A report discussing an experiment conducted to determine the effect of radiation on the melting point of Tempilaq, a commercially available, temperature-indicating liquid.

This technical report provides supplementary information on the Brookhaven nuclear reactor. It details added safety systems, tests, expounds on information included in the original report, describes liquid wastes system, and describes different procedures for operating the nuclear reactor.

Technical report. Three extractions of a diethyl ether solution of uranyl nitrate with small portions of water are effective in removing rare earths, as is shown by radio-gadolinium and radio-europium tracer experiments. A study of representative ethers, alcohols, ketones, and esters showed that diethyl ether and a mixture of 85% ethyl methyl ketone with 15% xylene are the best solvents for the extraction.

Technical report containing short reports on (1) Mass spectrometer studies; (2) Purification of heavy water; and (3) Equilibration studies.

Technical report abstract. A rapid procedure for the preparation of very pure carrier-free Zr and Nb tracer involves the chloroform extraction of the cupferrides of Zr and Nb activities from process solutions. Zr and Nb form very stable chloroform soluble cupferrides in acid solutions (CK-993) and are separated from other fission elements almost quantitatively to yield pure mixture of Zr and Nb activity. A minimum of operations is required and the method is easily adaptable to remote control.

Abstract. the electrodeposition of uranium metal, in the form of tree-like deposits, from molten strontium halide baths is described. Under the best conditions studied, approximately 40% recovery is attained. Freedom from side-reactions of the reduced uranium with anode products and/or refractory materials, and high cathode current densities appear to be essential to the success of the process. the refining of uranium under similar conditions appears to occur quite readily, with approximately 50% current efficiency. The preparation of UI3 is also described.

Abstract. A satisfactory method has been found for dissolving thorium metal and thorium oxide in heat-treated 25-12 stainless steel vessels without excessive corrosion of the vessels. The dissolution medium consists of strong HNO3 containing a small amount of fluoride or fluo-silicate. the fluoride required has no harmful effects on a subsequent solvent-extraction step for a separation of uranium isotopes from the dissolved thorium.

The following documents were compiled into a quarterly report that was to be published in the Radiobiology Volume of the PPR. The following reports provide data from the Biology department of the University of Chicago between May and August of 1947.

Abstract: "Samples of dust are collected from the atmosphere with a Mine Safety Appliance Co. electrostatic precipitator and analyzed for uranium by means of a dropping mercury electrode apparatus. Two to three micrograms of uranium can be detected in a cell solution volume of 1 ml. Iron, nickel and chromium present in shop dusts do not interfere. Copper may interfere if present in excess but may be removed by a sulfide precipitation. Directions for preparation of cell solution and operation of the Polarograph are given. The polarographic method described may be used for determination of uranium in samples other than atmospheric dusts."

Abstract: "The heat of solution of UCl4 solid has been measured and found to change appreciably with changing concentration of H+ or ionic strength. The heat of hydrolysis of U+4 to form UOH+3 is probably of the order of +11 kcal per mole" (p. 1).

Abstract: "Several chemical and physical characteristics of over seven hundred charges are computing with their performance in the process units. No correlation is attainable."

From introduction: "This study is concerned with the shape of the electrodes of high-voltage insulator and with the method of joining them to the dielectric. The study is limited to insulators operating in vacuum, with special interest in the cases where strong magnetic fields are present. It is further limited to insulators with the high-voltage electrodes maintained at negative potential. The object of the study was to obtain information that would aid in improving the design of the insulators in two respects. First, to decrease to a minimum the number of charged particles set free which may directly or indirectly cause early failure of the insulator. Second, to increase the voltages at which partial or complete flashovers occur. Therefore, experiments were made to determine the principal phenomenon which have as their primary source the insulator under high electrical stress in vacuum."

The following document presents designs and blueprints to the bubble-cap column built to replace a nitric acid concentrator.

This report discusses an analysis on the exchange reaction between iodine and unipositive iodine with pyridine.

From introduction: "The present report covers the results of an extended investigation of magnesium oxychloride cements and concretes. In this study the effects of the composition of the cement or concrete on its physical and mechanical properties were determined. In addition, the stability of the mixes was observed."

Report discussing specifications for the design of a waste heat steam boiler "for the purpose of generating steam to operate a condensing steam turbine electric generator from the clean hot radioactive air that has cooled the atomic energy reactor of [a] laboratory under a pressure less than atmospheric."

Abstract: "The need often arises for determining the critical chemical concentration of uranium solution in the conical bottom of a plant reactor or storage vessel, or the dimension if the concentration is known. This report describes the mathematical analysis of Poisson's equation for a spherical sector, which approximates a right circular cone. The ratio of the critical dimension of an equivalent sphere to the height of the sector for various sector angles is derived from a comparison of first eigenvalues. No description of further relations between composition and dimensions is discussed in the report."

The following report describes an experiment on the aluminum nitrate process for the conversion of tuballoy tetrafluoride to tuballoy peroxide and the solutions resulting.

The purpose of this report is to present a method of impregnating beryllium oxide with uranium and to describe the properties of beryllium oxide and of commercial beryllium oxide ceramics.

A report on the Sleepy Cat Mt. District in the White River Uplift Area.

From summary: "A method for the preparation of normal uranyl carbonate has been developed. Heretofore, this compound has been known only as a rare, naturally occurring material." The report further discusses the physical properties of the compound, its solubility in water, and its interaction with sodium carbonate.

Report discussing the properties and methods of forming ceramic bodies of alkaline earth and other refractory solids. These materials can be used for "reaction chambers, crucibles for melting metals, casting solids, insulation shields, thermocouple shields and other heat resistant bodies...High calcium lime was found to have the necessary chemical and thermal properties for many of the above uses."

This report for the month of July, 1949 discusses progress regarding work on the carbonate process and the recovery of uranium and vanadium from carbonate liquors.

Report discussing progress made by the National Research Corporation in developing preparation methods for ductile zirconium for the month of July, 1949.