The production of cross-type control rods having a span of 4-7/8 in., and an arm thickness of 1/8 in., was studied. Extrusion techniques were developed for producing cross-type control rods from each of two alloys; one containing 75% silver-25% cadmium, and the other containing 67% silver-30% cadmium-3% copper. Fabrication of the extruded crosses into clad control rods for the Mark I naval reactor was attempted. A set of unclad control rods for the Zero Power Reactor was produced. The effect of copper, nickel, aluminum, palladium, and indium, singly and in various combinations, on the physical and mechanical properties of silver cadmium was studied. Data are given on the work hardening and annealing of binary silver-cadmium alloys, and on the precipitation hardening of certain complex silver cadmium alloys. A materials specification and suggested fabrication procedure were established for nickel-clad extruded silver-cadmium control rods.

Progress is reported on (1) experimental breeder reactor program, (2) solvent extraction, (3) fluoride volatilization separation process, (4) elevated temperature separations, (5) denitration of uranyl nitrate in a fluidized bed, (6) development of analytical techniques, (7) processing and utilization of radioactive wastes.

In the a study of plutonium production, the analytical solutions of the various isotope production equations are difficult and time consuming when spatial variation of the flux is considered. In an effort to reduce the time and labor required to determine the integrated production of a given thermal reactor, a graphical method of analysis is presented. The method is based on the assumption that the reactor may be divided into a relatively small number of regions such that the flux in each of these regions may be assumed constant. The production of the given isotope for each region is then read from the appropriate graph. The total production is obtained by adding the productions of all the regions.

Report describing the research and development activities related to nuclear chemistry and radiochemistry and basic chemistry conducted by the Argonne National Laboratory Chemistry Division, Section C-1.

This report was written by different scientist on various experiments of solid state, physical chemistry, radiochemistry and analytical, and special problems.

This report deals with the (1.1) physical properties of graphite, (1.2) effects of pile irradiation on the properties of graphite, (1.3) effect of irradiation on "ceramic" materials, (1.4) effects of radiation on ice -- the x-ray induced luminescence of ice, (1.5) investigation of color centers and other optical properties of single crystals. (2.1) radiation chemistry of liquids, (2.2) application of mass spectrometry to chemical problems, (2.3) vapor pressure and heat of vaporization of uranium, (3.1) nuclear properties of Zr93 and Nb93m from fission, (3.2) mass distribution in the spontaneous fission of Cm242, (3.3) Upper limit to the lifetimes of the first excited states of Th236, U234, and Pu236, (3.4) on the one-body model of alpha radioactivity, (4.1) spectrographic analysis, (4.2) chemical analysis, (5.1) paramagnetic resonance measurements, and (5.2) the 60-inch cyclotron.

Report issued by the Argonne National Laboratory over design studies conducted on Argonaut reactors for training and research purposes. As stated in the abstract, "the design presented in the form of a steady-state analysis based upon the small-signal linearization of the reactor kinetics transfer function. The measured controller performance and construction details of the equipment is given" (p. 7). This report includes tables, illustrations, and photographs.

From Abstract: "This report describes a counting system capable of processing input pulses at an average rate in excess of 3 x 10 to the fifth power counts per second with less than 10 percent counting loss due to instrumental dead time."

Report regarding the fabrication of a transparent meltdown facility for the purpose of photographing simulated meltdowns.

Report containing a method "for comparing the influence of various fuel element geometries on rector core shape or different specifications of thermal performance"(p. 7).

Report issued by the Argonne National Laboratory discussing the design and construction of equipment for reactor fuels. As stated in the summary, "the report describes the development, prototype construction, methods of testing, and leak detection of a modular hood design to be used in housing equipment and processes for the Argonne National Laboratory Fuel Fabrication Facility" (p. 9). This report includes tables, illustrations, and photographs.

Water corrosion tests on mechanically jacketed and pinholed thorium slugs show that these slugs fail in a manner similar to that observed for mechanically jacketed and tested uranium slugs. The proposed mechanism for the water corrosion of these jacketed slugs is analogous to the water corrosion mechanism of jacketed uranium slugs presented in the project lecture. A bare thorium slug appeared to be more resistant to corrosion by water than a mechanically jacketed slug during the first half of the autoclave test. After approximately 90 hours of testing both the bare and the mechanically jacketed thorium slugs were severely corroded by water.

A fuel element assembly in which a uranium slug is bonded to an impact extruded aluminum can by means of aluminum-silicon eutectic, and in which the can is capped with a thin aluminum disc, brazed and welded to the can, may contain,(a) imperfections common to brazed and welded metal sections, and (b) inhomogeneities arising from oxidation of uranium, and alloy formation between uranium, aluminum and silicon.

This report deals with the (1.1) physical properties of graphite, (1.2) effects of pile irradiation on the properties of graphite, (1.3) effect of irradiation on "ceramic" materials, (1.4) effects of radiation on ice -- the x-ray induced luminescence of ice, (1.5) investigation of color centers and other optical properties of single crystals. (2.1) radiation chemistry of liquids, (2.2) application of mass spectrometry to chemical problems, (2.3) vapor pressure and heat of vaporization of uranium, (3.1) nuclear properties of Zr93 and Nb93m from fission, (3.2) mass distribution in the spontaneous fission of Cm242, (3.3) Upper limit to the lifetimes of the first excited states of Th236, U234, and Pu236, (3.4) on the one-body model of alpha radioactivity, (4.1) spectrographic analysis, (4.2) chemical analysis, (5.1) paramagnetic resonance measurements, and (5.2) the 60-inch cyclotron.

On June 2, 1952, 15:52 hours, a large reactivity change was made manually in a ZPR-1 assembly causing a power excursion of about one kwh, which resulted in damage to the reactor core components and radiation exposure of some of the operating personnel to perhaps several rep. None of the contributing causes is reviewed here nor are the measures which were taken to reduce the probability of a recurrence discussed since these are considered administrative matters beyond the scope of this technical report. It is intended only to describe the incident, estimate the exposures and present available clinical data.