Calculation of Stagewise Contacting Systems (open access)

Calculation of Stagewise Contacting Systems

From abstract: General expressions relating product stream compositions to the operating conditions of countercurrent stagewise extraction columns are derived by an inductive method, and the conversion of the general equations to ones involving the particular case of constant extraction factor is demonstrated. For comparison, the derivation of simple column equations by the use of finite difference equations is included.
Date: May 22, 1953
Creator: Bloom, J. L. & Auer, P. L.
System: The UNT Digital Library
The Determination of Adsorbed Moisture on Uranium and Uranium Oxide: A New Method for Moisture Determinations (open access)

The Determination of Adsorbed Moisture on Uranium and Uranium Oxide: A New Method for Moisture Determinations

Abstract: "A method is described for determining moisture on uranium and uranium oxides. This method should also be applicable to solid samples which, when heated, do not decompose to form water or liberate a substance which will react with Fischer's reagent. The method should be especially applicable to samples which are insoluble in alcohol or Karl Fischer reagent under normal titration conditions, or which will themselves react with the reagent. The amount of moisture on uranium and uranium oxide was found to be 0.02% except when the oxide was found to be 0.02% except when the oxide source was uranyl sulfate. In this case, the moisture content was found to be 0.1%. Modifications of the procedure and apparatus are presented for improving the accuracy and shortening the time necessary for the determination."
Date: April 22, 1953
Creator: Hibbits, James O. & Zucker, Donald
System: The UNT Digital Library
The Chemistry of Uranium(VI) Orthophosphate Solutions (open access)

The Chemistry of Uranium(VI) Orthophosphate Solutions

From introduction: This is the first in a series of reports describing an investigation of the chemistry of uranium(VI) orthophosphate solutions which is at present underway in this laboratory. Spectrophotometric, potentiometric and solubility studies have been carried out, and it is the first of these which is reported here.
Date: June 22, 1953
Creator: Baes, Charles F., Jr.; Schreyer, J. M. & Lesser, J. M.
System: The UNT Digital Library
A correlation of the magnetic susceptibilities of thorium, uranium, and plutonium with crystal structure (open access)

A correlation of the magnetic susceptibilities of thorium, uranium, and plutonium with crystal structure

Report describing potential correlations of magnetic susceptibilities of the elements thorium, uranium, and plutonium with their crystal structures.
Date: July 22, 1953
Creator: Comstock, A. Allen
System: The UNT Digital Library
Influence of Absorption on the Effective Value of Eta (open access)

Influence of Absorption on the Effective Value of Eta

This report follows calculations performed to determine the effect of epithermal capture on the value of eta to be used in lattice calculations.
Date: January 22, 1953
Creator: Cohen, E. Richard, 1922-
System: The UNT Digital Library
Decontamination of Portable Instruments (open access)

Decontamination of Portable Instruments

The decontamination of portable instruments by the Calibration Unit has presented a problem for some time. Most of the contamination is in the 100 to 500 c/m or 500 to 2000 d/m range. Higher levels of contamination can usually be reduced to these levels, but further cleaning proves quite difficult
Date: May 22, 1953
Creator: Unruh, C. M.
System: The UNT Digital Library
Wet Fluoride Studies:  Calcium Plutonium (IV) Fluoride (open access)

Wet Fluoride Studies: Calcium Plutonium (IV) Fluoride

Laboratory studies have shown that the double salt, CaF2-PuF4, can be precipitated by rapid addition of hydro-fluoric acid to solutions containing 25 to 75 g Pu/1, caleium equimolar to plutonium, and 1 to 10 M HNO3. The precipitate, which is subsequently washed with water and dried to 300 degrees C in dehumidified, deoxygenated argon, can be reduced thermally by calcium to give high yields of plutonium metal.
Date: December 22, 1953
Creator: Branin, P. B.
System: The UNT Digital Library