BS>The preparation of niobium was attempted by a number of chemical and electrochemical routes. Chemical reduction of oxides and halides such as Nb/sub 2/O/sub 5/, K/sub 2/NbOF/sub 5/, K/sub 2/NbF/sub 7/, and NbCl/sub 5/ was conducted with varying degrees of success. Aqueous electrochemical reduction has not yet yielded a metallic deposit. The electrolysis of molten baths containing K/sub 2/NbOF/sub 5/ or K/sub 2/NbF/sub 7/ produced niobium metal. The more promising methods of preparation for Nb metal at the present time include the reaction of Nb/sub 2/O/sub 5/ with C, the H/sub 2/ and active metal reduction of NbC1/sub 5/, and electrolysis of K/sub 2/NbF/sub 7/- NaC1 melts. (auth)

In this report ten cases of acute radiation syndrome are described resulting from two accidents occurring at the Los Alamos Scientific Laboratory of unique nature involving fissionable material. These cases are described in considerable detail. The report comprises ten sections. This volume, part II of the report, is comprised of sections entitled: (1) the Biological Basis for the Clinical Response seen in the Acute radiation Syndrome, (2) Clinical Signs and Symptoms, (3) Discussion of Hematological Findings, (4) Chemistry of the Blood and Urine, (5) Discussion of Pathological Findings, and (6) Reconsiderations of the Calculated Radiation Doses in Terms of the Observed Biological Response of the Patients. This report was prepared primarily for the clinician who is interested in radiation injuries and therefore emphasis has been placed on the correlation of clinical and pathological changes with the type of cytogenetic change known to be produced by ionizing radiation.

The efficient prosecution of the research and process development on polonium, radium, actinium, waste disposal, and alpha-neutron sources requires the use of a wide variety of instrumental techniques such as: alpha, beta, gamma, and neutron counters and survey meters; emission, absorption, and mass spectroscopy: x-ray and electron diffraction; microbalances; and calorimeters. The complex and kaleidoscopic aspects of our research program require; (1) The application of standard instruments and techniques to a variety of problems; (2) The development of new techniques for the use of standard instruments; and (3) The development of new or improved Instruments. The sum of the above three categories constitutes the field of supporting research. The amplifier for counting pulses of wide dynamic range which was developed for counting beta particles in the presence of alphas has operated so satisfactorily that it has been decided to attempt to adopt it for neutron counting. Substantial improvement at medium counting rates has already been obtained but results at high counting rates are not as satisfactory. The development of a survey meter for monitoring fast neutrons has been under way for sometime. The attainment of higher efficiency has been attempted by the use of a dual-chambered counter tube. The tube …

This quarterly progress report gives an overview of the University of Rochester Atomic Energy Project for April 1, 1950 thru June 30, 1950. Sections included are entitled (1) Biological Effects of External Radiation (X-rays and gamma rays), (2) Biological Effects of External Radiation (Infra-red and ultraviolet), (3) Biological effects of radioactive materials (polonium, radon, thoron, and miscellaneous project materials), (4) Uranium, (5) Beryllium, (7) thorium, (8) fluoride, (9) zirconium, (10) special materials, (11) Isotopes, (12) Outside services, (12) Project health, (13) Health physics, (14) Special Clinical Service, and (15) Instrumentation (Spectroscopy, electron microscopy, x-ray and nuclear radiation detectors, x-ray diffraction, and electronics).

Quarterly progress report of the unclassified sections at Brookhaven National Laboratory providing updates about research and findings.

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This is a progress report of the production reactors on the Hanford Reservation for the month of November 1950. This report takes each division (e.g. manufacturing, medical, accounting, occupational safety, security, reactor operations, etc.) of the site and summarizes its accomplishments and employee relations for that month.

This is a progress report of the production reactors on the Hanford Reservation for the month of September 1950. This report takes each division (e.g., manufacturing, medical, accounting, occupational safety, security, reactor operations, etc.) of the site and summarizes its accomplishments and employee relations for that month.