The Extraction of Uranium into Hexone as Uranyl Thiocyanate from Thorium Nitrate Solutions (open access)

The Extraction of Uranium into Hexone as Uranyl Thiocyanate from Thorium Nitrate Solutions

Technical report with six sections describing the process: (1) The reaction of HN)3 with HSCN; (2) The distribution of nitric acid between hexone and water; (3) The distribution of HSCN between hexone and water; (4) The solubility of thorium sulfate in various extraction solutions; (5) The distribution of protoactinium and fission elements between hexone and aqueous thiocyanate solutions; and (6) Separation of uranium from thorium by extraction into hexone as UO2(SCH)a.
Date: May 18, 1945
Creator: Reas, William H.
System: The UNT Digital Library
Stabilizer for Temperature Control Equipment (open access)

Stabilizer for Temperature Control Equipment

From abstract: "A simple electronic circuit is described, the use of which greatly improves the temperature regulations obtainable with Beta equipment. The circuit utilizes the time derivative of the temperature to counteract oscillation and overshoot. No other changes are required in existing equipment for installation of the stabilizer."
Date: May 14, 1945
Creator: Macleish, K. G. & Palmer, R. C.
System: The UNT Digital Library
Progress Report on Corrosion Tests in TCl₄ (open access)

Progress Report on Corrosion Tests in TCl₄

This report describes progress in testing the corrosion resistance of alloys of TCl₄. The steps and conditions of the testing procedures are given as well as conclusions and photos of TCl₄.
Date: May 26, 1945
Creator: Mash, Donald R.
System: The UNT Digital Library
Development of Equipment for the Purification of Mercury by Distillation (open access)

Development of Equipment for the Purification of Mercury by Distillation

Abstract: "An investigation of the mercury salvage program has resulted in the development of an improved high compacity type of distillation apparatus. The still, electrically heated and essentially automatic in its operation, will produce at a rate greater than 75 pounds per hour and develop a product 99.99% pure or better. This still will handle the lowest grade crude of amalgam that can pass through the feed lines and will continue to develop a pure prodcut for comparatively long periods of time. The clean-out operation is amazingly simple and convenient and may be done within one-half hour while the apparatus itself is still hot. Two models of this design are scheduled for installation in a mercury recovery room of the Alpha Analytical Department of Building No. 9207."
Date: May 26, 1945
Creator: Lee, J. E. & Susano, C. D.
System: The UNT Digital Library
Analysis for Oxide in Thorium Metal (open access)

Analysis for Oxide in Thorium Metal

Abstract. to estimate the oxygen picked up by thorium in casting a rapid method of running the acid insoluble content was developed. the quickest procedure consists of reacting with mixed acids, fuming with perchloric and filtration to separate the "free" thorium from the "combined". The precipitate is ignited and weighed as thorium dioxide.
Date: May 12, 1945
Creator: Ayers, A. S.
System: The UNT Digital Library
Analysis of Heavy Water by Equilibration (open access)

Analysis of Heavy Water by Equilibration

Technical report discussing that the deuterium concentration of heavy water can be determined by equilibrating the water with deuterium gas in the presence of a catalyst with subsequent analysis of the equilibrated gas on the mas spectrometer. The apparatus for equilibration analyses maybe be considered in three parts: 1) apparatus for introducing the ingredients into the reaction chambers; 2) the reaction chambers; 3) the mass spectrometer for analysis of the equilibrated gas. The isotopic composition of the deuterium gas to be used as the starting material is primarily governed by what gases are available. In general it is best to use gas within about one percent on either side of the final equilibrium composition. No reaction takes place between deuterium gas and water molecules in the absence of a catalyst. Platinum oxide is used as the catalyst.
Date: May 15, 1945
Creator: Fischer, R. B.; Potter, R. A. & Voskuyl, R. J.
System: The UNT Digital Library