Report discussing testing of a Hughes Falcon missile, C configuration, to determine the stability and control characteristics of the missile while rolling. Information about the time histories, normal force due to angle of attack, pitching moment due to angle of attack, damping, and control effectiveness is provided.

The development of ionic methods for the determination of corrosive products in the highly radioactive Homogeneous Reactor (HR) fuels has been of major interest in the work of the Ionic Analyses Laboratory. Methods for the spectrophotometric determination of aluminum and for the polarographic determination of iron in HR fuels have been developed. The polarographic determination of molybdenum in uranyl sulfate solutions was studied. A polarographic method for the determination of zinc was developed. A fluorometric method for the determination of microgram amounts of fluoride was studied. Three organic reagents were investigated as precipitants for microgram quantities of zirconium in HR fuel. The automatic photometric titration technique was applied to the determination of thorium and of sulfate. A method was developed for the ion-exchange separation and potentiometric titration of cobalt. The ultraviolet absorption spectra of technetium and rhenium were studied.

A study of the variables involved in regeneration was undertaken to determine means of improving the regeneration efficiency and increasing the useful life of a reactor. Information gained from regeneration studies on a 4-inch-diameter by 8-foot-high column indicates that the present regeneration procedure is optimum as to quantity, concentration, and rate of addition of regenerant solution. It appears feasible to restore a plugged reactor by washing off all the silver nitrate from the packing and recoating by a normal regeneration cycle. Such a procedure could be utilized only if there is sufficient dead space in the bottom of the reactor to hold the wash solution.

Calculated data and graphs describing the effects of batch thermal-neutron irradiation of thorium, the usual method of operation of heterogeneous reactors, are presented. The buildup and decay of U233, Pa233, other heavy isotopes, and fission products are considered on the basis of best available cross-section and fission-yield data. The effects of these irradiation products on the Thorex chemical separation process are indicated briefly.