Operation of a Free-Electron Laser from the Extreme Ultraviolet to the Water Window (open access)

Operation of a Free-Electron Laser from the Extreme Ultraviolet to the Water Window

We report results on the performance of a free-electron laser operating at a wavelength of 13.7 nm where unprecedented peak and average powers for a coherent extreme-ultraviolet radiation source have been measured. In the saturation regime, the peak energy approached 170 {micro}J for individual pulses, and the average energy per pulse reached 70 {micro}J. The pulse duration was in the region of 10 fs, and peak powers of 10 GW were achieved. At a pulse repetition frequency of 700 pulses per second, the average extreme-ultraviolet power reached 20mW. The output beam also contained a significant contribution from odd harmonics of approximately 0.6% and 0.03% for the 3rd (4.6 nm) and the 5th (2.75 nm) harmonics, respectively. At 2.75 nm the 5th harmonic of the radiation reaches deep into the water window, a wavelength range that is crucially important for the investigation of biological samples.
Date: December 17, 2007
Creator: Ackermann, W.; Asova, G.; Ayvazyan, V.; Azima, A.; Baboi, N.; Bahr, J. et al.
Object Type: Article
System: The UNT Digital Library
SOFTWARE QUALITY ASSURANCE FOR EMERGENCY RESPONSE CONSEQUENCE ASSESSMENT MODELS AT DOE'S SAVANNAH RIVER SITE (open access)

SOFTWARE QUALITY ASSURANCE FOR EMERGENCY RESPONSE CONSEQUENCE ASSESSMENT MODELS AT DOE'S SAVANNAH RIVER SITE

The Savannah River National Laboratory's (SRNL) Atmospheric Technologies Group develops, maintains, and operates computer-based software applications for use in emergency response consequence assessment at DOE's Savannah River Site. These applications range from straightforward, stand-alone Gaussian dispersion models run with simple meteorological input to complex computational software systems with supporting scripts that simulate highly dynamic atmospheric processes. A software quality assurance program has been developed to ensure appropriate lifecycle management of these software applications. This program was designed to meet fully the overall structure and intent of SRNL's institutional software QA programs, yet remain sufficiently practical to achieve the necessary level of control in a cost-effective manner. A general overview of this program is described.
Date: December 17, 2007
Creator: Hunter, C
Object Type: Article
System: The UNT Digital Library
Stable SUSY breaking model with O(10) eV gravitino from combined D-term gauge mediation and U(1)' mediation (open access)

Stable SUSY breaking model with O(10) eV gravitino from combined D-term gauge mediation and U(1)' mediation

We show a calculable example of stable supersymmetry (SUSY) breaking modelswith O(10) eV gravitino mass based on the combination of D-term gauge mediationand U(1)' mediation. A potential problem of the negative mass squared for theSUSY standard model (SSM) sfermions in the D-term gauge mediation is solvedby the contribution from the U(1)' mediation. On the other hand, the splittingbetween the SSM gauginos and sfermions in the U(1)' mediation iscircumvented bythe contributions from the D-term gauge mediation. Since the U(1)' mediation doesnot introduce any new SUSY vacua, we achieve a completely stable model underthermal effects. Our model, therefore, has no cosmological difficulty.
Date: December 17, 2007
Creator: Nakayama, Yu & Nakayama, Yu
Object Type: Article
System: The UNT Digital Library
Magnetic Measurements and Simulations for a 4-magnet Dipole Chicane for the International Linear Collider (open access)

Magnetic Measurements and Simulations for a 4-magnet Dipole Chicane for the International Linear Collider

T-474 at SLAC is a prototype BPM-based energy spectrometer for the ILC. We describe magnetic measurements and simulations for the 4-magnet chicane used in T-474.
Date: December 17, 2007
Creator: Schreiber, H. J.; Viti, M.; /DESY; Duginov, V. N.; Kostromin, S. A.; Morozov, N. A. et al.
Object Type: Article
System: The UNT Digital Library
A celestial gamma-ray foreground due to the albedo of small solar system bodies and a remote probe of the interstellar cosmic ray spectrum (open access)

A celestial gamma-ray foreground due to the albedo of small solar system bodies and a remote probe of the interstellar cosmic ray spectrum

We calculate the {gamma}-ray albedo flux from cosmic-ray (CR) interactions with the solid rock and ice in Main Belt asteroids and Kuiper Belt objects (KBOs) using the Moon as a template. We show that the {gamma}-ray albedo for the Main Belt and Kuiper Belt strongly depends on the small-body mass spectrum of each system and may be detectable by the forthcoming Gamma Ray Large Area Space Telescope (GLAST). The orbits of the Main Belt asteroids and KBOs are distributed near the ecliptic, which passes through the Galactic center and high Galactic latitudes. If detected, the {gamma}-ray emission by the Main Belt and Kuiper Belt has to be taken into account when analyzing weak {gamma}-ray sources close to the ecliptic, especially near the Galactic center and for signals at high Galactic latitudes, such as the extragalactic {gamma}-ray emission. Additionally, it can be used to probe the spectrum of CR nuclei at close-to-interstellar conditions, and the mass spectrum of small bodies in the Main Belt and Kuiper Belt. The asteroid albedo spectrum also exhibits a 511 keV line due to secondary positrons annihilating in the rock. This may be an important and previously unrecognized celestial foreground for the INTErnational Gamma-Ray Astrophysics Laboratory …
Date: December 17, 2007
Creator: Moskalenko, Igor V.; Porter, Troy A.; Digel, Seth W.; Michelson, Peter F. & Ormes, Jonathan F.
Object Type: Article
System: The UNT Digital Library
A stable finite difference method for the elastic wave equation on complex geometries with free surfaces (open access)

A stable finite difference method for the elastic wave equation on complex geometries with free surfaces

The isotropic elastic wave equation governs the propagation of seismic waves caused by earthquakes and other seismic events. It also governs the propagation of waves in solid material structures and devices, such as gas pipes, wave guides, railroad rails and disc brakes. In the vast majority of wave propagation problems arising in seismology and solid mechanics there are free surfaces. These free surfaces have, in general, complicated shapes and are rarely flat. Another feature, characterizing problems arising in these areas, is the strong heterogeneity of the media, in which the problems are posed. For example, on the characteristic length scales of seismological problems, the geological structures of the earth can be considered piecewise constant, leading to models where the values of the elastic properties are also piecewise constant. Large spatial contrasts are also found in solid mechanics devices composed of different materials welded together. The presence of curved free surfaces, together with the typical strong material heterogeneity, makes the design of stable, efficient and accurate numerical methods for the elastic wave equation challenging. Today, many different classes of numerical methods are used for the simulation of elastic waves. Early on, most of the methods were based on finite difference approximations …
Date: December 17, 2007
Creator: Appelo, D & Petersson, N A
Object Type: Article
System: The UNT Digital Library
A Language for Specifying Compiler Optimizations for Generic Software (open access)

A Language for Specifying Compiler Optimizations for Generic Software

None
Date: December 17, 2007
Creator: Willcock, J J
Object Type: Thesis or Dissertation
System: The UNT Digital Library
Cost-Effective Cementitious Material Compatible with Yucca Mountain Repository Geochemistry (open access)

Cost-Effective Cementitious Material Compatible with Yucca Mountain Repository Geochemistry

The current plans for the Yucca Mountain (YM) repository project (YMP) use steel structures to stabilize the disposal drifts and connecting tunnels that are collectively over 100 kilometers in length. The potential exist to reduce the underground construction cost by 100s of millions of dollars and improve the repository's performance. These economic and engineering goals can be achieved by using the appropriate cementitious materials to build out these tunnels. This report describes the required properties of YM compatible cements and reviews the literature that proves the efficacy of this approach. This report also describes a comprehensive program to develop and test materials for a suite of underground construction technologies.
Date: December 17, 2004
Creator: Dole, LR
Object Type: Report
System: The UNT Digital Library
FLOWSHEET FOR ALUMINUM REMOVAL FROM SLUDGE BATCH 6 (open access)

FLOWSHEET FOR ALUMINUM REMOVAL FROM SLUDGE BATCH 6

Samples of Tank 12 sludge slurry show a substantially larger fraction of aluminum than originally identified in sludge batch planning. The Liquid Waste Organization (LWO) plans to formulate Sludge Batch 6 (SB6) with about one half of the sludge slurry in Tank 12 and one half of the sludge slurry in Tank 4. LWO identified aluminum dissolution as a method to mitigate the effect of having about 50% more solids in High Level Waste (HLW) sludge than previously planned. Previous aluminum dissolution performed in a HLW tank in 1982 was performed at approximately 85 C for 5 days and dissolved nearly 80% of the aluminum in the sludge slurry. In 2008, LWO successfully dissolved 64% of the aluminum at approximately 60 C in 46 days with minimal tank modifications and using only slurry pumps as a heat source. This report establishes the technical basis and flowsheet for performing an aluminum removal process in Tank 51 for SB6 that incorporates the lessons learned from previous aluminum dissolution evolutions. For SB6, aluminum dissolution process temperature will be held at a minimum of 65 C for at least 24 days, but as long as practical or until as much as 80% of the …
Date: December 17, 2008
Creator: Pike, J & Jeffrey Gillam, J
Object Type: Report
System: The UNT Digital Library
The Kinematics of Molecular Cloud Cores in the Presence of Driven and Decaying Turbulence: Comparisons with Observations (open access)

The Kinematics of Molecular Cloud Cores in the Presence of Driven and Decaying Turbulence: Comparisons with Observations

In this study we investigate the formation and properties of prestellar and protostellar cores using hydrodynamic, self-gravitating Adaptive Mesh Refinement simulations, comparing the cases where turbulence is continually driven and where it is allowed to decay. We model observations of these cores in the C{sup 18}O(2 {yields} 1), NH{sub 3}(1, 1), and N{sub 2}H{sup +}(1 {yields} 0) lines, and from the simulated observations we measure the linewidths of individual cores, the linewidths of the surrounding gas, and the motions of the cores relative to one another. Some of these distributions are significantly different in the driven and decaying runs, making them potential diagnostics for determining whether the turbulence in observed star-forming clouds is driven or decaying. Comparing our simulations with observed cores in the Perseus and {rho} Ophiuchus clouds shows reasonably good agreement between the observed and simulated core-to-core velocity dispersions for both the driven and decaying cases. However, we find that the linewidths through protostellar cores in both simulations are too large compared to the observations. The disagreement is noticeably worse for the decaying simulation, in which cores show highly supersonic in fall signatures in their centers that decrease toward their edges, a pattern not seen in the observed …
Date: December 17, 2007
Creator: Offner, S R; Krumholz, M R; Klein, R I & McKee, C F
Object Type: Article
System: The UNT Digital Library
Recent Developments in the MCNP-POLIMI Postprocessing Code (open access)

Recent Developments in the MCNP-POLIMI Postprocessing Code

The design and analysis of measurements performed with organic scintillators rely on the use of Monte Carlo codes to simulate the interaction of neutrons and photons, originating from fission and other reactions, with the materials present in the system and the radiation detectors. MCNP-PoliMi is a modification of the MCNP-4c code that models the physics of secondary particle emission from fission and other processes realistically. This characteristic allows for the simulation of the higher moments of the distribution of the number of neutrons and photons in a multiplying system. The present report describes the recent additions to the MCNP-PoliMi post-processing code. These include the simulation of detector dead time, multiplicity, and third order statistics.
Date: December 17, 2004
Creator: Pozzi, S.A.
Object Type: Report
System: The UNT Digital Library
Actinide Sorption in Rainier Mesa Tunnel Waters from the Nevada Test Site (open access)

Actinide Sorption in Rainier Mesa Tunnel Waters from the Nevada Test Site

The sorption behavior of americium (Am), plutonium (Pu), neptunium (Np), and uranium (U) in perched Rainier Mesa tunnel water was investigated. Both volcanic zeolitized tuff samples and groundwater samples were collected from Rainier Mesa, Nevada Test Site, NV for a series of batch sorption experiments. Sorption in groundwater with and without the presence of dissolved organic matter (DOM) was investigated. Am(III) and Pu(IV) are more soluble in groundwater that has high concentrations of DOM. The sorption K{sub d} for Am(III) and Pu(IV) on volcanic zeolitized tuff was up to two orders of magnitude lower in samples with high DOM (15 to 19 mg C/L) compared to samples with DOM removed (< 0.4 mg C/L) or samples with naturally low DOM (0.2 mg C/L). In contrast, Np(V) and U(VI) sorption to zeolitized tuff was much less affected by the presence of DOM. The Np(V) and U(VI) sorption Kds were low under all conditions. Importantly, the DOM was not found to significantly sorb to the zeolitized tuff during these experiment. The concentration of DOM in groundwater affects the transport behavior of actinides in the subsurface. The mobility of Am(III) and Pu(IV) is significantly higher in groundwater with elevated levels of DOM resulting …
Date: December 17, 2007
Creator: Zhao, P.; Zavarin, M.; Leif, R.; Powell, B.; Singleton, M.; Lindvall, R. et al.
Object Type: Report
System: The UNT Digital Library
Engineered and Administrative Safety Systems for the Control of Prompt Radiation Hazards at Accelerator Facilities (open access)

Engineered and Administrative Safety Systems for the Control of Prompt Radiation Hazards at Accelerator Facilities

The ANSI N43.1 Standard, currently in revision (ANSI 2007), sets forth the requirements for accelerator facilities to provide adequate protection for the workers, the public and the environment from the hazards of ionizing radiation produced during and from accelerator operations. The Standard also recommends good practices that, when followed, provide a level of radiation protection consistent with those established for the accelerator communities. The N43.1 Standard is suitable for all accelerator facilities (using electron, positron, proton, or ion particle beams) capable of producing radiation, subject to federal or state regulations. The requirements (see word 'shall') and recommended practices (see word 'should') are prescribed in a graded approach that are commensurate with the complexity and hazard levels of the accelerator facility. Chapters 4, 5 and 6 of the N43.1 Standard address specially the Radiation Safety System (RSS), both engineered and administrative systems, to mitigate and control the prompt radiation hazards from accelerator operations. The RSS includes the Access Control System (ACS) and Radiation Control System (RCS). The main requirements and recommendations of the N43.1 Standard regarding the management, technical and operational aspects of the RSS are described and condensed in this report. Clearly some aspects of the RSS policies and practices …
Date: December 17, 2007
Creator: Liu, James C.; Vylet, Vashek & Walker, Lawrence S.
Object Type: Article
System: The UNT Digital Library
Modeling of Carbon Tetrachloride Flow and Transport in the Subsurface of the 200 West Disposal Sites: Large-Scale Model Configuration and Prediction of Future Carbon Tetrachloride Distribution Beneath the 216-Z-9 Disposal Site (open access)

Modeling of Carbon Tetrachloride Flow and Transport in the Subsurface of the 200 West Disposal Sites: Large-Scale Model Configuration and Prediction of Future Carbon Tetrachloride Distribution Beneath the 216-Z-9 Disposal Site

Three-dimensional simulations considered migration of dense, nonaqueous phase liquid (DNAPL) consisting of CT and co disposed organics in the subsurface as a function of the properties and distribution of subsurface sediments and of the properties and disposal history of the waste. Simulations of CT migration were conducted using the Water-Oil-Air mode of Subsurface Transport Over Multiple Phases (STOMP) simulator. A large-scale model was configured to model CT and waste water discharge from the major CT and waste-water disposal sites.
Date: December 17, 2008
Creator: Oostrom, Mart; Thorne, Paul D.; Zhang, Z. F.; Last, George V. & Truex, Michael J.
Object Type: Report
System: The UNT Digital Library
West Valley Demonstration Project Annual Site Environmental Report Calendar Year 2007 (open access)

West Valley Demonstration Project Annual Site Environmental Report Calendar Year 2007

Annual Site Environmental Report for the West Valley Demonstration Project (WVDP) for Calendar Year 2007. The report summarizes the calendar year (CY) 2007 environmental protection program at the WVDP. Monitoring and surveillance of the facilities used by the DOE are conducted to verify protection of public health and safety and the environment.
Date: December 17, 2008
Creator: Division, West Valley Environmental Services LLC (WVES) and URS - Washington
Object Type: Report
System: The UNT Digital Library
Closeout Report Department of Energy Grant DE-FG02 95ER40931 Advanced Map Methods for the Description of Particle Beam Dynamics (open access)

Closeout Report Department of Energy Grant DE-FG02 95ER40931 Advanced Map Methods for the Description of Particle Beam Dynamics

The above grant was active at Michigan State University from 1994 until 2007. We summarize and document the various activities and key output under the grant, including degrees awarded to graduate students at MSU and through the VUBeam program sponsored by the grant, the books, publications and reports produced, the meetings organized, and the presentations given.
Date: December 17, 2008
Creator: Berz, Martin & Makino, Kyoko
Object Type: Report
System: The UNT Digital Library
Slant Path Distances Through Cells in Cylindrical Geometry and an Application to the Computation of Isophotes (open access)

Slant Path Distances Through Cells in Cylindrical Geometry and an Application to the Computation of Isophotes

In computer programs involving two-dimensional cylindrical geometry, it is often necessary to calculate the slant path distance in a given direction from a point to the boundary of a mesh cell. A subroutine, HOWFAR, has been written that accomplishes this, and is very economical in computer time. An example of its use is given in constructing the isophotes for a low altitude nuclear fireball.
Date: December 17, 2007
Creator: Symbalisty, Rodney Whitaker Eugene
Object Type: Report
System: The UNT Digital Library
SEADS 3.0 Sectoral Energy/Employment Analysis and Data System (open access)

SEADS 3.0 Sectoral Energy/Employment Analysis and Data System

SEADS 3.0, the Sectoral Energy/Employment Analysis and Data System, is a revision and upgrading of SEADS–PC, a software package designed for the analysis of policy that could be described by modifying final demands of consumer, businesses, or governments (Roop, et al., 1995). If a question can be formulated so that implications can be translated into changes in final demands for goods and services, then SEADS 3.0 provides a quick and easy tool to assess preliminary impacts. And SEADS 3.0 should be considered just that: a quick and easy way to get preliminary results. Often a thorough answer, even to such a simple question as, “What would be the effect on U. S. energy use and employment if the Federal Government doubled R&D expenditures?” requires a more sophisticated analytical framework than the input-output structure embedded in SEADS 3.0. This tool uses a static, input-output model to assess the impacts of changes in final demands on first industry output, then employment and energy use. The employment and energy impacts are derived by multiplying the industry outputs (derived from the changed final demands) by industry-specific energy and employment coefficients. The tool also allows for the specification of regional or state employment impacts, though …
Date: December 17, 2007
Creator: Roop, Joseph M.; Anderson, David A.; Schultz, Robert W. & Elliott, Douglas B.
Object Type: Report
System: The UNT Digital Library
A Non-Electrostatic Surface Complexation Approach to Modeling Radionuclide Migration at the Nevada Test Site: I. Iron Oxides and Calcite (open access)

A Non-Electrostatic Surface Complexation Approach to Modeling Radionuclide Migration at the Nevada Test Site: I. Iron Oxides and Calcite

Reliable quantitative prediction of contaminant transport in subsurface environments is critical to evaluating the risks associated with radionuclide migration. As part of the Underground Test Area (UGTA) project, radionuclide transport away from various underground nuclear tests conducted in the saturated zone at the Nevada Test Site (NTS) is being examined. In the near-field environment, reactive transport simulations must account for changes in water chemistry and mineralogy as a function of time and their effect on radionuclide migration. Unlike the K{sub d} approach, surface complexation (SC) reactions, in conjunction with ion exchange and precipitation, can be used to describe radionuclide reactive transport as a function of changing environmental conditions. They provide a more robust basis for describing radionuclide retardation in geochemically dynamic environments. The interaction between several radionuclides considered relevant to the UGTA project and iron oxides and calcite are examined in this report. The interaction between these same radionuclides and aluminosilicate minerals is examined in a companion report (Zavarin and Bruton, 2004). Selection criteria for radionuclides were based on abundance, half-life, toxicity to human and environmental health, and potential mobility at NTS (Tompson et al., 1999). Both iron oxide and calcite minerals are known to be present at NTS in …
Date: December 17, 2004
Creator: Zavarin, M & Bruton, C J
Object Type: Report
System: The UNT Digital Library
Correlated Nitrogen and Carbon Anomalies in an Anhydrous Interplanetary Dust Particle - Implications for Extraterrestrial Organic Matter Accreted by the Prebiotic Earth (open access)

Correlated Nitrogen and Carbon Anomalies in an Anhydrous Interplanetary Dust Particle - Implications for Extraterrestrial Organic Matter Accreted by the Prebiotic Earth

Given the ubiquitous presence of H and N isotopic anomalies in interplanetary dust particles (IDPs) and their probable association with carbonaceous material, the lack of similar isotopic anomalies in C has been a major conundrum. We report here the first observation of correlated N and C isotopic anomalies in organic matter within an anhydrous IDP. The {sup 15}N composition of the anomalous region is the highest seen to date in an IDP and is accompanied by a moderate depletion in {sup 13}C. Our observations establish the presence of hetero-atomic organic compounds of presolar origin among the constant flux of carbonaceous material accreting to the terrestrial planets within IDPs. Theoretical models suggest that low temperature formation of organic compounds in cold interstellar molecular clouds does produce C and N fractionations, but it remains to be seen if these models can reproduce the specific effects we observe here.
Date: December 17, 2003
Creator: Floss, C; Stadermann, F J; Bradley, J P; Dai, Z; Bajt, S & Graham, G
Object Type: Article
System: The UNT Digital Library
Kinematics of Gamma-Ray Burst and their Relationship to Afterglows (open access)

Kinematics of Gamma-Ray Burst and their Relationship to Afterglows

A strong correlation is reported between gamma-ray burst (GRB) pulse lags and afterglow jet-break times for the set of bursts (seven) with known redshifts, luminosities, pulse lags, and jet-break times. This may be a valuable clue toward understanding the connection between the burst and afterglow phases of these events. The relation is roughly linear (i.e. doubling the pulse lag in turn doubles the jet break time) and thus implies a simple relationship between these quantities. We suggest that this correlation is due to variation among bursts of emitter Doppler factor. Specifically, an increased speed or decreased angle of velocity, with respect to the observed line-of-site, of burst ejecta will result in shorter perceived pulse lags in GRBs as well as quicker evolution of the external shock of the afterglow to the time when the jet becomes obvious, i.e. the jet-break time. Thus this observed variation among GRBs may result from a perspective effect due to different observer angles of a morphologically homogeneous populations of GRBs. Also, a conjecture is made that peak luminosities not only vary inversely with burst timescale, but also are directly proportional to the spectral break energy. If true, this could provide important information for explaining the …
Date: December 17, 2001
Creator: Salmonson, J D
Object Type: Article
System: The UNT Digital Library
Evaluating Cumulative Ecosystem Response to Restoration Projects in the Lower Columbia River and Estuary, 2008 (open access)

Evaluating Cumulative Ecosystem Response to Restoration Projects in the Lower Columbia River and Estuary, 2008

Draft annual report for the Cumulative Effects Study for the US Army Corps of Engineers, Portland District
Date: December 17, 2009
Creator: Johnson, Gary E.; Diefenderfer, Heida L.; Borde, Amy B.; Dawley, Earl M.; Ebberts, Blaine D.; Roegner, G. Curtis et al.
Object Type: Report
System: The UNT Digital Library
CHARACTERIZATION OF THE TANK 18F SAMPLES (open access)

CHARACTERIZATION OF THE TANK 18F SAMPLES

The Savannah River National Laboratory (SRNL) was asked by Liquid Waste Operations to characterize Tank 18F closure samples. Tank 18F slurry samples analyzed included the liquid and solid fractions derived from the 'as-received' slurry materials along with the floor scrape bottom Tank 18F wet solids. These samples were taken from Tank 18F in March 2009 and made available to SRNL in the same month. Because of limited amounts of solids observed in Tank 18F samples, the samples from the north quadrants of the tank were combined into one North Tank 18F Hemisphere sample and similarly the south quadrant samples were combined into one South Tank 18F Hemisphere sample. These samples were delivered to the SRNL shielded cell. The Tank 18F samples were analyzed for radiological, chemical and elemental components. Where analytical methods yielded additional contaminants other than those requested by the customer, these results were also reported. The target detection limits for isotopes analyzed were 1E-04 {micro}Ci/g for most radionuclides and customer desired detection values of 1E-05 {micro}Ci/g for I-129, Pa-231, Np-237, and Ra-226. While many of the minimum detection limits, as specified in the technical task request and task technical and quality assurance plans were met for the species …
Date: December 17, 2009
Creator: Oji, L.; Click, D. & Diprete, D.
Object Type: Report
System: The UNT Digital Library
VALIDATION OF ANALYTICAL METHODS AND INSTRUMENTATION FOR BERYLLIUM MEASUREMENT: REVIEW AND SUMMARY OF AVAILABLE GUIDES, PROCEDURES, AND PROTOCOLS (open access)

VALIDATION OF ANALYTICAL METHODS AND INSTRUMENTATION FOR BERYLLIUM MEASUREMENT: REVIEW AND SUMMARY OF AVAILABLE GUIDES, PROCEDURES, AND PROTOCOLS

This document proposes to provide a listing of available sources which can be used to validate analytical methods and/or instrumentation for beryllium determination. A literature review was conducted of available standard methods and publications used for method validation and/or quality control. A comprehensive listing of the articles, papers, and books reviewed is given in Appendix 1. Available validation documents and guides are listed in the appendix; each has a brief description of application and use. In the referenced sources, there are varying approaches to validation and varying descriptions of validation at different stages in method development. This discussion focuses on validation and verification of fully developed methods and instrumentation that have been offered up for use or approval by other laboratories or official consensus bodies such as ASTM International, the International Standards Organization (ISO) and the Association of Official Analytical Chemists (AOAC). This review was conducted as part of a collaborative effort to investigate and improve the state of validation for measuring beryllium in the workplace and the environment. Documents and publications from the United States and Europe are included. Unless otherwise specified, all documents were published in English.
Date: December 17, 2008
Creator: Ekechukwu, A.
Object Type: Article
System: The UNT Digital Library