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A method for sputtering with low frequency alternating current (open access)

A method for sputtering with low frequency alternating current

Low frequency alternating current sputtering is provided by connecting a low frequency alternating current to a high voltage transformer having outer taps and a center tap for stepping up the voltage of the alternating currentThe center tap of the tmsformer is connected to a vacuum vessel containing argon or helium gas. Target electrodes, in close proximity to each other, and containing material with which the substrates will be coated, are connected to the outer taps of the ftwsformer. With an applied potential, the gas will ionize and sputtering from the target electrodes onto the substrate will then result. The target electrodes can be copper or boron, and the substrate can be stainless steel, aluminum, or titanium. Copper coatings produced are used in place of nickel and/or copper striking.
Date: December 31, 1993
Creator: Timberlake, John R.
System: The UNT Digital Library
Apparatus and method for extracting power from energetic ions produced in nuclear fusion (open access)

Apparatus and method for extracting power from energetic ions produced in nuclear fusion

This invention is comprised of an apparatus and method of extracting power from energetic ions produced by nuclear fusion in a toroidal plasma to enhance respectively the toroidal plasma current and fusion reactivity. By injecting waves of predetermined frequency and phase traveling substantially in a selected poloidal direction within the plasma, the energetic ions become diffused in energy and space such that the energetic ions lose energy and amplify the waves. The amplified waves are further adapted to travel substantially in a selected toroidal direction to increase preferentially the energy of electrons traveling in one toroidal direction which, in turn, enhances or generates a toroidal plasma current. In an further adaptation, the amplified waves can be made to preferentially increase the energy of fuel ions within the plasma to enhance the fusion reactivity of the fuel ions. The described direct, or in situ, conversion of the energetic ion energy provides an efficient and economical means of delivering power to a fusion reactor.
Date: December 31, 1993
Creator: Fisch, N. J. & Rax, J. M.
System: The UNT Digital Library
A means for positively seating a piezoceramic element in a piezoelectric valve during inlet gas injection (open access)

A means for positively seating a piezoceramic element in a piezoelectric valve during inlet gas injection

This invention is comprised of a piezoelectric valve in a gas delivery system which includes a piezoceramic element bonded to a valve seal and disposed over a valve seat, and retained in position by an O-ring and a retainer; and insulating ball normally biased by a preload spring against the piezoceramic element; and inlet gas port positioned such that upon admission of inlet gas into the valve. The piezoceramic element is positively seated. The inelt gas port is located only on the side of the piezoceramic element opposite the seal.
Date: December 31, 1993
Creator: Wright, K. E.
System: The UNT Digital Library
Direct current sputtering of boron from boron/carbon mixtures (open access)

Direct current sputtering of boron from boron/carbon mixtures

A method for coating a substrate with boron by sputtering includes lowering the electrical resistance of a boron-containing rod to allow electrical conduction in the rod; placing the boron-containing rod inside a vacuum chamber containing substrate material to be coated; applying an electrical potential between the boron target material and the vacuum chamber; countering a current avalanche that commences when the conduction heating rate exceeds the cooling rate, and until a steady equilibrium heating current is reached and coating the substrate material with boron by sputtering from the boron-containing rod.
Date: December 31, 1993
Creator: Timberlake, John R.; Manos, Dennis & Nartowitz, Ed
System: The UNT Digital Library
Reactive multilayer synthesis of hard ceramic foils and films (open access)

Reactive multilayer synthesis of hard ceramic foils and films

Disclosed is method for synthesizing hard ceramic materials such as carbides, borides and aluminides, particularly in the form of coatings provided on another material so as to improve the wear and abrasion performance of machine tools, for example. Method involves the sputter deposition of alternating layers of reactive metals with layers of carbon, boron, or aluminum and the subsequent reaction of the multilayered structure to produce a dense crystalline ceramic. The material can be coated on a substrate or formed as a foil which can be coiled as a tape for later use.
Date: December 31, 1993
Creator: Makowiecki, Daniel M. & Holt, Joseph B.
System: The UNT Digital Library
Method for fabricating {sup 99}Mo production targets using low enriched uranium, {sup 99}Mo production targets comprising low enriched uranium (open access)

Method for fabricating {sup 99}Mo production targets using low enriched uranium, {sup 99}Mo production targets comprising low enriched uranium

A radioisotope production target and a method for fabricating a radioisotope production target is provided, wherein the target comprises an inner cylinder, a foil of fissionable material (low enriched U) circumferentially contacting the outer surface of the inner cylinder, and an outer hollow cylinder adapted to receive the substantially foil-covered inner cylinder and compress tightly against the foil to provide good mechanical contact therewith. The method for fabricating a primary target for the production of fission products comprises preparing a first substrate to receive a foil of fissionable material so as to allow for later removal of the foil from the first substrate, preparing a second substrate to receive the foil so as to allow for later removal of the foil from the second substrate; attaching the first substrate to the second substrate such that the foil is sandwiched between the first substrate and second substrate to prevent foil exposure to ambient atmosphere, and compressing the exposed surfaces of the first and second substrate to assure snug mechanical contact between the foil, the first substrate and the second substrate.
Date: December 31, 1993
Creator: Wiencek, T. C.; Matos, J. E. & Hofman, G. L.
System: The UNT Digital Library
Fluid sampling system (open access)

Fluid sampling system

This invention comprises a fluid sampling system which allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped up into a sampling jet of venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decrease, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodicially leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.
Date: December 31, 1993
Creator: Houck, E.D.
System: The UNT Digital Library
An improved system and method for networking electrochemical devices (open access)

An improved system and method for networking electrochemical devices

An improved electrochemically active system and method including a plurality of electrochemical devices, such as fuel cells and fluid separation devices are disclosed, in which the anode and cathode process-fluid flow chambers are connected in fluid-flow arrangements so that the operating parameters of each of said plurality of electrochemical devices which are dependent upon process-fluid parameters may be individually controlled to provide improved operating efficiency. Improvements in operation include improved power efficiency and improved fuel utilization in fuel cell power generating systems and reduced power consumption in fluid separation devices and the like through interstage process fluid parameter control for series networked electrochemical devices. The improved networking method includes recycling of various process flows to enhance the overall control scheme.
Date: December 31, 1993
Creator: Williams, M.C.; Wimer, J.G. & Archer, D.H.
System: The UNT Digital Library
Volatile organic compound sensing devices (open access)

Volatile organic compound sensing devices

Apparatus employing vapochromic materials in the form of inorganic double complex salts which change color reversibly when exposed to volatile organic compound (VOC) vapors is adapted for VOC vapor detection, VOC aqueous matrix detection, and selective VOC vapor detection. The basic VOC vapochromic sensor is incorporated in various devices such as a ground probe sensor, a wristband sensor, a periodic sampling monitor, a soil/water penetrometer, an evaporative purge sensor, and various vacuum-based sensors which are particularly adapted for reversible/reusable detection, remote detection, continuous monitoring, or rapid screening of environmental remediation and waste management sites. The vapochromic sensor is used in combination with various fiber optic arrangements to provide a calibrated qualitative and/or quantitative indication of the presence of VOCs.
Date: December 31, 1993
Creator: Lancaster, G.D.; Moore, G.A.; Stone, M.L. & Regen, W.K.
System: The UNT Digital Library
Retractable pin dual in-line package test clip (open access)

Retractable pin dual in-line package test clip

This invention is a Dual In-line Package (DIP) test clip for use when troubleshooting circuits containing DIP integrated circuits. This test clip is a significant improvement over existing DIP test clips in that it has retractable pins which will permit troubleshooting without risk of accidentally shorting adjacent pins together when moving probes to different pins on energized circuits or when the probe is accidentally bumped while taking measurements.
Date: December 31, 1993
Creator: Bandzuch, G.S. & Kosslow, W.J
System: The UNT Digital Library
High temperature metallic diffraction gratings and process of manufacturing same (open access)

High temperature metallic diffraction gratings and process of manufacturing same

This invention is comprised of a method of applying diffraction gratings or images directly to the surface of a substrate wherein the gratings or images are capable of withstanding high temperatures, pressures, humidity and other such conditions related to materials testing. The method includes coating the surface of the substrate with an uniform layer of metal which is then overlaid with a layer of photo-resist material. Next, after contacting the photo-resist material with a master image containing regions of opacity and transparency, electromagnetic radiation is directed through the master image to expose the photo-resist material such that a contact print of the master image is produced on the photo-resist material. Then, after removing the master image, the photo-resist material is developed so as to remove unhardened portions thereof and leave corresponding portions of the metal layer uncovered. Finally, after removing or etching the uncovered portions of the metal layer, the remaining photo-resist material is removed to produce a metallic diffraction grating or image of predetermined size and pattern on the surface of the substrate.
Date: December 31, 1993
Creator: Deason, V. A.; Hsu, Karen M. & Miller, R. L.
System: The UNT Digital Library
Mercury-Free Dissolution of Aluminum-Clad Fuel in Nitric Acid (open access)

Mercury-Free Dissolution of Aluminum-Clad Fuel in Nitric Acid

It is the purpose of this invention to provide a continuous optimum process for the dissolution of aluminum, without the use of a mercury catalyst. Ile invention generally stated is: a process for dissolution of aluminum comprising: preparing a mixture of nitric acid`and fluoboric acid in a makeup vessel or individual reagents in separate vessels; placing an aluminum element in a dissolver vessel having an overflow; transferring a portion of the mixture of nitric acid and fluoboric acid to the dissolver vessel from the makeup vessel; heating the dissolver vessel and mixture to a boiling temperature and holding that temperature until a desired concentration of dissolved aluminum is achieved; adding a constant flow influent of the mixture of nitric acid and fluoboric acid to the dissolver vessel; and collecting an effluent from the dissolver vessel overflow, said effluent containing a mixture of aluminum nitrate, nitric acid, fluoboric acid, water, and dissolved fuel components. The variables in the above process can be temperature, effluent flow rate, and concentration of the acids as will be discussed later. For corrosion control, it may be necessary to initiate reaction at a decreased HNO{sub 3} concentration and to increase it after a sufficient concentration of …
Date: December 31, 1993
Creator: Christian, J. D. & Anderson, P. A.
System: The UNT Digital Library
Fiber optic sensor for detecting damage location and shock wave velocity (open access)

Fiber optic sensor for detecting damage location and shock wave velocity

This invention is comprised of a shock velocity and damage location sensor providing a means of measuring shock speed and damage location. The sensor consists of a long series of time-of-arrival `points` constructed with fiber optics. The fiber optic sensor apparatus measures shock velocity as the fiber sensor is progressively crushed as a shock wave proceeds in a direction along the fiber. The light received by a receiving means changes as time-of-arrival points are destroyed as the sensor is disturbed by the shock. The sensor may comprise a transmitting fiber bent into a series of loops and fused to a receiving fiber at various places, time-of-arrival points, along the receiving fibers length. At the `points` of contact, where a portion of the light leaves the transmitting fiber and enters the receiving fiber, the loops would be required to allow the light to travel backwards through the receiving fiber toward a receiving means. The sensor may also comprise a single optical fiber wherein the time-of-arrival points are comprised of reflection planes distributed along the fibers length. In this configuration, as the shock front proceeds along the fiber it destroys one reflector after another. The output received by a receiving means from …
Date: December 31, 1993
Creator: Weiss, J.D.
System: The UNT Digital Library
Apparatus and method for laser deposition of durable coatings (open access)

Apparatus and method for laser deposition of durable coatings

Disclosed are method and apparatus for depositing durable coatings onto the surface of a substrate without heating the entire substrate to high temperatures by using lasers to heat the substrate and dissociate a deposition gas. The apparatus comprises a deposition chamber for enclosing the substrate upon which a coating is to be deposited, gas delivery means for directing a flow of deposition gas on the substrate, a first laser for heating the substrate, and a second laser for irradiating the deposition gas to dissociate the gas. The method includes placing a substrate within a vacuum deposition chamber and directing a flow of deposition gas on the substrate. Then the substrate is heated with a first laser while the deposition gas is irradiated with a second laser to dissociate the deposition gas.
Date: December 31, 1993
Creator: Veligdan, J.T.; Vanier, P. & Barletta, R.E.
System: The UNT Digital Library
A staged fluidized-bed comubstion and filter system (open access)

A staged fluidized-bed comubstion and filter system

A staged fluidized-bed combustion and filter system for substantially reducing the quantity of waste through the complete combustion into ash-type solids and gaseous products. The device has two fluidized- bed portions, the first primarily as a combustor/pyrolyzer bed, and the second as a combustor/filter bed. The two portions each have internal baffles to define stages so that material moving therein as fluidized beds travel in an extended route through those stages. Fluidization and movement is achieved by the introduction of gasses into each stage through a directional nozzle. Gases produced in the combustor/pyrolyzer bed are permitted to travel into corresponding stages of the combustor/filter bed through screen filters that permit gas flow but inhibit solids flow. Any catalyst used in the combustor/filter bed is recycled. The two beds share a common wall to minimize total volume of the system. A slightly modified embodiment can be used for hot gas desulfurization and sorbent regeneration. Either side-by-side rectangular beds or concentric beds can be used. The system is particularly suited to the processing of radioactive and chemically hazardous waste.
Date: December 31, 1993
Creator: Mei, J.S. & Halow, J.S.
System: The UNT Digital Library
Ammonia release method for depositing metal oxides (open access)

Ammonia release method for depositing metal oxides

A method of depositing metal oxides on substrates which is indifferent to the electrochemical properties of the substrates and which comprises forming ammine complexes containing metal ions and thereafter effecting removal of ammonia from the ammine complexes so as to permit slow precipitation and deposition of metal oxide on the substrates.
Date: December 31, 1993
Creator: Silver, G.L. & Martin, F.S.
System: The UNT Digital Library
End moldings for cable dielectrics (open access)

End moldings for cable dielectrics

End moldings for high-voltage cables are described wherein the dielectric insulator of the cable is heated and molded to conform to a desired shape. As a consequence, high quality substantially bubble- free cable connectors suitable for mating to premanufactured fittings are made. Disclosed are a method for making the cable connectors either in the field or in a factory, molds suitable for use with the method, and the molded cable connectors, themselves.
Date: December 31, 1993
Creator: Roose, L.D.
System: The UNT Digital Library
Indirect-Fired Gas Turbine Bottomed With Fuel Cell (open access)

Indirect-Fired Gas Turbine Bottomed With Fuel Cell

An indirect-heated gas turbine cycle is bottomed with a fuel cell cycle with the heated air discharged from the gas turbine being directly utilized at the cathode of the fuel cell for the electricity-producing electrochemical reaction occurring within the fuel cell. The hot cathode recycle gases provide a substantial portion of the heat required for the indirect heating of the compressed air used in the gas turbine cycle. A separate combustor provides the balance of the heat needed for the indirect heating of the compressed air used in the gas turbine cycle. Hot gases from the fuel cell are used in the combustor to reduce both the fuel requirements of the combustor and the NOx emissions therefrom. Residual heat remaining in the air-heating gases after completing the heating thereof is used in a steam turbine cycle or in an absorption refrigeration cycle. Some of the hot gases from the cathode can be diverted from the air-heating function and used in the absorption refrigeration cycle or in the steam cycle for steam generating purposes.
Date: December 31, 1993
Creator: Micheli, Paul L.; Williams, Mark C. & Parsons, Edward L.
System: The UNT Digital Library
Method of removal of heavy metal from molten salt in IFR fuel pyroprocessing (open access)

Method of removal of heavy metal from molten salt in IFR fuel pyroprocessing

An electrochemical method of separating heavy metal values from a radioactive molten salt including Li halide at temperatures of about 500{degree}C. The method comprises positioning a solid Li-Cd alloy anode in the molten salt containing the heavy metal values, positioning a Cd-containing cathode or a solid cathode positioned above a catch crucible in the molten salt to recover the heavy metal values, establishing a voltage drop between the anode and the cathode to deposit material at the cathode to reduce the concentration of heavy metals in the salt, and controlling the deposition rate at the cathode by controlling the current between the anode and cathode.
Date: December 23, 1993
Creator: Gay, E.C.
System: The UNT Digital Library
Interline Transfer CCD Camera (open access)

Interline Transfer CCD Camera

An interline CCD sensing device for use in a camera system, includes an imaging area sensitive to impinging light, for generating charges corresponding to the intensity of the impinging light. Sixteen independent registers R1 - R16 sequentially receive the interline data from the imaging area, corresponding to the generated charges. Sixteen output amplifiers S1 - S16 and sixteen ports P1 - P16 for sequentially transferring the interline data, one pixel at a time, in order to supply a desired image transfer speed. The imaging area is segmented into sixteen independent imaging segments A1 - A16, each of which corresponds to one register, on output amplifier, and one output port. Each one of the imaging segments A1 - A16 includes an array of rows and columns of pixels. Each pixel includes a photogate area, an interline CCD channel area, and an anti-blooming area. The anti-blooming area is, in turn, divided into an anti-blooming barrier and an anti-blooming drain.
Date: December 31, 1993
Creator: Prokop, Mark S.; McCurnin, Thomas W.; Stump, Charles J. & Stradling, Gary L.
System: The UNT Digital Library
Method and apparatus for dissipating remanent fields and preserving diamagnetism of ceramic superconductors (open access)

Method and apparatus for dissipating remanent fields and preserving diamagnetism of ceramic superconductors

A method for dissipating a remanent field, created when a magnetic field is brought into contact with a superconductor, while preserving the diamagnetism of a superconductor comprises the steps of (1) providing a ceramic superconductor; (2) continuously or intermittently generating an AC current to the ceramic superconductor; and (3) gradually decreasing the AC current until the undesired remanent field is dissipated.
Date: December 1993
Creator: Youngdahl, C. A.
System: The UNT Digital Library
Reusable vibration resistant integrated circuit mounting socket (open access)

Reusable vibration resistant integrated circuit mounting socket

This invention discloses a novel form of socket for integrated circuits to be mounted on printed circuit boards. The socket uses a novel contact which is fabricated out of a bimetallic strip with a shape which makes the end of the strip move laterally as temperature changes. The end of the strip forms a barb which digs into an integrated circuit lead at normal temperatures and hold it firmly in the contact, preventing loosening and open circuits from vibration. By cooling the contact containing the bimetallic strip the barb end can be made to release so that the integrated circuit lead can be removed from the socket without damage either to the lead or to the socket components.
Date: December 31, 1993
Creator: Evans, C.N.
System: The UNT Digital Library
Use of CHELEX-100{reg_sign} for radionuclide purification (open access)

Use of CHELEX-100{reg_sign} for radionuclide purification

A method for selectively removing yttrium-90 from its parent strontium-90 contained in an environmental sample includes loading the sample onto a column containing a chelating ion-exchange resin capable of retaining yttrium-90; washing the column with a solution capable of removing strontium, calcium and other contaminants from the yttrium-90 fraction retained on the column; removing excess acetate salts from the column; eluting yttrium-90 solution from the column and adjusting the pH of this solution to about 2.7; filtering the yttrium-90 solution and weighting this solution for gravimetric yield; and, counting the yttrium-90 containing solution with a radiological counter for a time sufficient to achieve the statistical accuracy desired. It is preferred that the chelating ion-exchange resin is a bidente ligand having the chemical name iminodiacetic acid mounted on a divinyl benzene substrate, converted from sodium form to ammonia form. Its name is Chelex-100{reg_sign}.
Date: December 1993
Creator: Huntley, M. W.
System: The UNT Digital Library
Visual cluster analysis and pattern recognition template and methods (open access)

Visual cluster analysis and pattern recognition template and methods

This invention is comprised of a method of clustering using a novel template to define a region of influence. Using neighboring approximation methods, computation times can be significantly reduced. The template and method are applicable and improve pattern recognition techniques.
Date: December 31, 1993
Creator: Osbourn, Gordon Cecil & Martinez, Rubel Francisco
System: The UNT Digital Library