A series of W-5 Re/W-26 Re thermocouples have been electron beam welded at the Hamilton Standard Division at our request. This technical report is a summary of our evaluation of these joints. These weldments did exhibit incomplete fusion in cap welds and some porosity in undesirable lead junction shapes. In fairness, this was a single attempt to make a difficult joint, and the objective of ungrounded 1/16 OD clad joints was met. As noted by Hamilton, two changes are necessary to improve this joint design: (1) swaging to forming the clad end rather than crimping prior to cap welding. (2) using a fixture with rotary motion on a tilting axis.

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Comparisons between experimental data obtained from single-phase gaseous hydrogen cool-down with those computed from a computer program have shown excellent agreements.

Technical report. From report : "The method of least squares refinement is based on the prediction of the theory of errors that, if the errors of the observed structure factors follow the Gaussian distribution, the most nearly correct atomic parameters will be those which result in the minimization of the residual R = Σi [√wi(|Fo| - |Fc|)i]2."

Technical report. From Abstract : "The crystal structure of bis(meta-chlorobenzoyl) methane has been determined by three dimensional anisotropic least squares refinement of scintillation counter data. The molecule was found to be nearly planar with a maximum deviation from the least squares molecular plane of 0.068Å and an average deviation of 0.023Å. Fourier transform techniques to locate phenyl rings provided the key to the structure determination. The intramolecular bond distances and thermal parameters of the oxygen atoms support a resonant, enol ring with a symmetric, intramolecular hydrogen bond. The structure confirms conslusions from the structure of bis(meta-bromobenzoyl) methane where the symmetry of the molecule was forced by the crystal symmetry."