wakefield, Ernest
System: The UNT Digital Library
Accumulation and Distribution of Radioactive Strontium, Barium-Lanthanum, Fission Mixture and Sodium in Goldfish (open access)

Accumulation and Distribution of Radioactive Strontium, Barium-Lanthanum, Fission Mixture and Sodium in Goldfish

This report details an experiment undergone to determine the amount of radioactive strontium, barium-lanthanum, fission mixture, and sodium accumulated by and distributed within non-feeding goldfish. The report includes tables detailing the findings.
Date: February 15, 1945
Creator: Prosser, C. Ladd (Clifford Ladd), 1907-2002; Pervinsek, William; Arnold, Jane; Svihla, George & Tompkins, P. C.
System: The UNT Digital Library
The Crystal Structure of Ba3(PO4)2 and Sr3(PO4)2 (open access)

The Crystal Structure of Ba3(PO4)2 and Sr3(PO4)2

From introduction: "This article gives an account of the determination of the complete crystal structures of the normal orthophosphates of barium and strontium."
Date: April 10, 1945
Creator: Zachariasen, William H. (William Houlder), 1906-1979
System: The UNT Digital Library
Range of U235 Fission Fragments in Photographic Emulsion (open access)

Range of U235 Fission Fragments in Photographic Emulsion

From abstract: "A fine-grain emulsion has been found which is sensitive only to the densely ionizing fission fragments. This emulsion was soaked in uranyl acetate and exposed to slow neutrons. The ranges in the emulsion of about four-hundred fission fragments were measured. The resulting distribution shows a sharp maximum at 23 microns of emulsion. No ternary fissions or large-angle scattering of fragments were observed."
Date: October 17, 1945
Creator: Richards, H. T.
System: The UNT Digital Library
Mass Spectrographic Analysis of Solids (open access)

Mass Spectrographic Analysis of Solids

Technical report regarding he purpose of the investigation was to evaluate the Chicago mass spectrograph as an analytical instrument for solids.
Date: November 15, 1945
Creator: Garrison, Warren Manford, 1915-
System: The UNT Digital Library