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Prediction of Corrosion of Alloys in Mixed-Solvent Environments
Corrosion is much less predictable in organic or mixed-solvent environments than in aqueous process environments. As a result, US chemical companies face greater uncertainty when selecting process equipment materials to manufacture chemical products using organic or mixed solvents than when the process environments are only aqueous. Chemical companies handle this uncertainty by overdesigning the equipment (wasting money and energy), rather than by accepting increased risks of corrosion failure (personnel hazards and environmental releases). Therefore, it is important to develop simulation tools that would help the chemical process industries to understand and predict corrosion and to develop mitigation measures. To create such tools, we have developed models that predict (1) the chemical composition, speciation, phase equilibria, component activities and transport properties of the bulk (aqueous, nonaqueous or mixed) phase that is in contact with the metal; (2) the phase equilibria and component activities of the alloy phase(s) that may be subject to corrosion and (3) the interfacial phenomena that are responsible for corrosion at the metal/solution or passive film/solution interface. During the course of this project, we have completed the following: (1) Development of thermodynamic modules for calculating the activities of alloy components; (2) Development of software that generates stability diagrams …
Date:
June 5, 2003
Creator:
A. Anderko, P. Wang, R. D. Young, D. P. Riemer, P. McKenzie and M. M. Lencka (OLI Systems Inc.) & Laboratory), S. S. Babu and P. Angelini (Oak Ridge National
System:
The UNT Digital Library
Systematics of Fission-Product Yields
None
Date:
May 5, 2002
Creator:
A.C.Wahl
System:
The UNT Digital Library
INCONEL 690 CORROSION IN WTP (WASTE TREATMENT PLANT) HLW (HIGH LEVEL WASTE) GLASS MELTS RICH IN ALUMINUM & BISMUTH & CHROMIUM OR ALUMINUM/SODIUM
Metal corrosion tests were conducted with four high waste loading non-Fe-limited HLW glass compositions. The results at 1150 C (the WTP nominal melter operating temperature) show corrosion performance for all four glasses that is comparable to that of other typical borosilicate waste glasses, including HLW glass compositions that have been developed for iron-limited WTP streams. Of the four glasses tested, the Bi-limited composition shows the greatest extent of corrosion, which may be related to its higher phosphorus content. Tests at higher suggest that a moderate elevation of the melter operating temperature (up to 1200 C) should not result in any significant increase in Inconel corrosion. However, corrosion rates did increase significantly at yet higher temperatures (1230 C). Very little difference was observed with and without the presence of an electric current density of 6 A/inch{sup 2}, which is the typical upper design limit for Inconel electrodes. The data show a roughly linear relationship between the thickness of the oxide scale on the coupon and the Cr-depletion depth, which is consistent with the chromium depletion providing the material source for scale growth. Analysis of the time dependence of the Cr depletion profiles measured at 1200 C suggests that diffusion of Cr …
Date:
November 5, 2009
Creator:
AA, KRUGER; Z, FENG; H, GAN & IL, PEGG
System:
The UNT Digital Library
Infiltration Heat Recovery in Building Walls: Computational Fluid Dynamics Investigations Results
Conventional calculations of heating (and cooling) loads for buildings assume that conduction heat loss (or gain) through walls is independent of air infiltration heat loss (or gain). During passage through the building envelope, infiltrating air substantially exchanges heat wall insulation leading to partial recovery of heat conducted through the wall. The Infiltration Heat Recovery (IHR) factor was introduced to quantify the heat recovery and correct the conventional calculations. In this study, Computational Fluid Dynamics was used to calculate infiltration heat recovery under a range of idealized conditions, specifically to understand factors that influence it, and assess its significance in building heat load calculations. This study shows for the first time the important effect of the external boundary layers on conduction and infiltration heat loads. Results show (under the idealized conditions studied here) that (1) the interior details of the wall encountered in the leakage pa th (i.e., insulated or empty walls) do not greatly influence the IHR, the overall relative location of the cracks (i.e., inlet and outlet locations on the wall) has the largest influence on the IHR magnitude, (2) external boundary layers on the walls substantially contribute to IHR and (3) the relative error in heat load calculations …
Date:
August 5, 2002
Creator:
Abadie, Marc O.; Finlayson, Elizabeth U. & Gadgil, Ashok J.
System:
The UNT Digital Library
Electricity: The Road Toward Restructuring
The Public Utility Holding Company Act of 1935 (PUHCA) and the Federal Power Act (FPA) were enacted to eliminate unfair practices and other abuses by electricity and gas holding companies by requiring federal control and regulation of interstate public utility holding companies. Comprehensive energy legislation has passed the House and Senate. The House passed H.R. 6 on April 11, 2003. On July 31, 2003, the Senate suspended debate on S. 14, inserted the text of H.R. 4 (107th Congress) as a substitute, and passed H.R. 6. A conference agreement was reached November 17, 2003, and passed by the House the next day. H.R. 6 includes an electricity title that would, in part, repeal PUHCA, would prospectively repeal the mandatory purchase requirement under PURPA, and would create an electric reliability organization. On June 15, 2004, H.R. 4503, a comprehensive energy policy bill, passed the House.
Date:
June 5, 2002
Creator:
Abel, Amy & Parker, Larry
System:
The UNT Digital Library
A Low Cost Experimental Neutron Chain Reactor Part 2
Description of cooling, shielding, controls are discussed for 100 kw and 1 Mw operation of a low cost experimental neutron chain reactor.
Date:
February 5, 1954
Creator:
Abernathy, Fred H.; Barrett, Lawrence G.; Berger, William A.; Dever, John A.; Maurer, John F.; Mesler, Russell B. et al.
System:
The UNT Digital Library
Discovery of Very High Energy Gamma Rays from PKS 1424+240 and Multiwavelength Constraints on its Redshift
We report the first detection of very-high-energy (VHE) gamma-ray emission above 140GeV from PKS 1424+240, a BL Lac object with an unknown redshift. The photon spectrum above 140GeV measured by VERITAS is well described by a power law with a photon index of 3.8 {+-}0.5{sub stat} {+-} 0.3{sub syst} and a flux normalization at 200 GeV of (5.1 {+-} 0.9{sub stat} {+-} 0.5{sub syst}) x 10{sup -11} TeV{sup -1} cm{sup -2} s{sup -1}, where stat and syst denote the statistical and systematical uncertainty, respectively. The VHE flux is steady over the observation period between MJD 54881 and 55003 (2009 February 19 to June 21). Flux variability is also not observed in contemporaneous high energy observations with the Fermi Large Area Telescope (LAT). Contemporaneous X-ray and optical data were also obtained from the Swift XRT and MDM observatory, respectively. The broadband spectral energy distribution (SED) is well described by a one-zone synchrotron self-Compton (SSC) model favoring a redshift of less than 0.1. Using the photon index measured with Fermi in combination with recent extragalactic background light (EBL) absorption models it can be concluded from the VERITAS data that the redshift of PKS 1424+240 is less than 0.66.
Date:
April 5, 2012
Creator:
Acciari, V. A.; Aliu, E.; Arlen, T.; Aune, T.; Bautista, M.; Beilicke, M. et al.
System:
The UNT Digital Library
Biological Conversion of Synthesis Gas
Syngas is known to contain approximately 1 percent H[sub 2]S, along with CO[sub 2], C0[sub 2], H[sub 2] and CH[sub 4]. Similarly, the syngas may become contaminated with oxygen, particularly during reactor start-up and during maintenance. Previous studies with the water-gas shift bacterium Rhodospirillum rubrum have shown that the bacterium is tolerant of small quantities of oxygen, but the effects of oxygen on CO-consumption are unknown. Similarly, R. rubrum is known to be tolerant of H[sub 2]S, with high concentrations of H[sub 2]S negatively affecting CO-uptake. Batch experiments were thus carried out to determine the effects of H[sub 2]S and O[sub 2] on CO-uptake by R. rubrum. The results of these experiments were quantified by using Monod equations modified by adding terms for CO, H[sub 2]S and O[sub 2] inhibition. The techniques used in determining kinetic expressions previously shown for other gas-phase substrate bacterial systems including R. rubrum were utilized.
Date:
January 5, 1993
Creator:
Ackerson, M. D.; Clausen, E. C. & Gaddy, J. L.
System:
The UNT Digital Library
Biological Conversion of Synthesis Gas. Project Status Report, October 1, 1992--December 31, 1992
Syngas is known to contain approximately 1 percent H{sub 2}S, along with CO{sub 2}, C0{sub 2}, H{sub 2} and CH{sub 4}. Similarly, the syngas may become contaminated with oxygen, particularly during reactor start-up and during maintenance. Previous studies with the water-gas shift bacterium Rhodospirillum rubrum have shown that the bacterium is tolerant of small quantities of oxygen, but the effects of oxygen on CO-consumption are unknown. Similarly, R. rubrum is known to be tolerant of H{sub 2}S, with high concentrations of H{sub 2}S negatively affecting CO-uptake. Batch experiments were thus carried out to determine the effects of H{sub 2}S and O{sub 2} on CO-uptake by R. rubrum. The results of these experiments were quantified by using Monod equations modified by adding terms for CO, H{sub 2}S and O{sub 2} inhibition. The techniques used in determining kinetic expressions previously shown for other gas-phase substrate bacterial systems including R. rubrum were utilized.
Date:
January 5, 1993
Creator:
Ackerson, M. D.; Clausen, E. C. & Gaddy, J. L.
System:
The UNT Digital Library
Microstructural dependence of cavitation damage in polycrystalline materials. Final report, 1 November 1992--31 October 1994
Microstructure of a sample of Inconel X-750 damaged by ISCC (intergranular stress corrosion cracking) was examined after fatigue precracking in a high-temperature environment of deaerated water. Orientation imaging microscopy was used to reveal the microstructure adjacent to the crack path. General high-angle boundaries were found to be most susceptible to cracking. An ordering of the susceptibilities to ISCC damage was proposed; all boundaries have been classified into one of 12 categories. A model is proposed to predict the crack path for ISCC based on ex situ record of damage probabilities. The cracking is modeled as a Markov chain on a regular hexagonal array of grain boundaries representing the connectivity of the network.
Date:
February 5, 1996
Creator:
Adams, B.L.
System:
The UNT Digital Library
Tank Characterization Report for Single Shell Tank (SST) 241-TX-118
None
Date:
May 5, 2000
Creator:
Adams, M. R.
System:
The UNT Digital Library
Recovery of Uranium From Fiberglass Air Filters
Abstract: Various procedures for extracting uranium from fiberglass air filters have been tested and compared. Satisfactory results which involve the least amount of handling are obtained by simply washing the material with hot 1:1 hydrochloric acid.
Date:
August 5, 1946
Creator:
Adams, R. H.; Rogers, J. A. & Brown, K. B.
System:
The UNT Digital Library
Attrition Resistant Fischer-Tropsch Catalysts Based on FCC Supports
Commercial spent fluid catalytic cracking (FCC) catalysts provided by Engelhard and Albemarle were used as supports for Fe-based catalysts with the goal of improving the attrition resistance of typical F-T catalysts. Catalysts with the Ruhrchemie composition (100 Fe/5 Cu/4.2 K/25 spent FCC on mass basis) were prepared by wet impregnation. XRD and XANES analysis showed the presence of Fe{sub 2}O{sub 3} in calcined catalysts. FeC{sub x} and Fe{sub 3}O{sub 4} were present in the activated catalysts. The metal composition of the catalysts was analyzed by ICP-MS. F-T activity of the catalysts activated in situ in CO at the same conditions as used prior to the attrition tests was measured using a fixed bed reactor at T = 573 K, P = 1.38 MPa and H{sub 2}:CO ratio of 0.67. Cu and K promoted Fe supported over Engelhard provided spent FCC catalyst shows relatively good attrition resistance (8.2 wt% fines lost), high CO conversion (81%) and C{sub 5}+ hydrocarbons selectivity (18.3%).
Date:
February 5, 2010
Creator:
Adeyiga, Adeyinka
System:
The UNT Digital Library
Reduction of oxides of nitrogen exposures at pickling operation, 313 Building, 300 area
None
Date:
December 5, 1949
Creator:
Adley, F. E.
System:
The UNT Digital Library
Carbon transport in the bottom boundary layer. Final report
This report summarizes the activities and findings from a field experiment devised to estimate the rates and mechanisms of transport of carbon across the continental shelves. The specific site chosen for the experiment was the mid-Atlantic Bight, a region off the North Carolina coast. The experiment involved a large contingent of scientists from many institutions. The specific component of the program was the transport of carbon in the bottom boundary layer. The postulate mechanisms of transport of carbon in the bottom boundary layer are: resuspension and advection, downward deposition, and accumulation. The high turbulence levels in the bottom boundary layer require the understanding of the coupling between turbulence and bottom sediments. The specific issues addressed in the work reported here were: (a) What is the sediment response to forcing by currents and waves? (b) What is the turbulence climate in the bottom boundary layer at this site? and (c) What is the rate at which settling leads to carbon sequestering in bottom sediments at offshore sites?
Date:
October 5, 1998
Creator:
Agrawal, Yogesh C.
System:
The UNT Digital Library
Trade and the Americas
None
Date:
March 5, 2002
Creator:
Ahearn, Raymond J.
System:
The UNT Digital Library
Trade Primer: Qs and As on Trade Concepts, Performance, and Policy
The 112th Congress has a full legislative and oversight agenda on international trade. The agenda may include considering legislation to implement pending free trade agreements with Panama, South Korea, and Colombia, enhanced enforcement of U.S. trade agreements, as well as oversight of the World Trade Organization's Doha Round and trade relations with China. This report provides information and context for many of these topics. The report is divided into four sections in a question-and-answer format: trade concepts, U.S. trade performance, formulation of U.S. trade policy, and trade and investment issues.
Date:
January 5, 2011
Creator:
Ahearn, Raymond J.
System:
The UNT Digital Library
Exploring Prompt Measurement Methods for (n,2n) Cross Sections on Radioactive Targets
This report summarizes a study of possible neutron detection technologies for performing prompt (n,2n) measurements on radioactive targets of the type that could be made at the Rare Isotope Accelerator (RIA). The report recommends conducting further research on high-pressure {sup 3}He gas scintillators as it is the best candidate technology. These detectors meet the requirements of a fast response time (fall times around 5-10 ns), gamma ray suppression, (all gamma rays below about 900 keV can be easily discriminated against), and can be easily configured into a 4{pi} array. The one requirement that these detectors fall short is efficiency, but less than a factor of 10 improvement is needed. The possibility of pulse shape discrimination should also be explored for these detectors as this would help to distinguish gamma rays above 900 keV from neutrons. In addition to R&D work on these detectors, Monte Carlo simulations and target development are also recommended areas of further study.
Date:
January 5, 2006
Creator:
Ahle, L.
System:
The UNT Digital Library
San Francisco State University IAC 02-06 Final Report
The Industrial Assessment Center (IAC) at San Francisco State University (SFSU) has served the cause of energy efficiency as a whole, and in particular for small and medium-sized manufacturing facilities in northern and central California, within a approximately 150 miles (radial) of San Francisco since 1992. In the current reporting period (September 1, 2002 through November 31, 2006) we have had major accomplishments, which include but are not limited to: - Performing a total of 94 energy efficiency and waste minimization audit days of 87 industrial plants - Recommending and analysis of 809 energy efficiency measures - Training 22 energy engineers, most of whom have joined energy services companies in California. - Disseminating energy efficiency information among local manufacturers - Acting as an information source for energy efficiency for local manufacturers and utilizes - Cooperating with local utilities and California Energy Commission in their energy efficiency projects - Performing various assignments by DOE such as dissemination of information on SEN initiative, conducting workshops on energy efficiency issues, contacting large energy user plants - Establishing a course on “Energy: Resources, Alternatives and Conservation” as a general education course at SFSU - Bringing energy issues to the attention of students in classrooms
Date:
March 5, 2007
Creator:
Ahmad R. Ganji, Ph.D., P.E., IAC DIrector
System:
The UNT Digital Library
Seeing the Nature of the Accelerating Physics: It's a SNAP
For true insight into the nature of dark energy, measurements of the precision and accuracy of the Supernova/Acceleration Probe (SNAP) are required. Precursor or scaled-down experiments are unavoidably limited, even for distinguishing the cosmological constant. They can pave the way for, but should not delay, SNAP by developing calibration, refinement, and systematics control (and they will also provide important, exciting astrophysics).
Date:
August 5, 2005
Creator:
Albert, J.; Aldering, G.; Allam, S.; Althouse, W.; Amanullah, R.; Annis, J. et al.
System:
The UNT Digital Library
Sample Proficiency Test exercise
The current format of the OPCW proficiency tests has multiple sets of 2 samples sent to an analysis laboratory. In each sample set, one is identified as a sample, the other as a blank. This method of conducting proficiency tests differs from how an OPCW designated laboratory would receive authentic samples (a set of three containers, each not identified, consisting of the authentic sample, a control sample, and a blank sample). This exercise was designed to test the reporting if the proficiency tests were to be conducted. As such, this is not an official OPCW proficiency test, and the attached report is one method by which LLNL might report their analyses under a more realistic testing scheme. Therefore, the title on the report ''Report of the Umpteenth Official OPCW Proficiency Test'' is meaningless, and provides a bit of whimsy for the analyses and readers of the report.
Date:
February 5, 2006
Creator:
Alcaraz, A.; Gregg, H. & Koester, C.
System:
The UNT Digital Library
FACT (Version 2.0) - Subsurface Flow and Contaminant Transport Documentation and User's Guide
This report documents a finite element code designed to model subsurface flow and contaminant transport, named FACT. FACT is a transient three-dimensional, finite element code designed to simulate isothermal groundwater flow, moisture movement, and solute transport in variably saturated and fully saturated subsurface porous media.
Date:
May 5, 2000
Creator:
Aleman, S. E.
System:
The UNT Digital Library
Volume reduction system for solid and liquid TRU waste from the nuclear fuel cycle: January--March 1978
The laboratory cyclone incinerator, which started operation in January, 1978, has been developed to study the effects of burning feed containing radionuclides other than /sup 238/Pu. These isotopes must be removed from the off-gas during incineration. Preliminary data from early runs show that the combustion efficiency of the incinerator can still be improved. Controlled experiments were conducted on the pressed ash-cement pellet matrix to define compressive strength, mechanical stability, density, and effect of curing environment (wet cure and dry cure). Leachability studies were initiated on pressed sludge/cement matrix in distilled water at ambient temperature. Compressive strengths of sludge/cement pressed matrix samples were investigated. Physical and chemical attributes of incinerated ash were evaluated in relationship to the ash/cement matrix. 7 figs., 6 tables.
Date:
May 5, 1978
Creator:
Alexander, B.M.; Batchelder, D.A.; Doty, J.W. & Lewis, E.L.
System:
The UNT Digital Library
The Wild and Scenic Rivers Act and Federal Water Rights
This report discusses federal authority over water, and federal "reserved" and non-reserved water rights. Based on the language of the act and its legislative history, it appears that the act creates federal water rights. The act does not specify the quantity of the right. The amount of the federal right is likely to vary from river to river depending on the river's flows, the unappropriated flows in the river at the time of designation, and the values for which the river is being protected.
Date:
March 5, 2007
Creator:
Alexander, Kristina
System:
The UNT Digital Library