A total of nine clad plates, containing uranium -5 w/o zirconium 1.5 w/o niobium alloy cores and clad with Zircaloy-II, were rolled in plain carbon steel jackets, heat treated, physically evaluated, and corrosion tested. All these plates were found to be within predetermined dimensional tolerance in width, thickness, length, cladding thickness, and core distribution. Improved control of wielding variables and of the length of the seal pin projecting above the end plugs resulted in the elimination of frequently observed segmented inclusions at the seal pin interfaces.

"Properly designed and fitted respirators have been effective devices for reducing the inhalation of toxic aerosols. The degree of protection afforded by these devices has not been quantitatively measured under actual work conditions except by bioassay or other elaborate techniques. This report describes a new quantitative technique for evaluating over-all respiratory performance under conditions comparable to exposure to highly toxic radioactive materials such as plutonium and non-radioactive materials such as beryllium."

Technical report. From Introduction : "The nuclear volume dependent isotope shift of optical spectral lines has long been a very useful means for studying the changes in the nuclear size or shape for different isotopes of heavy elements."

From introductory paragraphs: "The central problems in neutron research are the understanding of nuclear structure and the study of the properties of nuclear particles, particularly the properties of the neutron. The most fruitful attack on these problems is the determination of the probability of interactions between neutrons and nuclei, i.e., the measurement of neutron cross sections. Ideally, this involves the study of all possible types of neutron interaction with all available nuclei at all neutron energies...The discussion in this paper will omit the interactions leading to neutron productions, and will be limited to the intersections of neutrons with stable nuclei."

Under the stimulus of electronic materials development - particularly thin-film studies - and the need for space environmental simulation chambers, a very rapid increase in the availability of industrial-sized vacuum components and systems operable in the ultrahigh vacuum range has taken place in the last three years. It is the purpose of this paper to explore the design considerations of ultrahigh vacuum systems for metallurgical applications.

A replica electron microscope study of as-polished and cathodically etched surfaces of pyrolytic carbon coating on fuel particles has been made in an attempt to characterize coatings that showed as much as a 30% difference in bult density. High and low density coating could be characterized by their polished surface textures; however, these features were not indicative of the true structure as seen by direct electron transmission. Microvoids detected by the transmission study of cleavage flakes exist on too fine a scale to be observed either optically or by electron microscope examination of replicas of the polished surface. Other features such as the effect of cathodic and chemical etching, coating delamination, and duplex coating interfaces have also been examined.

In a sense, the whole process of differentiation is one of directed functional mosaicism. It is, however, the accidental or random juxtaposition in the same organism of cells having actually or effectively different genotypes that is generally thought of as true mosaicism. The study of this condition constitutes a perfect meeting place for the fields of genetics and developmental biology, providing, as it does, interrelated information on mutability, cell lineage (including the special problems of cell lineage of the germ line), and the effect of genotype on part of the organism versus the whole. The discovery in recent years that most or all of one X chromosome of the normal mammalian female become randomly inactivated early in development, an event that leads to functional mosaicism, provides us with a great potential tool for the study of gene action. The present paper will attempt to bring together results of diverse observations and experiments (many of them as yet unpublished) bearing on both genetic and functional mosaicism in the mouse.

To properly assess the "sensitivity" of explosives systems under impact conditions we must obtain detailed information on these mechanisms by which explosives are ignited by impact. It is necessary to know which impact conditions represent the greatest hazard to explosive materials, as well as to know for a given impact condition the relative responses of explosives of interest. I should like to describe to you a program sponsored jointly by the Department of Defense and the Atomic Energy Commission to attain this type of information. A wide variety of impact experiments have been conducted using geometrical arrangements of explosive, plastic, and metal which are relatively simple compared to complete ordnance systems. All of these tests have employed billets of explosive fabricated by standard production techniques, and the billets have been sufficiently large that ignition, once started, has something of the same opportunity to grow or decay as in full scale ordnance assemblies. From these relatively simple tests there has accrued much new useful information on the behavior of explosives under impact. With this new information providing a base from which to work, it is hoped that theoretical calculations on impact phenomena will in the future make a bigger contribution to …

In the course of modern physics research, the need frequently arises for storage of large quantities of electrical energy which can be periodically discharged at high peak power into a load. Until recently, the homopolar machine has been an intriguing device having considerable academic interest but little practical value. In recent years, successful machines have been developed to utilize liquid-metal brush systems. The liquid-metal brush overcomes all the problems associated with current collection power loss, frictional loss, and limiting peripheral velocity. Consequently, these machines are now worth serious consideration where high-current dc generation is required. The main purpose in setting up a homopolar generator test program was to establish the limits to which an essentially standard commercially available generator of this type could be pushed.

First paragraph of report: M. Neumann and H. Sherrard reported the development of a wire spark chamber experiment toward receiving digitized spark information. Since late 1962 our effort has been directed toward a wire-chamber with a core memory, using standard ferrite cores, and toward an on-line operation between spark chamber and computer.

Abstract: The exhibit shows that colloidal aggregates (10 to 20 mu) of human serum albumin I131 may be used safely by intravenous injection to perform photoscans of the heart, liver, spleen, stomach, and salivary glands in man. Large particle size suspensions (10 to 50 mu) of the same material are being investigated experimentally in animals for scanning the lungs after intravenous injection and the brain following injection into an internal carotid artery. The advantages of this test material are the relatively low radiation exposure to the target organs and the number of organs that may be examined. Radiation exposure is low because of the rapid turnover in the target organs and removal from the body, mainly by urinary excretion, within 72 hours. The mechanism of liver-spleen localization with this organic colloid is the same as for inorganic colloidal radiogold198, namely, rapid removal from the blood by the phagocytic cells of the liver and spleen. However, in contrast to the inorganic colloid, which remains in the phagocytic cells permanently, albumin is digested by proteolytic enzymes and the I131 abel is set free to re-enter the general circulation. With the thyroid blocked, the I131 is excreted mainly in the urine as free …

Task A: Modification and Preparation of Experimental Facility. Facility engineering and layout is about seventy-five percent complete. Task B: Design and Construction of Test Sections. The major dimensions and characteristics of the metal and glass test sections have been calculated. One feasibility test of the electrically conducting coating on samples of glass tubing has been completed. Task C: Design and Construction of Test Stand, Task E: Pressure and Temperature Instrumentation for Test Section and Task F: Power Supply for Test Section. Preliminary engineering has been initiated on these tasks. The planned approach has been defined in each case. For Task E the transducer specifications have been defined and quotations on and/or sample units of the transducers have been requested. Tasks C and F can proceed with detailing as soon as drafting on Task B is about 50 percent complete. This point is scheduled to be reached during the first part of July. Task D: Void Fraction Instrumentation. The requirements for the x-ray instrumentation have been considered in the course of Task B and the x-ray power supply is presently on hand. The detailed engineering effort on this task is not scheduled to begin before July.

Abstract. The rate constants for the reaction of the hydrated electron eaq with a number of solutes and with radicals formed in water radiolysis are reported. Hydrated electrons were formed in the electron pulse irradiated solutions at concentrations in the range from 1 to 10 pM. Their reaction was followed by the decay of the optical absorption of eaq at 5780 A. Generally a 04 psec pulse of 15 MeV electrons was used. In the absence of eaq scavengers, second-order kinetics prevailed owing to the dominance of the reactions,eaq+eaq, eaq+H, and eaq+H202 when OH radical scavengers were present in alkaline solution. An analysis of the decay curves leads to values for keaq+eaq and keaq+H of 0.9~ 1010 and 3 x 1010 M-1 sec-1, respectively. With scavenger present in excess over [eaq], pseudo first-order kinetics were found and rate constants for a number of inorganic and organic compounds are reported. The agreement of these and other rate constants with diffusion-controlled reaction theory is discussed.

Abstract. By means of the pulse radiolysis technique a short-lived transient species has been observed in irradiated de-aerated ethanol and methanol, exhibiting an optical absorption throughout the visible and near infra-red. This transient is suggested to be the solvated electron on the basis of the nature of the spectrum, the reactivity with hydrogen ion and with various organic electron acceptors, and the formation of mononegative ions of some of these acceptors. The absolute rate constants have been determined for the reactions of the solvated electron with hydrogen ion, oxygen and benzyl chloride in ethanol and methanol. The diphenylide ion was found to be short-lived in ethanol. The absolute rate constant for the first-order decay of the diphenylide ion has been determined.

The following quarterly report covers the period during February 16 to May 15, 1963. This report is divided into sections covering the separate activities during this period, studying the thermal behavior of the F-center in RbCl.

Abstract. An a priori calculation of the radiolysis of oxygen gas in the pressure ; range 10-3 to 100 atm has been made. In the low background region (1- 100 atm) all track effects have been considered. The calculated G(O3) values seem to be in reasonable agreement with experiment if only one excited oxygen molecule is initially formed per ion pair. Effects of pressure, LET and dose rate have been discussed. The radiation-induced chain decomposition of O3 has not been considered.

Quarterly progress report on Accurate Nuclear Fuel Burnup Analysis project.

A potential performance limitation of superheat fuel is the susceptibility of the fuel cladding to low cycle fatigue failure. Two simplified analytical methods are presented to estimate the cyclic lifetime of circular superheat fuel cladding. One failure relation is based on a displacement method. The other failure relation is based on a stress method. These relations were compared with data from the literature, and with data involving damage obtained by Reynolds. A recommended design procedure involving the relations is presented. The technique was applied to the SADE 4B experiment with moderate success. These cycling relations involve only mechanical damage imposed by cycling, with a modification for additional damage caused by radiation; they do not include any other potential performance limiting mechanisms, such as stress corrosion, which are normally factored into the over-all fuel design. This work work done under Task C (Materials Development) of the Nuclear Superheat Project, AEC Contract AT(04-3)-189 - Project Agreement 13.

Data relating to the binary and ternary systems involving beryllium oxide are presented . The survey deals with all available literature up to December 1962.

Tests were run at the General Electric Company, Atomic Power Equipment Department, to determine the burnout conditions for a non-uniformly heated rod in an annular geometry.

A process was developed in which stainless steel-clad UO2 fuel rods are fabricated by high-temperature coextrusion. The process has a potential of being a more economical method for the preparation of stainless steel-clad UO2 fuel rods than the conventional pellet process. Consequently, it was considered advantageous to evaluate the irradiation characteristics of fuel rods fabricated in this manner. Therefore, 24 coextruded fuel rods were manufactured for evaluation in a reactor. The required amounts of UO2 and clad were soaked in separate containers at 1875 and 760 degree C, respectively. The containers were removed from their respective furnaces and were coextruded in one pass. A force of 450 to 475 tons was used, and a reduction ratio of 18 to 1 was obtained. The coextruded rods were cut to the approximate length, and the ends were sealed with an acid-resistant tape. The carbon steel can covering the stainless steel clad was removed by immersion in 1:1 nitric acid for 20 minutes. The rods were visually inspected, the specified lengths of clad and fuel were obtained by machining, and the correct diameter was obtained by belt sanding. The fabrication of the fuel rods was completed by inserting the plenum support tubes and …

This report summarises all the results obtained to date from a programme on the effects of neutron irradiation on the properties of beryllium metal. Results are presented on changes in density and mechanical properties in material fabricated by various routes and irradiated to fast neutron doses from 1019 nvt to 6 x 1023 nvt and at temperatures in the range 75ºC — 700ºC, Summaries of electron microscopy observations and electrical resistivity measurements, which are reported in more detail elsewhere., are also given, It is concluded that all the observed property changes can be interpreted in terms of the distribution of helium which is produced by fast neutron transmutation reactions in beryllium and that damage due to defect production is negligible for irradiation temperatures of 75ºC and above. Density changes duetoheiium bubble formation are shown to be very small but serious deterioration of mechanical properties can occur. The mechanical property changes and the distribution of helium are shown to be very dependent on material history and on the irradiation temperature. The standard Lucas Heights hot extruded material is shown to retain good mechanical properties for irradiation temperatures above 550ºC but serious loss of low temperature ductility is found to occur for …

The diffusion length of thermal neutrons in beryllium oxide of effective density 2.86 g cm-3 has been measured as 29.9 +- 0.8 cm. Using published experimental values for the diffusion constant of beryllium oxide, a value of [sigma] a = 9.0 +- 0.5 mb is deduced for the effective 2200m/s microscopic absorption cross-section.

Introduction: The object of Project Agreement 22, Task 1, is to develop improved detectors which can operate up to 1000 F for in-core power monitoring. Several ideas have been developed to achieve this goal: (1) root mean square fluctuation voltage measurement of ion chamber signals, (2) thermocouple-type detectors, and (3) fabrication developments.