From abstract: The concept of using high intensity beta radiation from an isotopic source, Sr-90, inside a high temperature, high pressure chemical reactor has been developed for potential radiation chemical processes. Distinct advantages include high utilizable intensity from a relatively small source with a minimum of shielding against external radiation.

Summary: The Regnault Method as applied to tritium purity determinations is described. The operating difficulties, such as temperature and humidity changes, static charges, excessive vibrations, contamination with air and helium, etc., and the methods currently in use for minimizing such difficulties, are discussed. A discussion of ion-chamber calibrations, and the correlation of ion-chamber results with Regnault Method results, are included. A precision of ±1% has been obtained, but the accuracy is not yet known.

A pile gas leak detection system consisting of a purchased mass spectrographic type of helium detector, a long sampling line for use in remote or relatively inaccessable locations, a pump to pull a continuous sample of gas from the tip of the probe to the detector, and a rotameter to measure the gas flow rate in the sampling line has been developed, calibrated, operationally tested. The system is practical for use in locating all pile gas leaks larger than about 0.1 cubic foot per hour.

Abstract: The counting accuracy of the Chicago Scalers, Models 961A and 961B, is a function of the bias setting of the limiter (V2). this report gives quantitative data supporting this thesis. A method of making bias settings is suggested. These tests were run at the suggestion of Mr. V. C. Hanson.

Abstract: Pure UO2F2 is made by reaction between anhydrous HF and pure UO3. Although it is difficult to prepare free of water, it is not very hygroscopic. Prolonged heating at 100-105 degrees releases 99.9% of the water in an aqueous solution; the rate of loss of water is very small after saturation is reached. X-ray diffraction data give a density of 6.2 for the solid. The density of a 1.004 M solution is 1.274; the density of a saturated solution (5.130 M) is 2.400. The densities of F-9 solutions have been calculated from the densities of ordinary aqueous solutions, and the values are compared graphically. Data on the solubility indicate that there is a small increase in the range 25-100 degrees. Recovery of pure F-9 from a solution is hampered by hydrolysis of U)2F2 to give HF. The HF may be held back by addition of UO3 or CaO; the use of the latter, however, makes more difficult the recovery of all the F-9. Molar conductivities of UO2F2 solutions at 25 degrees, as well as the specific conductivities of a 1 molar solution containing various concentrations of UO3, have been determined. The addition of UO3 lowers the conductivity. The low …