Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores (open access)

Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores

Abstract: "Dissolution of carnotite in several readily liquefiable gases, including ammonia, sulfur dioxide, chlorine, and nitrogen dioxide, was found to be negligible, even in the presence of uranium complexing agents. No low-boiling liquids have been found which will dissolve carnotite directly. Treatment with various sulfur chloride will convert carnotite to a form soluble in water or in certain organic solvents. Also, carnotite can be readily dissolved in HCl-acidified ethanol, methanol, or acetone. Amenability tests on nine western ores with HCl-methanol solvent indicated that uranium extractions greater than 90 per cent could be obtained if sufficient acid was used to insure some free acidity in the pregnant liquor. Temple Mountain and Sinbad-Muddy River ores were exceptions to this, uranium extractions being only about 50-60 per cent. Vanadium extractions were invariably lower than uranium extractions. Chemical analyses are presented for nine western ores."
Date: January 15, 1953
Creator: Ewing, R. A.; Pobereskin, M.; Kiehl, S. J.; Foley, D. D.; Filbert, Robert B.; Kimball, R. B. et al.
System: The UNT Digital Library
Identification of Reaction Products Formed During Magnesium Reduction of Uranium Tetrafluoride: Report (open access)

Identification of Reaction Products Formed During Magnesium Reduction of Uranium Tetrafluoride: Report

Abstract: "This report describes the results of X-ray diffraction examination of reaction products from a series of experiments performed by Mallinckrodt Chemical Works as an acid in understanding the process of bomb reduction of UF4. UF4 is initially reduced to UF3 by magnesium at 560 C., and subsequently to metal at 600 C. MgF2 from the initial reaction forms a coating on the magnesium which retards the final spontaneous reaction."
Date: May 15, 1953
Creator: Schwartz, C. M. & Vaughan, D. A.
System: The UNT Digital Library
Corrosion-Resistant Materials for Hydrofluoric Acid : Progress Report (open access)

Corrosion-Resistant Materials for Hydrofluoric Acid : Progress Report

Introduction: Among the many corrosion problems encountered in the production of uranium tetrafluoride and uranium metal from ores and concentrates, some of the most serious occur where hydrofluoric acid must be handled.
Date: June 15, 1953
Creator: Pray, H. A.; Fink, F. W.; Friedl, B. E. & Braun, W. J.
System: The UNT Digital Library
Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores (open access)

Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores

This report describes progress in testing non-aqueous extraction methods for leaching Western ores of uranium and vanadium.
Date: April 15, 1953
Creator: Ewing, R. A.; Pobereskin, M.; Kimball, R. B. & Bearse, A. E.
System: The UNT Digital Library
Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores (open access)

Progress Report on Nonaqueous Extractive Methods for Western Uranium Ores

The following progress report is part of a series of reports on the study of nonaqueous extractive methods for western uranium ores. This report continues studies on HCl-methanol leaching of Western ores, primarily on Temple Mountain ores.
Date: July 15, 1953
Creator: Ewing, R. A.; Pobereskin, M.; Kiehl, S. J.; Foley, D. D.; Filbert, Robert B.; Kimball, R. B. et al.
System: The UNT Digital Library
Investigation of the Behavior of NaOH-UO₃ Slurries in Small Flow Loops (open access)

Investigation of the Behavior of NaOH-UO₃ Slurries in Small Flow Loops

From introduction: "This report presents the results of an experimental program to evaluate engineering problems which might be encountered when circulating NaOH-UO3 slurry through a thermal cycle."
Date: September 15, 1953
Creator: Stang, J. H.; Lagedrost, J. F.; Simons, E. M. & Dayton, R. W.
System: The UNT Digital Library