Technical report containing short articles on (1) Determination of physical constants for U233; (2) Determination of decay chain of U233; (3) Extraction of U233; (4) Extracting solvents for uranium; (5) Factors affecting the extraction uranium and thorium by organic solvents, especially ether; and (6) Analysis of ore samples for protoactinium.

Abstract: "The determination of trace concentrations of uranium in synthetic materials, ores, soils and water by neutron radioactivation analysis is described. The principles of the activation analysis method as applied to trace uranium determination, the processing of irradiated specimens, and some examples of the results obtained by this method of analysis are discussed in this paper."

Activities in a program to develop techniques in the use of pulsed neutron sources to measure shutdown parameters related to large thermal power reactors are reported. In the course of this program, a new theory was suggested and an experimental apparatus was designed and built. Experiments were carried out to test the new model. This present report contains additional data and information extracted from the experiments at PG&E Humboldt Bay Power Reactor at Eureka, California. During the last days of 1963 a number of control rod and fuel bundle worth measurements were made in the ESADA Vallecitos Experimental Superheat Reactor (EVESR) using the (k[beta]/[script l] technique. A description of the experiments is given in the text of the report and some results are reported. A computer program was written to perform the data analysis of the pulsed neutron experiments and the code is discussed in the Appendix.

This report deals with a group of both theoretical and experimental investigations which have been carried out, utilizing Core 15, one in a series of critical assemblies that have been constructed at Atomics International's Epithermal Critical Experiments Laboratory (ECEL).

Report that "is a supplement to IDO-16332, "The Engineering Test Reactor Critical Facility Hazards Summary Report", presenting information on the conduct in the Facility of certain experiments which are expected to be operated in the Engineering Test Reactor" (p. 3).

Two methods are described for extending the Thomas-Fermi model of a compressed atom to molecules or mixtures of the type Z Zn. The methods are applied to H2O at zero temperature to determine pressure and internal energy as functions of the density, the position of the protons relative to the oxygen nucleus, and the electrostatic potential distribution within the molecule.

A generalization of the Lindemann law is used in connection with the Murnaghan equation of state for a solid to derive theoretically the empirical Simon equation for the fusion curve. For the alkali metals it is shown that experimental values of the temperature exponent in the Simon equation are quantitatively compatible with the theoretical evaluation given, and, furthermore, that the theory can predict approximate values of the experiment, in practice.

This report describes the flow meter for measuring air-flow rate through special hoods that allow the decrease in flow rate.

Abstract: "The reaction between nitrogen and carbon dioxide, under irradiation with 40 Mev alpha particles from the Berkeley 60 inch cyclotron, was studied at gas temperatures near 50 C and total pressures of about 600 millimeters of Hg, contained in Pyrex capsules. The range of gas compositions investigated included the pure components, as well as mixtures with and without trace oxygen. In all mixtures, a steady state concentration of nitrogen oxides of about 0.15 millimeter was reached after a few microampere hours exposure. The mass-spectrometer analytical procedure employed did not permit identification of the individual species of oxides present. This report is based on studies conducted for the Atomic Energy Commission under Contract AT-11-1-GEN-8."

The following report provides data describing the total electron beam current as a function of A-12 beam radius. The beam is investigated using the provided equations.

Part A. The major effort during the past year has been the construction of a suitable vacuum furnace for studying the effects of temperature and pressure on the wettability of metals by glass. A systems was completed that was capable of subjecting test combinations up to temperatures of 1400 degree C at a working pressure of 1 x 10(-5) mm. of Hg. Part B. A compound, identified by X-ray analysis as sodium meta tantalate (na2Ta2O6), was found at the interface between a sodium silicate glass and tantalum metal which had been heated in vacuum to 1000 degree C. thermodynamic calculations, followed by further experimental evidence, were used to determine the chemical reaction between tantalum and sodium silicate which resulted in the formation of Na2Ta3O6. the compound was synthesized by other methods, and its structure investigated.

Abstract: "Since the first report on the use of amines as uranium extractants (ORNL-1734) over eighty additional organo-nitrogen compounds have been examined for their ability to extract uranium from aqueous solutions, particularly sulfate solutions, of the types usually encountered in uranium ore processing. As before, the more promising of these (as well as other compounds previously reported) have been examined further with respect to other characteristics essential to practical application, i.e., reagent loss to the aqueous phase, compatibility with practicable diluents, influence of commonly present anions, reagent stability, sufficient selectivity for uranium, adequate phase separation properties, compatibility with practicable stripping methods, etc. The potential cost and availability of the reagents tested, i.e., certain secondary and tertiary amines, have shown even greater promise as practicable extraction agents than many of the promising compounds previously tested. In addition to the work with sulfate liquors, cursory studies have been made of uranium extraction from fluoride and sulfate-fluoride solutions. Extractions of other metals from sulfate liquors, i.e., titanium and thorium, have been briefly examined."

Abstract: "A measurement of the heat liberated when chlorine trifluoride reacts with water has been made in a simple Dewar calorimeter. The chlorine trifluoride vapor was bubbled into approximately 20 moles of water; the weight of material used, heat equivalent of the calorimeter, and the temperature rise of the water and calorimeter were determined. From these data an average value for the heat of reaction was calculated to be 81.0 +/- 0.4 kcal/mole. Analysis of the reaction solution and evolved gas showed the following to be present: hydrogen fluoride, hydrogen chloride, chlorine, oxygen, and probably oxygen-chlorine compounds."

Two principle reasons exist for the extension of high pressure research to temperatures near absolute zero. First, the comparison of certain data with theory (such as the pressure-volume relationship) is more meaningful if the effects of thermal vibrations can be ignored. Second, there are phenomena which can be studied only at low temperatures. These include superconductivity, the properties of solid helium and other inert gases, some electronic phenomena, etc.

Technical report containing the detailed design of the equipment within the reactor shield, reviewed in 1950. Contains various summaries on engineering design and development, reactor physics, chemical studies, and corrosion.

Report documenting the ongoing research and developments of the Oak Ridge National Laboratory's Homogeneous Reactor Project.

Abstract: "The deuterium plasma which is ejected by a 6000-ampere pulsed current through a rail-type spark source has a yield in the forward direction which is a factor of 5 to 10 greater than that in the perpendicular direction. This effect is believed to be due to the magnetic propulsion of the plasma."

A first iteration of the diffusion theory result is executed for the thermal flux distribution in a 7.5" graphite-uranium lattice cell using the integral equation formulation of transport theory.

Abstract: In the Biology Division, the maintenance of animals containing radioactive materials posed many problems. In addition to routine care of the animals, protection had to be provided for the personnel who worked with the contaminated animals. Frequent air changed in the room in which the animals were caged were necessary: farm workers were required to wear masks; animal cages were checked regularly for radiation; acid was used on the sawdust in the excrete pens; and a new, more efficient type of cage was designed. The most import feature of the new cage was that the support for the screen floor was outside the confines of the cage. Stainless steel was the preferred metal for case construction. Photographs and working drawings of cages for mice, rats, guinea pigs, rabbits, and goats, and several types of metabolism cases are included in this paper. Cage decontamination was accomplished with the aid of complexing agents such as citric acid or sodium tartrate. Under certain conditions, nitric acid was used.

The following report describes a reactor that was designed to provide a research facility for testing various materials in a high intensity radiation field.

Report discussing the progress of various research projects by members of the Mathematics Panel at Oak Ridge National Laboratory for the quarter ending April 30, 1952.

"An analysis is presented of the accidental release of activity following the operation of the NS "Savannah" at the New York Shipbuilding Corporation docks in Camden, New Jersey. Although a number of accidents are considered, the report is primarily concerned with the environmental activity levels and subsequent exposures which would result from the "maximum credible accident" (p. v).

Report that describes the research and developments of the Nuclear Safety Research and Development Program of the Oak Ridge National Laboratory.

Report documenting ongoing research and development carried out by the Instrumentation and Controls Division of the Oak Ridge National Laboratory.