Ten-Cycle Bench-Scale Study of Simplified Clay-Hydrogen Chloride Process for Alumina Production (open access)

Ten-Cycle Bench-Scale Study of Simplified Clay-Hydrogen Chloride Process for Alumina Production

From abstract: This U.S. Bureau of Mines (USBM) research simplified an earlier hydrogen chloride (HCl) leachsparge process developed by the USBM to recover reduction-grade alumina from domestic kaolin clay. Improvements were made by decreasing the initial leaching acid concentration from 25 to 20 pct, decreasing the leaching time from 1 to 2 h to 15 to 30 min, eliminating the solvent extraction step for Fe removal, and eliminating the step to recover the Al content of the bleedstream circuit. A 10-cycle bench-scale experiment of the simplified process showed that the ferric chloride (FeC 3) concentration built up to 9.3 g/L in the recycle stream. This did not interfere with any of the unit operations or final alumina product purity because Fe forms stable soluble chloride complexes when sparged with HC and is easily washed from the large aluminum chloride hexahydrate (ACH) crystals. The reduced leaching time and acid concentration did not decrease Al extraction.
Date: 1995
Creator: Shanks, D. E.
System: The UNT Digital Library
Argonne National Laboratory-East Site Environmental Report for Calendar Year 1994 (open access)

Argonne National Laboratory-East Site Environmental Report for Calendar Year 1994

This report discusses the results of the environmental protection program at Argonne National Laboratory-East (ANL) for 1994. To evaluate the effects of ANL operations on the environment, samples of environmental media collected on the site, at the site boundary, and off the ANL site were analyzed and compared to applicable guidelines and standards. A variety of radionuclides was measured in air, surface water, groundwater, soil, grass, and bottom sediment samples. In addition, chemical constituents in surface water, groundwater, and ANL effluent water were analyzed.
Date: May 1995
Creator: Golchert, N. W. & Kolzow, R. G.
System: The UNT Digital Library
Physics Division Annual Review: April 1, 1994-March 31, 1995 (open access)

Physics Division Annual Review: April 1, 1994-March 31, 1995

Annual report of activities of the Argonne National Laboratory Physics Division, including heavy-ion nuclear physics research, operation and development of ATLAS, medium-energy nuclear physics research, theoretical physics, atomic and molecular physics research.
Date: August 1995
Creator: Argonne National Laboratory. Physics Division.
System: The UNT Digital Library
Mineral and Energy Resources of the Roswell Resource Area, East-Central New Mexico (open access)

Mineral and Energy Resources of the Roswell Resource Area, East-Central New Mexico

The following report presents geological data taken from studies made on the mineral and energy resources in the surface and subsurface within the Roswell Resource Area in east-central New Mexico.
Date: 1995
Creator: Bartsch-Winkler, S. & Donatich, Alessandro J.
System: The UNT Digital Library