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Apparatus for preparing a sample for mass spectrometry (open access)

Apparatus for preparing a sample for mass spectrometry

Disclosed is an apparatus for preparing a sample for analysis by a mass spectrometer system. The apparatus has an entry chamber and an ionization chamber separated by a skimmer. A capacitor having two space-apart electrodes followed by one or more ion-imaging lenses is disposed in the ionization chamber. The chamber is evacuated and the capacitor is charged. A valve injects a sample gas in the form of sample pulses into the entry chamber. The pulse is collimated by the skimmer and enters the ionization chamber. When the sample pulse passes through the gap between the electrodes, it discharges the capacitor and is thereby ionized. The ions are focused by the imaging lenses and enter the mass analyzer, where their mass and charge are analyzed.
Date: December 31, 1992
Creator: Villa-Aleman, E.
System: The UNT Digital Library
Photoconversion of organic materials into single-cell protein (open access)

Photoconversion of organic materials into single-cell protein

A process is described for converting organic materials (such as biomass wastes) into sterile, high-grade bacterial protein suitable for use an animal feed or human food supplements. In a preferred embodiment the process involves thermally gasifying the organic material into primarily carbon monoxide, hydrogen and nitrogen products, followed by photosynthetic bacterial assimilation of the gases into cell material, which can be high as 65% protein. The process is ideally suited for waste recycling and for food production under zero-gravity or extra-terrestrial conditions.
Date: December 31, 1991
Creator: Weaver, P. F.
System: The UNT Digital Library
An apparatus for remotely handling components (open access)

An apparatus for remotely handling components

The inventive apparatus for remotely handling barlike components which define a longitudinal direction includes a gripper mechanism for gripping the component including first and second gripper members longitudinally fixedly spaced from each other and oriented parallel to each other in planes transverse to the longitudinal direction. Each gripper member includes a jaw having at least one V-groove with opposing surfaces intersecting at a base and extending radially relative to the longitudinal direction for receiving the component in an open end between the opposing surfaces. The V-grooves on the jaw plate of t he first and second gripper members are aligned in the longitudinal direction to support the component in the first and second gripper members. A jaw is rotatably mounted on and a part of each of the first and second gripper members for selectively assuming a retracted mode in which the open end of the V-groove is unobstructed and active mode in which the jaw spans the open end of the V-groove in the first and second gripper members. The jaw has a locking surface for contacting the component in the active mode to secure the component between the locking surface of the jaw and the opposing surfaces of …
Date: December 31, 1992
Creator: Szkrybalo, G. A. & Griffin, D. L.
System: The UNT Digital Library
Monitoring and analyzing waste glass compositions (open access)

Monitoring and analyzing waste glass compositions

None
Date: December 31, 1992
Creator: Schumacher, R. F.
System: The UNT Digital Library
High adherence copper plating process (open access)

High adherence copper plating process

A process is described for applying copper to a substrate of aluminum or steel by electrodeposition and for preparing an aluminum or steel substrate for electrodeposition of copper. Practice of the invention provides good adhesion of the copper layer to the substrate.
Date: December 31, 1992
Creator: Mignardot, H.
System: The UNT Digital Library
Improved morphology in electrochemically grown conducting polymer films (open access)

Improved morphology in electrochemically grown conducting polymer films

A conducting polymer film with an improved space filling is formed on a metal electrode surface. A self-assembling monolayer is formed directly on the metal surface where the monolayer has a first functional group that binds to the metal surface and a second chemical group that forms a chemical bonding site for molecules forming the conducting polymer. The conducting polymer is then conventionally deposited by electrochemical deposition. In one example, a conducting film of polyaniline is formed on a gold electrode surface with an intermediate monolayer of p-aminothiophenol.
Date: December 31, 1990
Creator: Rubinstein, I.; Gottesfeld, S. & Sabatani, E.
System: The UNT Digital Library
Magnetic levitation configuration incorporating levitation, guidance and linear synchronous motor (open access)

Magnetic levitation configuration incorporating levitation, guidance and linear synchronous motor

A propulsion and suspension system for an inductive repulsion type magnetically levitated vehicle which is propelled and suspended by a system which includes propulsion windings which form a linear synchronous motor and conductive guideways, adjacent to the propulsion windings, where both combine to partially encircling the vehicle-borne superconducting magnets. A three phase power source is used with the linear synchronous motor to produce a traveling magnetic wave which in conjunction with the magnets propel the vehicle. The conductive guideway combines with the superconducting magnets to provide for vehicle leviation.
Date: December 31, 1992
Creator: Coffey, H. T.
System: The UNT Digital Library
A sequencing and fan-out mechanism for dataflow computing (open access)

A sequencing and fan-out mechanism for dataflow computing

A sequencing and data fanout mechanism is provided for a dataflow processor is activated by an input token which causes a sequence of operations to occur by initiating a first instruction to act on data contained within the token and then executing a sequential thread of instructions identified by either a repeat count and an offset within the token, or by an offset within each preceding instruction.
Date: December 31, 1991
Creator: Grafe, Victor G. & Hoch, James E.
System: The UNT Digital Library
Stabilized fuel with silica support structure (open access)

Stabilized fuel with silica support structure

This report describes a stabilized fuel which is supported by a silica support structure. The silica support structure provides a low density, high porosity vehicle for safely carrying hydrocarbon fuels. The silica support structure for hydrocarbon fuel does not produce toxic material residues on combustion which would pose environmentally sensitive disposal problems. The silica stabilized fuel composition is useful as a low temperature, continuous burning fire starter for wood or charcoal.
Date: December 31, 1991
Creator: Poco, J. F. & Hrubesh, L. W.
System: The UNT Digital Library
A method of noncontacting ultrasonic process monitoring (open access)

A method of noncontacting ultrasonic process monitoring

A method of monitoring a material during processing comprising the steps of (a) shining a detection light on the surface of a material; (b) generating ultrasonic waves at the surface of the material to cause a change in frequency of the detection light; (c) detecting a change in the frequency of the detection light at the surface of the material; (d) detecting said ultrasonic waves at the surface point of detection of the material; (e) measuring a change in the time elapsed from generating the ultrasonic waves at the surface of the material and return to the surface point of detection of the material, to determine the transit time; and (f) comparing the transit time to predetermined values to determine properties such as, density and the elastic quality of the material.
Date: December 31, 1991
Creator: Garcia, G. V.; Walter, J. B. & Telschow, K. L.
System: The UNT Digital Library
Semiconductor diode laser having an intracavity spatial phase controller for beam control and switching (open access)

Semiconductor diode laser having an intracavity spatial phase controller for beam control and switching

A high-power broad-area semiconductor laser having a intracavity spatial phase controller is disclosed. The integrated intracavity spatial phase controller is easily formed by patterning an electrical contact metallization layer when fabricating the semiconductor laser. This spatial phase controller changes the normally broad far-field emission bean, of such a laser into a single-lobed near-diffraction-limited beam at pulsed output powers of over 400 mW. Two operating modes, a thermal and a gain operating mode, exist for the phase controller, allowing for steering and switching the beam as the modes of operation are switched, and the emission beam may be scanned, for example, over a range of 1.4 degrees or switched by 8 degrees. More than one spatial phase controller may be integrated into the laser structure.
Date: December 31, 1992
Creator: Hohimer, J. P.
System: The UNT Digital Library
A method for the thermal characterization, visualization, and integrity evaluation of conducting material samples or complex structures (open access)

A method for the thermal characterization, visualization, and integrity evaluation of conducting material samples or complex structures

This invention is useful in thermal imaging of conducting materials, and is particularly useful in measuring thermal conductivity and thermal boundary conditions in composite anisotropic materials, in materials of irregular shape, and in materials for high-temperature applications. It also has utility in visualizing the integrity of complex structures such as a machine, power plant, or chemical plant. The method is for modeling a conducting material sample or structure (system) as an electrical network of resistances, for measuring electric resistance between selected leads attached to the surface of the system, and, using basic circuit theory, for translating measured resistances into temperatures or indications of integrity in corresponding regions of the system. 10 figs.
Date: December 31, 1991
Creator: Ortiz, M. G.
System: The UNT Digital Library
Microwave sintering of multiple aritcles (open access)

Microwave sintering of multiple aritcles

Disclosed are apparatus and method for producing articles of alumina and of alumina and silicon carbide in which the articles are sintered at high temperatures using microwave radiation. The articles are placed in a sintering container which is placed in a microwave cavity for heating. The rates at which heating and cooling take place is controlled.
Date: December 31, 1992
Creator: Blake, R. D. & Katz, J. D.
System: The UNT Digital Library
Ceramic tamper-revealing seals (open access)

Ceramic tamper-revealing seals

A tamper resistant seal is made of a brittle material with internal defects internally arranged in a random pattern to form a unique fingerprint characteristic of the seal which may be identified by ultrasonic scanning to determine whether tampering has occurred. It comprises a flexible metal or ceramic cable with composite ceramic ends or a U-shaped ceramic connecting element attached to a binding element plate or block cast from alumina or Zr, and connected to the connecting element by shrink fitting. Part of the binding element is cast with NiO{sub 2} particles, which allows ultrasonic scanning and the resulting fingerprint. 7 figs.
Date: December 31, 1991
Creator: Kupperman, D. S.; Raptis, A. C. & Sheen, Shuh-Haw
System: The UNT Digital Library
Compact self-contained electrical-to-optical converter/transmitter (open access)

Compact self-contained electrical-to-optical converter/transmitter

An electrical-to-optical converter/transmitter is disclosed. A first optical receiver and a second optical receiver are provided for receiving a calibrate command and a power switching signal, respectively, from a remote processor. A third receiver is provided for receiving an analog electrical signal from a transducer. A calibrator generates a reference signal in response to the calibrate command. A combiner mixes the electrical signal with the reference signal to form a calibrated signal. A converter converts the calibrated signal to an optical signal. A transmitter transmits the optical signal to the remote processor. A primary battery supplies power to the calibrator, the combiner, the converter, and the transmitter. An optically-activated switch supplies power to the calibrator, the combiner, the converter, and the transmitter in response to the power switching signal. An auxiliary battery supplies power continuously to the switch means.
Date: December 31, 1992
Creator: Seligmann, D. A.; Moss, W. C.; Valk, T. C. & Conder, A. D.
System: The UNT Digital Library
Passive decay heat removal system for water-cooled nuclear reactors (open access)

Passive decay heat removal system for water-cooled nuclear reactors

This document describes passive decay-heat removal system for a water-cooled nuclear reactor which employs a closed heat transfer loop having heat-exchanging coils inside an open-topped, insulated evaporator located inside the reactor vessel, below its normal water level, in communication with a condenser located outside of containment and exposed to the atmosphere. The heat transfer loop is located such that the evaporator is in a position where, when the water level drops in the reactor, it will become exposed to steam. Vapor produced in the evaporator passes upward to the condenser above the normal water level. In operation, condensation in the condenser removes heat from the system, and the condensed liquid is returned to the evaporator. The system is disposed such that during normal reactor operations where the water level is at its usual position, very little heat will be removed from the system, but during emergency, low water level conditions, substantial amounts of decay heat will be removed.
Date: December 31, 1990
Creator: Forseberg, C. W.
System: The UNT Digital Library
Tritium monitor (open access)

Tritium monitor

This invention is comprised of a system for continuously monitoring the concentration of tritium in an aqueous stream. The system pumps a sample of the stream to magnesium-filled combustion tube which reduces the sample to extract hydrogen gas. The hydrogen gas is then sent to an isotope separation device where it is separated into two groups of isotopes: a first group of isotopes containing concentrations of deuterium and tritium, and a second group of isotopes having substantially no deuterium and tritium. The first group of isotopes containing concentrations of deuterium and tritium is then passed through a tritium detector that produces an output proportional to the concentration of tritium detected. Preferably, the detection system also includes the necessary automation and data collection equipment and instrumentation for continuously monitoring an aqueous stream.
Date: December 31, 1992
Creator: Chastagner, P.
System: The UNT Digital Library
Open apex shaped charge-type explosive device having special disc means with slide surface thereon to influence movement of open apex shaped charge liner during collapse of same during detonation (open access)

Open apex shaped charge-type explosive device having special disc means with slide surface thereon to influence movement of open apex shaped charge liner during collapse of same during detonation

An open apex shape charge explosive device is disclosed having an inner liner defining a truncated cone, an explosive charge surrounding the truncated inner liner, a primer charge, and a disc located between the inner liner and the primer charge for directing the detonation of the primer charge around the end edge of the disc means to the explosive materials surrounding the inner liner. The disc comprises a material having one or more of: a higher compressive strength, a higher hardness, and/or a higher density than the material comprising the inner liner, thereby enabling the disc to resist deformation until the liner collapses. The disc has a slide surface thereon on which the end edge of the inner liner slides inwardly toward the vertical axis of the device during detonation of the main explosive surrounding the inner liner, to thereby facilitate the inward collapse of the inner liner. In a preferred embodiment, the geometry of the slide surface is adjusted to further control the collapse or {beta} angle of the inner liner.
Date: December 31, 1992
Creator: Murphy, M. J.
System: The UNT Digital Library
Laser patterning of laminated structures for electroplating (open access)

Laser patterning of laminated structures for electroplating

Disclosed is a process for laser patterning of a substrate so that it can be subsequently electroplated or electrolessly plated. The process utilizes a laser to treat an inactive (inert) layer formed over an active layer to either combine or remove the inactive layer to produce a patterned active layer on which electrodeposition can occur. The process is carried out by utilizing laser alloying and laser etching, and involves only a few relatively high yield steps and can be performed on a very small scale.
Date: December 31, 1992
Creator: Mayer, S. T. & Evans, L. B.
System: The UNT Digital Library
High resolution data acquisition (open access)

High resolution data acquisition

A high resolution event interval timing system measures short time intervals such as occur in high energy physics or laser ranging. Timing is provided from a clock pulse train and analog circuitry for generating a triangular wave synchronously with the pulse train. The triangular wave has an amplitude and slope functionally related to the time elapsed during each clock pulse in the train. A converter forms a first digital value of the amplitude and slope of the triangle wave at the start of the event interval and a second digital value of the amplitude and slope of the triangle wave at the end of the event interval. A counter counts the clock pulse train during the interval to form a gross event interval time. A computer then combines the gross event interval time and the first and second digital values to output a high resolution value for the event interval.
Date: December 31, 1992
Creator: Thornton, G. W. & Fuller, K. R.
System: The UNT Digital Library
Production of aluminum-26 (open access)

Production of aluminum-26

This invention is a method of producing Al-26 from potassium chloride by exposing it to a proton beam in order to break potassium and chlorine atoms into smaller pieces, which include Al-26. The Al-26 is isolated from the potassium chloride and substances produced by the beam by means of extraction and ion exchange.
Date: December 31, 1990
Creator: Steinkruger, F. J. & Phillips, D. R.
System: The UNT Digital Library
Preventive maintenance system for the photomultiplier detector blocks of pet scanners (open access)

Preventive maintenance system for the photomultiplier detector blocks of pet scanners

The present invention relates to a system for the preventive maintenance of the Photomultiplier Detector Blocks of PET Scanners. This system is used to automatically indicate the expected date of failure of a photomultiplier detector block and provide time for its replacement and maintenance in a scheduled preventive maintenance program, thus eliminating expensive unscheduled downtime of a PET Scanner due to photomultiplier failure.
Date: December 31, 1992
Creator: Levy, A. V. & Warner, D.
System: The UNT Digital Library
Tritium extraction furnace (open access)

Tritium extraction furnace

This invention is comprised of apparatus for heating an object such as a nuclear target bundle to release and recover hydrogen and contain the disposable residue for disposal. The apparatus comprises an inverted furnace, a sleeve/crucible assembly for holding and enclosing the bundle, conveying equipment for placing the sleeve onto the crucible and loading the bundle into the sleeve/crucible, a lift for raising the enclosed bundle into the furnace, and hydrogen recovery equipment including a trap and strippers, all housed in a containment having, negative internal pressure. The crucible/sleeve assembly has an internal volume that is sufficient to enclose and hold the bundle before heating; the crucible`s internal volume is sufficient by itself to hold and enclose the bundle`s volume after heating. The crucible can then be covered and disposed of, the sleeve, on the other hand, can be reused.
Date: December 31, 1992
Creator: Heung, L. K.
System: The UNT Digital Library
Process for forming one or more substantially pure layers in substrate material using ion implantation (open access)

Process for forming one or more substantially pure layers in substrate material using ion implantation

The method comprises selecting an implantable element and a substrate material to be implanted which, at the implant/anneal temperatures, have limited mutual solubility and have no intermediate phases formed. In an example, Be is implanted with 11 {times}10{sup 17} Al/cm{sup 2} at 200 keV and then annealed for 1 h at 500 C. Rutherford backscattering shows that layer formation occurred during the anneal. SEM shows rectangular Be defects in the Al layer. Other examples of implantable elements and suitable substrate materials are tabulated. 6 figs, 1 table. (DLC)
Date: December 31, 1990
Creator: Musket, R. G.; Brown, D. W. & Munir, Z. A.
System: The UNT Digital Library