Kinetics of the Beta Transformation of Uranium (open access)

Kinetics of the Beta Transformation of Uranium

From abstract: "When uranium is heat treated at low beta-phase temperatures and air cooled, the rate of loss of preferred orientation is markedly less than the rate of coarsening of the grain structure. A coarse-grained structure cannot therefore be taken as an infallible indication of satisfactory heat treatment. The final grain size of incompletely transformed metal is essentially equal to or larger than the starting grain size. Large-grained specimens can not be refined by interruption of the transformation at an intermediate stage."
Date: September 1957
Creator: McDonell, William R.
System: The UNT Digital Library
Radiation Bursts in U235 Solutions (open access)

Radiation Bursts in U235 Solutions

From abstract: "Calculations are made of the magnitude of the radiation bursts that can occur in a mixer-settler and in a large tank containing U235 solution if the concentration gets out of control. Various rates of increase in concentration are studied and various restraints are imposed on the expansion of the systems. The neutron kinetics equations, with five groups of delayed neutrons, and the equations relating the neutron flux to the pressure and volume of the gas formed by fission fragments are combined into a single first-order nonlinear differential matrix equation which is solved numerically on the IBM 650. In a mixer-settler containing 9.7 kg of U235 the magnitude of the burst was calculated to be about 10^17 fissions, both for low rates of increase in reactivity (<[or equal to]0.01% per sec) regardless of the confinement, and for an unconfined system regardless of the rate of increase reactivity. In a tank containing 88.9 kg of U235 successive bursts of about 10^19 fissions were calculated to occur about 0.5 second apart when the rate of increase in reactivity was about 0.1% per second."
Date: September 1958
Creator: Clark, Hugh K.
System: The UNT Digital Library
Formation of Hydrazoic Acid From Hydrazine in Nitric Acid Solutions (open access)

Formation of Hydrazoic Acid From Hydrazine in Nitric Acid Solutions

Technical report. From Abstract : "A study was made of the kinetics and stoichiometry of the formation of hydrazoic acid in nitric acid solutions containing hydrazine and ferrous sulfamate. The data were used to establish safe limits for the use of hydrazine in process solutions."
Date: September 1962
Creator: Dukes, E. Kenneth & Wallace, Richard M.
System: The UNT Digital Library
Determination of Neptunium in High Activity Waste (open access)

Determination of Neptunium in High Activity Waste

Technical report. From Abstract : "An existing ion exchange method was adapted for use in a shielded facility to separate Np237 from highly radioactive solutions. The subsequent determination of neptunium was made by alpha counting and alpha pulse height analysis. The coefficient of variation was $.8% (n=10) for a synthetic sample and 5.9% (n=23) for plant samples."
Date: September 1962
Creator: Holcomb, H. Perry
System: The UNT Digital Library
Determination of Neptunium by Extraction With Tri-n-Octylamine (open access)

Determination of Neptunium by Extraction With Tri-n-Octylamine

Technical report. From Abstract : "An analytical method was developed for the determination of Np237 in solutions that contain plutonium and fission products. Np (IV) was extracted into tri-n-octylamine. A quantitative recovery of a Np237 standard was obtained with a coefficient of variation of 1.0% (n=10). A coefficient of variation of 3% was obtained for seven analyses of a process sample."
Date: September 1962
Creator: Britt, Robert D., Jr.
System: The UNT Digital Library