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An Equation for the Anodic Stripping Curves of Thin Mercury Film Electrodes
None
Date:
June 25, 1965
Creator:
Roe, D. K. & Toni, J. E. A.
Object Type:
Report
System:
The UNT Digital Library
Raman Studies of Hydrido- and Deutero- Rhenium Tetracarbonyl Trimer
In a previous study the trimer of rhenium tetracarbonyl was found to be diamagnetic, suggesting the presence of hydrogen in the compound. This was supported by chemical analysis, which indicated about one hydrogen per rhenium, and the compound was formulated as [Re(C0)4H] 3• Subsequently a proton resonance was observed on a broad line spectrometer. In the original work the infrared spectra were compared for the hydride and deuteride; cyclohexane solutions were used for the CO stretching region and KBr discs were used for the rest of the spectrum. Surprisingly, the spectra of the hydride and deuteride showed only minor differences, insufficient to confirm the presence of hydrogen. No evidence of a hydrogen stretching frequency was found. In the present work, the previously unobserved Raman spectra were measured for the hydride and deuteride . In the solid state ratber striking shifts were observed in the CO stretching region. Also there is some evidence for a metal-hydrogen stretching band at the rather low frequency of 1100 cm-1. In an attempt to support the interpretation of the Raman spectra more detailed infrared studies of the solid in KBr discs were made. The hope was to observe a metal-hydrogen stretching frequency and to explain …
Date:
March 25, 1965
Creator:
Fellman, W.; Smith, J. Michael & Jones, L H
Object Type:
Report
System:
The UNT Digital Library
First single cluster corrosion test WANL hydrogen corrosion test facility
None
Date:
February 25, 1965
Creator:
Foster, R. D. & Gilchrist, M. C.
Object Type:
Report
System:
The UNT Digital Library
PERMEATION OF HYDROGEN THROUGH METALS
None
Date:
July 25, 1965
Creator:
Webb, R. W.
Object Type:
Report
System:
The UNT Digital Library
Hazards summary report, Supplement 3. Nuclear safety and operating limits: K Reactors
None
Date:
February 25, 1965
Creator:
Nilson, R. & Graves, S.M.
Object Type:
Report
System:
The UNT Digital Library
Evaluation of fuel particles
None
Date:
May 25, 1965
Creator:
Feild, A. L., Jr. & Brizes, W.F.
Object Type:
Report
System:
The UNT Digital Library