Method of Electrode Fabrication and an Electrode for Metal Chloride Battery (open access)

Method of Electrode Fabrication and an Electrode for Metal Chloride Battery

A method of fabricating an electrode for use in a metal chloride battery and an electrode are provided. The electrode has relatively larger and more uniform pores than those found in typical electrodes. The fabrication method includes the steps of mixing sodium chloride particles selected from a predetermined size range with metal particles selected from a predetermined size range, and then rigidifying the mixture. The electrode exhibits lower resistivity values of approximately 0.5 {Omega}cm{sup 2} than those resistivity values of approximately 1.0--1.5 {Omega}cm{sup 2} exhibited by currently available electrodes.
Date: October 9, 1990
Creator: Bloom, Ira D.; Nelson, Paul A. & Vissers, Donald R.
System: The UNT Digital Library
Halogenated high {Tc} superconductors and method of preparation (open access)

Halogenated high {Tc} superconductors and method of preparation

Disclosed is a method for producing a superconductor of the R-Ba-Cu-O system which comprises of selecting an insulating material of the formula RBa{sub x}Cu{sub y}O{sub z} where R is selected from the group consisting of Y, La, Pr, Nd, Sm, Eu, Gd, Ho, Er, Tm, and Lu, and where x ranges from about 1.7 to about 2.3, y ranges from about 2.7 to about 3.3 and z ranges from about 5.0 to about 6.99, and halogenating said material with a halogen selected from the group consisting of chlorine, bromine, iodine, and mixtures thereof, while maintaining said material at a temperature ranging from about 160 to about 440{degrees}C, for a period of time sufficient to cause incorporation of said halogen into said material. Also, disclosed are the materials produced by the method and articles of manufacture incorporating said materials as electronic circuitry components.
Date: November 14, 1990
Creator: Radousky, H. B.; Glass, R. S. & Fluss, M. J.
System: The UNT Digital Library
A method of genetically engineering acidophilic, heterotrophic, bacteria by electroporation and conjugation (open access)

A method of genetically engineering acidophilic, heterotrophic, bacteria by electroporation and conjugation

A method of genetically manipulating an acidophilic bacteria is provided by two different procedures. Using electroporation, chimeric and broad-host range plasmids are introduced into Acidiphilium. Conjugation is also employed to introduce broad-host range plasmids into Acidiphilium at neutral pH.
Date: August 7, 1990
Creator: Roberto, F. F.; Glenn, A. W. & Ward, T. E.
System: The UNT Digital Library
Process for fabrication of metal oxide films (open access)

Process for fabrication of metal oxide films

This invention is comprised of a method of fabricating metal oxide films from a plurality of reactants by inducing a reaction by plasma deposition among the reactants. The plasma reaction is effective for consolidating the reactants and producing thin films of metal oxides, e.g. electro-optically active transition metal oxides, at a high deposition rate. The presence of hydrogen during the plasma reaction enhances the deposition rate of the metal oxide. Various types of metal oxide films can be produced.
Date: July 17, 1990
Creator: Tracy, C. E.; Benson, D. & Svensson, S.
System: The UNT Digital Library
Method for preparing homogeneous single crystal ternary III-V alloys (open access)

Method for preparing homogeneous single crystal ternary III-V alloys

A method for producing homogenous single crystal III--V ternary alloys of high crystal perfection using a floating crucible system in which the outer crucible holds a ternary alloy of the composition desired to be produced in the crystal and an inner floating crucible having a narrow, melt-passing channel in its bottom wall holds a small quantity of melt of a pseudo-binary liquidus composition which would freeze into the desired crystal composition. The alloy of the floating crucible is maintained at a predetermined lower temperature than the alloy of the outer crucible, and a single crystal of the desired homogeneous alloy is pulled out of the floating crucible melt, as melt from the outer crucible flows into a bottom channel of the floating crucible at a rate that corresponds to the rate of growth of the crystal.
Date: August 14, 1990
Creator: Ciszek, T. F.
System: The UNT Digital Library
Highly conductive electrolyte composites and method of fabrication thereof (open access)

Highly conductive electrolyte composites and method of fabrication thereof

An electrolyte composite is manufactured by pressurizing a mixture of ionically conductive glass and an ionically conductive compound at between 12,000 and 24,000 pounds per square inch to produce a pellet. The resulting pellet is then sintered at relatively lower temperatures (800{degrees}C--1200{degrees}C), for example 1000{degrees}C, than are typically required (1400{degrees}C) when fabricating single constituent ceramic electrolytes. The resultant composite is 100 percent conductive at 250{degrees}C with conductivity values of 2.5 to 4 {times} 10{sup {minus}2} (ohm-cm){sup {minus}1}. The matrix exhibits chemical stability against sodium for 100 hours at 250 to 300{degrees}C.
Date: July 17, 1990
Creator: Hash, M. C. & Bloom, I. D.
System: The UNT Digital Library
Solid-state NMR imaging system (open access)

Solid-state NMR imaging system

An accessory for use with a solid-state NMR spectrometer includes a special imaging probe with linear, high-field strength gradient fields and high-power broadband RF coils using a back projection method for data acquisition and image reconstruction, and a real-time pulse programmer adaptable for use by a conventional computer for complex high speed pulse sequences.
Date: December 31, 1990
Creator: Gopalsami, N.; Dieckman, S. L. & Ellingson, W. A.
System: The UNT Digital Library
Selective epitaxy using the GILD process (open access)

Selective epitaxy using the GILD process

The present invention comprises a method of selective epitaxy on a semiconductor substrate. The present invention provides a method of selectively forming high quality, thin GeSi layers in a silicon circuit, and a method for fabricating smaller semiconductor chips with a greater yield (more error free chips) at a lower cost. The method comprises forming an upper layer over a substrate, and depositing a reflectivity mask which is then removed over selected sections. Using a laser to melt the unmasked sections of the upper layer, the semiconductor material in the upper layer is heated and diffused into the substrate semiconductor material. By varying the amount of laser radiation, the epitaxial layer is formed to a controlled depth which may be very thin. When cooled, a single crystal epitaxial layer is formed over the patterned substrate. The present invention provides the ability to selectively grow layers of mixed semiconductors over patterned substrates such as a layer of Ge{sub x}Si{sub 1-x} grown over silicon. Such a process may be used to manufacture small transistors that have a narrow base, heavy doping, and high gain. The narrowness allows a faster transistor, and the heavy doping reduces the resistance of the narrow layer. The …
Date: December 31, 1990
Creator: Weiner, K. H.
System: The UNT Digital Library
High density hexagonal boron nitride prepared by hot isostatic pressing in refractory metal containers (open access)

High density hexagonal boron nitride prepared by hot isostatic pressing in refractory metal containers

Boron nitride powder with less than or equal to the oxygen content of starting powder (down to 0.5% or less) is hot isostatically pressed in a refractory metal container to produce hexagonal boron nitride with a bulk density greater than 2.0 g/cc. The refractory metal container is formed of tantalum, niobium, tungsten, molybdenum or alloys thereof in the form of a cansister or alternatively plasma sprayed or chemical vapor deposited onto a powder compact. Hot isostatic pressing at 1800{degrees}C and 30 KSI (206.8 MPa) argon pressure for four hours produces a bulk density of 2.21 g/cc. Complex shapes can be made.
Date: December 31, 1990
Creator: Hoenig, C. L.
System: The UNT Digital Library
Ductile nickel-silicon alloy (open access)

Ductile nickel-silicon alloy

An improvement over prior compositions wherein the ductility of Ni-Si alloys are improved with minor alloying additions of hafnium or zirconium.
Date: August 6, 1990
Creator: Oliver, W. C.
System: The UNT Digital Library
Improved thermal storage module for solar dynamic receivers (open access)

Improved thermal storage module for solar dynamic receivers

This invention relates to a thermal storage apparatus and more particularly to an apparatus for use in conjunction with solar dynamic energy storage systems. The invention is comprised of a thermal energy storage system comprising a germanium phase change material and a graphite container.
Date: December 31, 1990
Creator: Beatty, R. L. & Lauf, R. J.
System: The UNT Digital Library
Process of converting starch to glucose and glucose to lactic acid (open access)

Process of converting starch to glucose and glucose to lactic acid

This document describes a method for converting starch into lactic acid of sufficient purity for use as a substrate for biodegradable plastics. The process is designed to work on industrial food waste streams such as potato wastes or cheese whey permeate. For potato waste, {alpha}-amylase and calcium chloride are added to the starch containing waste and incubated at a pH of 4--7, a temperature of 90--130{degree}C, and a pressure above 15 psi for not less than 15 minutes. At this point, glucoamylase is added and the mixture is incubated at a temperature of 50--70{degree}C and a pH below 6.5 for 4 hours. This results in the conversion of more than 90% of the starch into glucose, which is substantially free of microbial contamination. The hydrolysate is filtered, and introduced with additional nutrients to a fermentor containing a lactose producing microorganism to form a fermentation broth. This results in the fermentation of glucose to lactose, which is filtered and subjected to electrodialysis for purification. Conversion of glucose to lactic acid or lactate occurs with an efficiency of over 95%. 1 fig. (MHB)
Date: January 1, 1990
Creator: Tsai, TenLin; Sanville, Cynthia Y.; Coleman, Robert D. & Schertz, William W.
System: The UNT Digital Library
A unique system of Fe/Pd for magneto-optical recording and magnetic switching devices (open access)

A unique system of Fe/Pd for magneto-optical recording and magnetic switching devices

This invention is comprised of a high density magneto-optical information storage medium utilizing the properties of an ultrathin iron film on a palladium substrate. The present invention comprises a magneto-optical medium capable of thermal and magnetic stability and capable of possessing a vertical orientation of the magnetization vector for the magnetic material. Data storage relies on the temperature dependence of the coercivity of the ultrathin film. Data retrieval derives from the Kerr effect which describes the direction of rotation of a plane of polarized light traversing the ultrathin magnetic material as a function of the orientation of the magnetization vector.
Date: May 22, 1990
Creator: Liu, Chian Q. & Bader, S. D.
System: The UNT Digital Library
Method of separating organic contaminants from fluid feedstreams with polyphosphazene membranes (open access)

Method of separating organic contaminants from fluid feedstreams with polyphosphazene membranes

A method is provided for separating polar hydrocarbons from a fluid feedstream. The fluid feedstream is flowed across a first surface of a polyphosphazene semipermeable membrane. At least one polar hydrocarbon from the fluid feedstream permeates through the polyphosphazene semipermeable membrane to a second opposed surface of the semipermeable membrane. Then the permeated polar hydrocarbon is removed from the second opposed surface of the polyphosphazene semipermeable membrane. Outstanding and unexpected separation selectivities on the order of 10,000 were obtained for methylene chloride when a methylene chloride in water feedstream was flowed across the polyphosphazene semipermeable membrane in the invented method.
Date: December 31, 1990
Creator: McCaffrey, R. R. & Cummings, D. G.
System: The UNT Digital Library
Fiber optic detector (open access)

Fiber optic detector

This invention is comprised of a portable fiber optic detector that senses the presence of specific target chemicals by exchanging the target chemical for a fluorescently-tagged antigen that is bound to an antibody which is in turn attached to an optical fiber. Replacing the fluorescently-tagged antigen reduces the fluorescence so that a photon sensing detector records the reduced light level and activates an appropriate alarm or indicator.
Date: December 31, 1990
Creator: Partin, J. K.; Ward, T. E. & Grey, A. E.
System: The UNT Digital Library
Ammonia-treated phosphate glasses useful for sealing to metals (open access)

Ammonia-treated phosphate glasses useful for sealing to metals

A method of improving surface-dependent properties of phosphate glass such as durability and wear resistance without significantly affecting its thermal expansion coefficient is provided which comprises annealing the glass in a dry ammonia atmosphere at temperatures approximating the transition temperature of the glass. The ammonia annealing treatment of the present invention is carried out for a time sufficient to allow incorporation of a thin layer of nitrogen into the surface of the phosphate glass, and the treatment improves the durability of the glass without the reduction in the thermal expansion coefficient that has restricted the effectiveness of prior ammonia treatments. The improved phosphate glass resulting from this method is superior in wear resistance, yet maintains suitable thermal expansion properties so that it may be used effectively in a variety of applications requiring hermetic glass-metal seals.
Date: December 31, 1990
Creator: Brow, R. K. & Day, D. E.
System: The UNT Digital Library
Detection device for hazardous material (open access)

Detection device for hazardous material

This invention is comprised of a detection device that is activated by the interaction of a hazardous chemical with a coating interactive with said chemical on an optical fiber thereby reducing the amount of light passing through the fiber to a light detector. A combination of optical filters separates the light into a signal beam and a reference beam which after detection, appropriate amplification, and comparison with preset internal signals, activates an alarm means if a predetermined level of contaminant is observed.
Date: December 31, 1990
Creator: Partin, J. K. & Grey, A. E.
System: The UNT Digital Library
Counterrotating brushless dc permanent magnet motor (open access)

Counterrotating brushless dc permanent magnet motor

An brushless DC permanent magnet motor is provided for driving an autonomous underwater vehicle. In one embodiment, the motor comprises four substantially flat stators disposed in stacked relationship, with pairs of the stators being axially spaced and each of the stators comprising a tape-wound stator coil; and a first and second substantially flat rotors disposed between the spaced pairs of stators. Each of the rotors includes an annular array of permanent magnets embedded therein. A first shaft is connected to the first rotor and a second, concentric shaft is connected to the second rotor, and drive unit causes rotation of the two shafts in opposite directions. The second shaft comprises a hollow tube having a central bore therein in which the first shaft is disposed. Two different sets of bearings support the first and second shAfts. In another embodiment, the motor comprises two ironless stators and pairs and rotors mounted no opposite sides of the stators and driven by counterrotating shafts.
Date: December 31, 1990
Creator: Hawsey, R. A. & Bailey, J. M.
System: The UNT Digital Library
Improved catalysts and method (open access)

Improved catalysts and method

An improved catalyst and method for the oxyhydrochlorination of methane is disclosed. The catalyst includes a pyrogenic porous support on which is layered as active material, cobalt chloride in major proportion, and minor proportions of an alkali metal chloride and of a rare earth chloride. On contact of the catalyst with a gas flow of methane, HCl and oxygen, more than 60% of the methane is converted and of that converted more than 40% occurs as monochloromethane. Advantageously, the monochloromethane can be used to produce gasoline boiling range hydrocarbons with the recycle of HCl for further reaction. This catalyst is also of value for the production of formic acid as are analogous catalysts with lead, silver or nickel chlorides substituted for the cobalt chloride. 8 figs., 3 tabs.
Date: December 31, 1990
Creator: Taylor, C. E. & Noceti, R. P.
System: The UNT Digital Library
Real time Faraday spectrometer (open access)

Real time Faraday spectrometer

This invention is comprised of a charged particle spectrometer that contains a detection system which embodies the benefits of both foil-light emissions and faraday cups, yet it does not interfere with the particle beam. 5 Figs. (GHH)
Date: December 31, 1990
Creator: Smith, T. E. Jr.; Struve, K. W. & Colella, N. J.
System: The UNT Digital Library
A Stripline Fast Faraday Cup for measuring GHz structure of ion beams (open access)

A Stripline Fast Faraday Cup for measuring GHz structure of ion beams

The Stripline Fast Faraday Cup is a device which is used to quantitatively and qualitatively measure gigahertz time structure characteristics of ion beams with energies up to at least 30 Mev per nucleon. A stripline geometry is employed in conjunction with an electrostatic screen and a Faraday cup to provide for analysis of the structural characteristics of an ion beam. The stripline geometry allows for a large reduction in the size of the instrument while the electrostatic screen permits measurements of the properties associated with low speed ion beams.
Date: December 31, 1990
Creator: Bogaty, J. M.
System: The UNT Digital Library
A method and apparatus for continuous electrophoresis (open access)

A method and apparatus for continuous electrophoresis

A method and apparatus for conducting continuous separation of substances by electrophoresis are disclosed. The process involves electrophoretic separation combined with couette flow in a thin volume defined by opposing surfaces. By alternating the polarity of the applied potential and producing reciprocating short rotations of at least on of the surfaces relative to the other, small increments of separation accumulate to cause substantial, useful segregation of electrophoretically separable components in a continuous flow system.
Date: December 31, 1990
Creator: Watson, J. S.
System: The UNT Digital Library
Destruction of acid gas emissions (open access)

Destruction of acid gas emissions

A method of destroying NO{sub x} and SO{sub x} in a combustion gas is disclosed. The method includes generating active species by treating stable molecules in a high temperature plasma. Ammonia, methane, steam, hydrogen, nitrogen or a combustion of these gases can be selected as the stable molecules. The gases are subjected to plasma conditions sufficient to create free radicals, ions or excited atoms such as N, NH, NH{sub 2}, OH, CH and/or CH{sub 2}. These active species are injected into a combustion gas at a location of sufficiently high temperature to maintain the species in active state and permit them to react with NO{sub x} and SO{sub x}. Typically the injection is made into the immediate post-combustion gases at temperatures of 475--950{degrees}C. 1 fig.
Date: December 31, 1990
Creator: Mathur, M. P.; Fu, Yuan C.; Ekmann, J. M. & Boyle, J. M.
System: The UNT Digital Library
Wedge assembly for electrical transformer component spacing (open access)

Wedge assembly for electrical transformer component spacing

This invention is comprised of a wedge assembly that is easily inserted between two surface to be supported thereby, and thereafter expanded to produce a selected spacing between those surfaces. This wedge assembly has two outer members that are substantially identical except that they are mirror images of each other. Oppositely directed faces of these of these outer members are substantially parallel for the purpose of contacting the surfaces to be separated. The other faces of these outer members that are directed toward each other are tapered so as to contact a center member having complementary tapers on both faces. A washer member is provided to contact a common end of the outer members, and a bolt member penetrates this washer and is threadably received in a receptor of the center member. As the bolt member is threaded into the center member, the center member is drawn further into the gap between the outer members and thereby separates these outer members to contact the surfaces to be separated. In the preferred embodiment, the contacting surfaces of the outer member and the center member are provided with guide elements. The wedge assembly is described for use in separating the secondary windings …
Date: December 31, 1990
Creator: Baggett, F. E. & Cage, W. F.
System: The UNT Digital Library